Asian Journal of Water, Environment and Pollution, Vol. 15, No. 3 (2018), pp. 79–92.
DOI 10.3233/AJW-180046
Formulation, Physicochemical Analysis, Sustainable
Packaging-Storage Provision, Environment Friendly
Drying Techniques and Energy Consumption
Characteristics of Mango Leather Production: A Review
Tanmay Sarkar and Runu Chakraborty*
Food Technology and Biochemical Engineering Deprtment, Jadavpur University, Kolkata, India
* crunu@hotmail.com
Received March 14, 2018; revised and accepted April 6, 2018
Abstract: Mango leather is a dehydrated, flexible product prepared from ripe mango pulp having a sheet like
structure and consumed as dessert or snack. It is prepared with different formulations along with mango pulp,
sucrose, skim milk powder, gellan gum, coconut powder etc. Different formulations and physicochemical tests
have been done by researchers to ascertain desirable composition and nutrient characteristics of mango leather.
Drying techniques such as Sun drying, hot air drying, vacuum drying, microwave oven drying and infra-red
drying have been employed by researchers to dry the mango pulp and the dehydration behaviour in different
dryers had been studied. Mathematical modelling of the drying operation have been considered also. The energy
consumption during these drying processes is studied to suggest an eco-friendly dehydration option for mango
leather processing industry. The aim of the paper is to review the published papers on mango leather and to give
a collective view on methods of preparation, effects of drying condition, and effects of packaging and storage
for a sustainable ecosphere.
Key words: Mango leather, formulation, eco-friendly drying, energy consumption, sustainable packaging.
Introduction
The mango (Mangifera indica Linn.) belongs to the
Anacardiaceae family and due to its flavour, taste and
fragrance it is called the “King of fruits” (Nunes et
al., 2007). Apart from sensory superiorities, mango
have significant amount of bioactive compounds with
antioxidant activity. Ripe mango contains high gallic
acid and total polyphenols (Danalache et al., 2014).
The significant amount of vitamin C, β carotene and
minerals in ripe mango are helpful in prevention of
cardiovascular disease and cancer (Alothman et al.,
2010; Liu, 2003; Sanchez-Robles et al., 2009).
*Corresponding Author
More than 1000 varieties of mango are being
cultivated over the world occupying the second position
as a tropical crop in terms of production and coverage
area of cultivation (Solís-Fuentes and Durán-de-Bazúa,
2011; Muchiri et al., 2012). India produces 66% of total
world mango production (Shafique et al., 2006) and
holds the first position (Jahurul et al., 2015). Improper
post-harvest management and processing causes more
than 30% wastage (Carrillo-lopez et al., 2000; Rathore
et al., 2007). As mango is a climacteric fruit, improper
harvesting time, condition of ripening, and absence of
suitable storage facilities affect the price and availability
of mango. For the same reasons large portion of the
80
Tanmay Sarkar and Runu Chakraborty
produce is wasted (Lalel et al., 2003). Only about 2%
of total mango produced is processed whereas 20-30%
of total production is spoiled which costs about 480
million dollar (FAO, 2004).
Mango contains 81.7% of moisture; due to this high
moisture content it is perishable in nature and consumed
mostly as fresh (Hashmi et al., 2007). To obtain the
taste and benefits of mangoes at off season a variety
of processed mango products are produced like juice,
mango bar, jam, jelly, mango powder, canned mango
slices, mango purees and mango leather (Djantou et al.,
2011; Ledeker et al., 2014, Liu et al., 2014, Sogi et al.,
2015; Sriwimon and Boonsupthip et al., 2011; Hussain
et al., 2003). Among all these mango products mango
leather is most popular in India (Danalache et al., 2014).
Mango leather or mango bar can be produced by
dehydration of fresh mango pulp or pulp accompanied
by other ingredients (Raab and Oehler, 1976; Huang
and Hsieh, 2005; Maskan et al., 2002; Diamante et al.,
2014). Simultaneous moisture and heat transfer are the
main characteristics of drying through which perishable
ripe mango pulp can be transformed to mango leather
and can be suitable for long term storage (FAO, 2004).
Researchers formulate it with different components like
sugar, soy flour, skim milk powder, coconut powder,
pectin, acid, gum, preservatives etc. along with mango
pulp to meet desired sensory and textural property. The
evaporation of moisture from pulp along with other
ingredients gives the cohesive leathery texture of mango
leather (Vatthanakul et al., 2010).
