Edward Oconnor

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4,5-bridged-2,3,4,5-tetrahydro-1H-3-benzazepine-7-ols and derivatives and compositions and methods employing such compounds

4,5-CYCLOALKANO-3-BENZAZEPIN-7-OL-DERIVATIVES and Their Use

Cyclopropanation Using an Iron-Containing Methylene Transfer Reagent: 1,1-Diphenylcyclopropane

Organic Syntheses, 2003

Cyclopropanation using an iron-containing methylene transfer reagent: 1,1-diphenylcyclopropane re... more Cyclopropanation using an iron-containing methylene transfer reagent: 1,1-diphenylcyclopropane reactant: cyclopentadienyliron dicarbonyl dimer [C5H5(CO)2Fe]2, (0.50 mol equiv, 0.21 mol, 74.4 g; and ) intermediate: (η5-C5H5)(CO)2FeCH2S+(CH3)2 BF4− product: 1,1-diphenylcyclopropane solvent: nitromethane Keywords: alkylation, miscellaneous; cyclization, free radical-carbenoid/nitrenoid; cyclopropanation; metalation reactions, iron; metal-catalyzed reactions, iron; dioxane; nitromethane; tetrahydrofuran; chloromethyl methyl sulfide, stench, potential poison; dioxane, cancer suspect agent; methyl iodide; nitromethane, potential explosive; sodium, dispersion in mineral oil, fire hazard; stopcock to allow simultaneous addition of liquid reagents and inert gases

Generation of (.eta.5-cyclopentadienyl)dicarbonyliron carbene complexes via protonation of the corresponding alkenyl complexes

Journal of the American Chemical Society, 1982

... Acknowledgment. We are grateful to J. Lundquist, Roche A/S, for providing the sample of 15,15... more

Stable precursors of transition-metal carbene complexes. Simplified preparation and crystal structure of (.eta.5-cyclopentadienyl)[(dimethylsulfonium)methyl]dicarbonyliron(II) fluorosulfonate

Journal of the American Chemical Society, 1982

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A versatile new synthesis of organic compounds with chiral methyl groups: stereochemistry of protolytic rhenium-carbon bond cleavage in chiral alkyl complexes (.eta.5-C5H5)Re(NO)(PPh3)(R)

Journal of the American Chemical Society, 1987

Page 1. J. Am. Chem. SOC. 1987, 109, 4837-4844 4837 for the calculated ordering 3d &gt; 4d &a... more

Synthesis of (1, 2-13C2) 2-phosphoglycolic acid

Journal of Labelled Compounds and Radiopharmaceuticals, 1994

The synthesis of (1,2- 13C2) 2-phosphoglycelic acid, 5, from commercially-available (1,2- 13C2) b... more

Stable precursors of transition-metal carbene complexes. Simplified preparation and crystal structure of (. eta. 5-cyclopentadienyl)[(dimethylsulfonium) methyl] …

Journal of the American Chemical …, 1982

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(. eta. 5-C5H5)(CO) 2FeCH2S+ (CH3) 2 BF4-: a methylene transfer reagent for the direct cyclopropanation of alkenes

Journal of the American …, 1987

... Chem. 1986, 51, 1960. (e) Mohamadi, F.; Still, WC Tetrahedron Lett. 1986, 27, 893. 1,3-Coupli... more

4,5-bridged-2,3,4,5-tetrahydro-1H-3-benzazepine-7-ols and derivatives and compositions and methods employing such compounds

4,5-CYCLOALKANO-3-BENZAZEPIN-7-OL-DERIVATIVES and Their Use

Cyclopropanation Using an Iron-Containing Methylene Transfer Reagent: 1,1-Diphenylcyclopropane

Organic Syntheses, 2003

Generation of (.eta.5-cyclopentadienyl)dicarbonyliron carbene complexes via protonation of the corresponding alkenyl complexes

Journal of the American Chemical Society, 1982

... Acknowledgment. We are grateful to J. Lundquist, Roche A/S, for providing the sample of 15,15... more

Stable precursors of transition-metal carbene complexes. Simplified preparation and crystal structure of (.eta.5-cyclopentadienyl)[(dimethylsulfonium)methyl]dicarbonyliron(II) fluorosulfonate

Journal of the American Chemical Society, 1982

Download

A versatile new synthesis of organic compounds with chiral methyl groups: stereochemistry of protolytic rhenium-carbon bond cleavage in chiral alkyl complexes (.eta.5-C5H5)Re(NO)(PPh3)(R)

Journal of the American Chemical Society, 1987

Page 1. J. Am. Chem. SOC. 1987, 109, 4837-4844 4837 for the calculated ordering 3d &gt; 4d &a... more

Synthesis of (1, 2-13C2) 2-phosphoglycolic acid

Journal of Labelled Compounds and Radiopharmaceuticals, 1994

The synthesis of (1,2- 13C2) 2-phosphoglycelic acid, 5, from commercially-available (1,2- 13C2) b... more

Stable precursors of transition-metal carbene complexes. Simplified preparation and crystal structure of (. eta. 5-cyclopentadienyl)[(dimethylsulfonium) methyl] …

Journal of the American Chemical …, 1982

Download

(. eta. 5-C5H5)(CO) 2FeCH2S+ (CH3) 2 BF4-: a methylene transfer reagent for the direct cyclopropanation of alkenes

Journal of the American …, 1987

... Chem. 1986, 51, 1960. (e) Mohamadi, F.; Still, WC Tetrahedron Lett. 1986, 27, 893. 1,3-Coupli... more

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