To ascertain the desired quality of the processed mango
leather, researchers have done various physicochemical
analysis on it like proximate analysis, total ascorbic
acid content, determination of colour, textural analysis,
sensory analysis etc. Subject to the aim of research the
researchers optimise their formulation based on the test
results found.
Sun drying, being the most simplest and traditional
drying method, is used from the ancient period of
mankind. Though it gives natural colour and good
texture of final product, the exposure to ambient
environment and high time consumption are the
problems associated with this kind of drying technique
(Maskan et al., 2002). With progress in technology,
more effective drying techniques are employed to
produce mango leathers. The alternative drying methods
are like hot air drying, microwave drying, vacuum
drying, infra-red drying etc.
Most of the industries use convective type hot air
oven for drying. Direct and indirect drying processes
may cause crystallisation, shrinkage, puffing and desired
or undesired biochemical reaction which ultimately
affects the sensory, textural and nutritional qualities of
mango leather (Diamante et al., 2014). Researchers have
proposed different mathematical models for different
kind of drying operations to predict the dehydration
behaviour of the mango pulp.
Sun drying is free and renewable source of energy
suitable for small scale industry but not for medium and
large scale industry (Tiwari, 2016). Convection dryers
are not economically viable for medium and small scale
industries in developing countries like India (Ibrahim
et al., 2009; Jayaraman and Gupta, 1995; Banout et al.,
2010; Boughali et al., 2009). A substantial amount of
thermal energy is lost in convective drying as well as
inferior heat transfer quality is another disadvantage of
hot air drying. Infra-red dryers provide rapid drying and
low operational cost (Brooker et al., 1992; Strumillo,
1987; Nonhebel, 1973). Microwave drying is fastest
mode of drying as electromagnetic energy converted
directly to the kinetic energy during this process but
cell damage is the constrain associated with whereas
vacuum drying approach facilitates better quality of
product (Krulis et al., 2005; Kompany, 1993; Jaya and
Das, 2003; Zhang et al., 2006).
In this era of globalisation and competitive market
packaging and storage of mango leather to expand
its shelf life with respect to moisture content, water
activity, microbial stability, texture and acceptability are
the prime concern for industries (Irwandi et al., 1998).
The aim of this study is to consider the preparation
method for mango leather, the effect of formulation
on texture, sensory qualities, and the physicochemical
tests to obtain the quality parameters. In this study
the method of dehydration of mango pulp, the energy
consumption behaviour of these dehydration techniques
and packaging-storage conditions of mango leather are
also reviewed.
Method of Preparation
In general after receiving of fresh ripe mango it is
washed with potable water and then sorting is done.
Thereafter peeling and cutting operations are involved.
After extraction of pulp from ripe mangoes it may or
may not be blanched, then mixed with other ingredients
followed by heating which is an optional operation
depending on the method used. Then drying of pulp
is done followed by cutting, packing and labelling.
The schematic flow chart of general mango leather
production is shown in Figure 1.
Mango Leather Production: A Review
Figure 1: Flow chart of mango leather preparation.
Formulation of Mango Leather
Researchers have found different design to formulate
mango leather in order to meet shortcomings from
their point of view. Mir and Nath (1995) have prepared
mango bar from mangoes of Langra cultivar. After
washing, peeling and pulping it has been heated for 2
min at 91-93°C. They have increased the TSS to 30% by
addition of powdered cane sugar, 0.6% of CA and 1734
81
ppm potassium metabisulphite (KMS) as preservative.
Gowda et al. (1995) have prepared mango fruit bar
from Alphanso cultivar. 20% sugar, 0.2% CA and 700
ppm KMS are added to the pulp and dried to get good
quality of mango bar. Similar kind of formulation is
deliberated by Prasad and Nath (2002) where they
use mangoes of Totapuri cultivar; after washing,
peeling, pulping and it was heated for 2 min at 85°C.
Total soluble solids of pulp was raised to 30% using
powdered cane sugar, and 0.6% citric acid; whereas the
preservative KMS is replaced by 1000 ppm SO2 (Prasad
and Nath, 2002).
In a recent study Effah-Manu et al. (2013) have
prepared mango-sweet potato leather. They have used
mango of Keitt variety. The sweet potatoes have been
baked in an oven at 150-220°C for 2 h, 2.5 h and 3 h to
convert the starch to dextrin. Then it is cooled at 30°C
and the edible portion of sweet potatoes is homogenized
in a blender; thereafter it is mixed with mango pulp in
30:70, 20:80 and 10:90 ratios respectively. 0.1% sodium
benzoate and 0.2% citric acid are added to it. The final
mixture is smeared on 7 mm × 7 mm aluminium trays
coated with glycerol and dried. Though the overall
acceptability of this leather is good but the amount of
sweet potatoes incorporated is found insignificant by
researchers (Effah-Manu et al., 2013).
The plain mango leather from mango pulp of cultivar
Tommy Atkins is prepared by Azeredo et al. (2006)
without addition of any preservative. The mango puree
is passed through 1-mm sieve and the pulp is dried
to obtain leather with moisture content 15-18% and
optimise the time and temperature for production of the
mango leather. The synergistic effect of pH and water
activity inhibit microbial growth; thus, mango leathers
with shelf-life for several months has been produced
without the need of chemical preservatives.
A different kind of mango bar is formulated by
Florina Danalache et al. (2014) where they have used
mangoes of cultivar Palmer; after washing and cutting
it is pureed at room temperature by blender. The pulp
is heated at 88 ± 2°C in a water bath with addition of
1 gm of gellan powder per 100 gm of mango puree
with continuous stirring at a rotation speed of 1640
G using a four-blade impeller. The mixture is poured
in a rectangular silicone mould and kept at 22 ± 2°C
temperature to set.
Gujral and Khanna (2002) prepared mango leather
from Safaida variety, which is washed, peeled and
pulped. The pulp with TSS 10.6% has been blanched
at 80°C for 5 min, then cooled and 0.2% w/w of KMS
has been added to it. The mango pulp has been mixed
82
Tanmay Sarkar and Runu Chakraborty
with soy protein concentrate (0%; 4.5%; 9%), skim milk
powder (0%; 4.5%; 9%) and sucrose (0%; 4.5%; 9%).
250 g of this mixed pulp was poured on aluminium
trays of dimension 25.5 cm × 13 cm × 2 cm. After
drying it has been found that mango leather containing
4.5% skim milk powder and 4.5% sucrose is the most
acceptable (Gujral and Khanna, 2002).
Mangoes of Langra cultivar have been washed,
peeled and pulped by Gujral and Brar (2003). The
pulp was blanched at 80°C temperature for 5 min,
after cooling 0.2% of KMS has been added. 20%
of sugar has been added to the pulp of total solid
14.3% to increase its sweetness and total solids. Then
hydrocolloid has been incorporated to the mango pulp
at concentrations of 1, 2, and 3% w/w respectively.
250 g of this mixture has been spread over 25.5 cm ×
13 cm × 2 cm aluminum trays. After drying it is found
that incorporation of hydrocolloid significantly modified
the texture of mango leather. They also found that with
redness (a) and yellowness (b) values of mango leather
drop with increasing concentration of hydrocolloid
whereas the concentration of hydrocolloid has been
found insignificant in case of lightness value (L).
Gujral et al. (2013) produced mango leather by
blanching of pulp at 80°C for 5 min to inactivate
enzymes followed by addition of 1000 ppm of KMS as
preservative, sucrose at concentration of 0, 5, and 10%,
pectin at concentration of 0, 1, and 2%, maltodextrin
in concentration of 0, 2.5 and 5% and has been kept
overnight for hydration. Finally 300 g of this mixed
pulp has been poured in aluminum trays measuring
0.3 m × 0.1 m × 0.03 m. They found that drying rate,
drying rate constant and effective moisture diffusivity
have been significantly affected by the additives like
sucrose, pectin and maltodextrin.
G. Puspa et al. (2006) used Alphonso mango pulp
with 16% TSS along with sugar (50 g), corn flour (5
g), and lime juice (2 g) at different specified level in
mango leather preparation. Skim milk powder and
roasted defatted soy flour with 51.8% of protein content
is mixed together in the ratio of 1:1; this mixture has
been finally mixed with mango pulp at concentration of
10, 15, 20 and 25%. After drying it has been found by
the researchers that colour retention is higher for mango
leather enriched with 20 and 25% soy flour. Whereas
the mango leather enriched with 10 and 15% soy flour
have significantly higher values of sensory attributes.
Mango bar has been prepared by Prasad (2009) from
pulp of Totapuri cultivar. After washing, peeling and
pulping it has been acidified to 0.3% CA and blanched
at 85°C temperature for 5 min to inactivate enzymes.
Powdered cane sugar has been added in different extent
to this pulp to increase the TSS to 20, 25 and 30%. To
this mixture, roasted Bengal Gram flour and skim milk
powder has been added in concentration of 0, 5 and
10%. Citric acid has been added in order to maintain
acidity at 0.3, 0.45 and 0.6%. The final mixture has
been spread over stainless steel trays and dried. It has
been found that 5% (w/w) roasted Bengal gram and 5%
(w/w) skim milk powder at concentration gave superior
sensory qualities.
Parekh et al. (2014) prepared mango bar from
Kesar cultivar fortified with DCP (Desiccated coconut
powder). After washing and pulping of mango the pulp
has been passed through stainless steel sieve of 1 mm
mesh. The pulp has been blanched to destroy enzyme at
91-93 °C for 2 min and cane sugar has been incorporated
to increase the TSS at 30° Brix. KMS has been added
to the pulp at level of 0 and 1734 ppm, DCP has been
added to pulp at concentration of 0, 1, 2 and 3%. The
final mixture has been spread over trays smeared with
glycerine followed by drying. Investigators have found
that the mango bar with 2% DCP and 1734 ppm of KMS
has best sensory attributes, whereas interaction effect
of the treatment recipes has been found insignificant.
Methods of Drying
Sun Drying
When mango pulp is spread over metal tray for drying
an uneven surface is created. When Sun rays of shorter
wavelength fall on this rough surface, a part of it is
reflected back and the rest get absorbed by pulp. The
Sun rays of long wavelength cannot be absorbed by
pulp. The colour of mango pulp is the prime factor
for absorption of radiation wavelength from sun rays
(Nowak and Lewicki, 2004). Temperature can be
expressed as the average energy of molecular motion
according to the kinetic theory. Water molecules having
kinetic energy more than the escape energy and by
overcoming the cohesive force that binds the water
molecules in mango pulp will escape from the surface
of the pulp. The rate of evaporation is much lower as
it takes time for heat to migrate into the pulp from the
surrounding air.
The mango pulp mixture has been poured on
aluminium tray smeared with oil and exposed to open
air. Sun rays are directly incident on the pulp and
evaporate the moisture present within it. Due to the
reflection of the Sun rays on the shiny metal surface
the drying temperature rise up and ultimately a leathery
product can be obtained (Rameshwar, 1979).
Mango Leather Production: A Review
Hot-air Drying
It is the conventional drying method where heat is
transferred from the heated air to the pulp through the
mechanism of conduction of heat. After the absorption
of heat by the pulp the moisture diffuses from the pulp
surface to the hot air as well as the moisture diffuses
from the interior of pulp to the surface of the pulp. Both
the diffusion processes continue simultaneously until the
moisture content of pulp drops to a degree to achieve
the drying purpose. The temperature difference is the
driving force for the heat transfer while the driving
force of mass transfer is the concentration difference
of partial vapour pressure.
Mir and Nath (1995) produced mango leather in a
cross-flow cabinet dryer at 63 ± 2°C for time 14-16
hours, where the tray load was 9.8 kg/m2 to get final
moisture content of 22.9, 20.5 and 19.5% for plain
mango bar, mango-desiccated coconut powder (DCP)
bar and mango-soy protein concentrate (SPC) bar
respectively. The values of R2 for the BET model are
0.9067 and 0.4898 for plain mango bar and mangoDCP respectively. In comparison to the Henderson
model (R2 values 0.8370-0.9800) and GAB model (R2
values 0.8005-0.9325) for all the three types of mango
bars it has been found that the Oswin model (R2 values
0.9201-0.9731) and Smith model (R2 values 0.93780.9493) were better. Therefore Oswin model is pertinent
to drying all of the three types of mango bar whereas
the GAB model fits to predict the sorption behaviour
of plain mango bar only (Mohamad and Nath, 1995).
Hot air oven has been used by Gujral et al. (2013)
at 103±2°C for 24 h to dry the mango pulp. The
incorporation of sucrose and maltodextrin increases
the drying as more water is bounded with increase of
total soluble solid, whereas due to high water binding
property drying time increases in case of pectin addition.
Page’s model describes the drying characteristics as
well as the rate constant effectively with shape factor
within the range of 0.799–0.996. The R2 value has been
found 0.86. The effective moisture diffusivity calculated
by Fick’s second law of diffusion has been found in
the range of 1.65 to 4.03 × 10−7 m2/sec. In regression
analysis from the p-values it has been revealed that
sucrose followed by pectin and maltodextrin affect
the effective moisture diffusivity significantly (Gujral,
2013).
Cabinet dryer at temperature 60 ± 1°C and relative
humidity of 15% has been used by Gujral and Brar
(2003) to produce mango leather. The drying rate
constant and shape factor have been investigated by
them by using diffusion mechanism. The R2 values
83
lies in the range of 0.90-0.99. From the investigation
it has been established that during early two hours of
drying the rate of dehydration of mango leather is rapid;
thereafter a significant drop in drying rate is observed.
The incorporation of hydrocolloid significantly
decreases the rate of drying for initial two hours whereas
it has been found to have an insignificant effect on rate
of dehydration for later period of drying.
Gujral and Khanna (2002) produced mango leather
using hot air at a temperature of 60 ± 1°C and air
velocity of 3.5 m/s in a cabinet dryer. From regression
analysis, it has been found that increasing levels of
sucrose lowered the drying time whereas drying time
increases with increasing levels of skim milk powder
and soy protein concentrate in mango pulp, because of
water binding capacity of the protein molecules present
in the skim milk powder and soy protein concentrate.
Azeredo et al. (2006) prepared mango leather using
hot air oven to derive minimum drying time required to
attain leather with moisture content of 15-18%. Drying
temperature (60–80°C) and puree load (0.4–0.6 g/cm2)
have been selected as two independent variables to
conduct drying in accordance with central composite
design. Both the factors significantly affect the drying
time. The minimum drying time to produce mango
leather has been found 120 min at 80°C and with a
puree load of 0.5 g/cm2.
Prasad et al. (2002) studied the dehydration kinetics
of mango leather which is dried at 70 ± 1°C for 26 hours
with tray load 12.5 kg/m2 in cross flow cabinet dryer.
During the first eight hours of drying rate of dehydration
was higher. The incorporation of roasted Bengal gram
(RBF) in mango pulp slowed down the dehydration
rate. Thereafter, less moisture loss was observed till
20 hours of drying time for both plain mango pulp and
fortified mango pulp. Though after 14 hours and 16
hours of drying, the change in moisture content has been
found insignificant for plain and fortified mango pulp
respectively. Researchers found shape factors are 1.017
and 0.997 whereas drying constant (k) 0.318 and 0.255
for plain mango and mango-RBF leather respectively.
Parekha et al. (2014) conducted the quality evaluation
of mango bar fortified with desiccated coconut powder
using tray drier at 63 ± 2°C for 8-10 hours.
Microwave Drying
Microwave heating is one of the direct heating methods.
Microwaves are basically a form of electromagnetic
energy (300 MHz–300 GHz) which is generated by
magnetrons due to the mutual force of electric and
magnetic fields at right angle. The most common
84
Tanmay Sarkar and Runu Chakraborty
frequency used for drying of food material is 2450
MHz. When an oscillating electric field is incident on
the polar molecules present in mango pulp (water), the
permanently polarized dipolar molecules orient and
reorient themselves according to the direction of the
field at 2450 MHz, the orientation of the field changes
2450 million times per second. This consequences
oscillatory migration of ions in the food and generates
heat.
Pushpa et al. (2006) has produced mango leather
through microwave drier of 750 W and 2450 MHz
at power levels of 4, 8, 12, 16 and 20 W/g using 50
g of pulp with a power cycle of 30 s on and 30 s off
respectively to achieve moisture content of 12-15%.
Due to lower heat generation at lower power levels of
microwave oven, the rate of drying is slow so the time
required to dry the mango pulp is longer. They have
found that increasing soy flour level from 15 to 25%
is insignificant in variation of drying rates.
Infra-red Drying (IR Drying)
In IR drying without heating, radiation energy of the
adjacent air is transferred from the heating element to
the pulp surface. The radiation energy first impinges on
the top-most surface of pulp, penetrates it and finally
increases the sensible heat (Ginzburg, 1969). As thermal
degradation of heat-labile phytochemical occurs at
high temperature, the drying temperature should not
be too high (Rieger and Šesták, 1993). During drying,
as the moisture content decreases the transitivity and
reflectivity increases while the absorptivity of the dried
material decreases. The absorptivity, the skin depth
and the transitivity are the functions of the density,
wavelength of IR heating and properties of mango
pulp. IR drying is preferred over hot air drying due to
short drying time, high heat transfer coefficients and
simple material temperature control system (Nowak and
Lewicki, 2004). Because of these advantages IR drying
in combination with convection or vacuum is more in
practice in recent era (Mujumdar, 1995).
Effah-Manu et al. (2013) produced mango-sweet
potato leather with 15.4% moisture content, through
drying using flameless gas infrared catalytic heater at
45°C, 50°C and 55°C temperature. It has been found
that the cabinet, oven and solar dried jackfruit leather
had moisture contents of 18.85%, 14.79% and 18.5%
respectively (Okilya et al., 2010). From these results
of moisture content they concluded that in comparison
with cabinet, oven and solar dryer infra-red dryer is
more effective in producing mango leather.
Vacuum Drying
A vacuum dryer is an indirect type of heat dryer, that is,
pulp is in contact with heated surface of dryer. Therefore
drying is carried out by conduction mode. In this process
materials are dried in a low pressure environment
than normal atmospheric pressure and this results in a
reduced temperature heating. Heated steam or hot water
through hollow shelves is used as the heating medium.
For the major part of the drying cycle, temperatures can
be controlled with complete command and the mango
pulp remains at the boiling point of water.
Jaya and Das (2003) have considered vacuum drying
model for mango pulp. The ingredients (maltodextrin,
glycerol monostearate, and tri calcium phosphate at an
amount of 0.62, 0.015 and 0.015 kg/kg dry mango solid
respectively) have been mixed with mango pulp. In the
process of mixing a planetary mixer having its mixing
arm operated at 75 m/min peripheral speed for 15 to 20
min has been used; thereafter the pulp has been spread
on aluminum trays coated with teflon. This mixture has
been spread to 2, 3 and 4 mm thickness and dried at
temperatures 65, 70 and 75°C in a vacuum drier. The
absolute pressure has been maintained in the vacuum
dryer at 30–50 mmHg. They have found that the product
was leathery but non-sticky. They have also found that
during first 900 and 1000 s of drying, the reduction in
moisture content is high. Mango pulp with thickness
0.004 m dried at 65°C shows maximum drying time
of 10800 seconds and the pulp with thickness 0.002
m dried at 75°C shows minimum drying time of 3500
seconds. The value of R2 for actual and predicted
moisture content using predicted effective diffusivity
lies in the range of 0.991 to 0.997.
Researchers consider different models to predict the
product aspects which are listed in Table 1.
Energy Consumption Performance in
Different Drying Techniques
Drying is the process for producing mango leather
which is also the most energy intensive process in food
preservation (Brooker et al., 1992). Comparative view
of different drying methods employed during mango
leather processing by researchers is shown in Table 2.
The model for determining energy requirement during
different drying techniques involved in mango leather
production is as follows.
Energy Consumption of Hot Air Dryer
At different temperatures and air flow rates within the
hot air oven the energy consumption is calculated by
Mango Leather Production: A Review
85
Table 1: Mathematical models used by researchers
Method
Model
Generalised Maxwell model
Equation
Peleg model
Ê k1 k2 ˆ
σ(t) = s e + s 0 Á
Ë k1 + k2 .t ˜¯
Florina Danalache (2015)
Mir and Nath (1995)
È
˘
Ê t ˆ
Ê t ˆ
+ ºº + Ee ˙
σ(t) = e 0 Í E1 exp Á - ˜ + E2 exp Á ˜
Ë l1 ¯
Ë l2 ¯
ÍÎ
˙˚
BET
m=
m0, B CB aw
(1 - aw ) (1 - aw + awCB )
GAB
m=
Handerson
Oswin
Smith
K. Prasad (2002)
Diffusion mechanism
Azeredo et al. (2006)
Central composite design
CG KG m0,G aw
(1 - KG aw ) (1 - K G a w + CG K G aw )
(1- aw ) = e - K H m
nH
Ê aw ˆ
m = C0 Á
Ë 1 - aw ˜¯
n0
m = A – B ln (1 – aw)
MR =
M - Me
= A exp ( - kt )
M0 - Me
Y = b0 +
Â
3
b X
n =1 n n
Â
Gujral and Khanna (2002) Central composite design
Y = b0 +
Â
3
n =1
Diffusion mechanism
Gujral et al. (2013)
Central composite design
MR =
Parekh et al. (2014)
3
b X2
n = 1 nm n
+
b X X
n < m nm n m
Â
3
b X2
n = 1 nm n
+
3
b X X
n < m nm n m
M - Me
= A exp ( - kt )
M0 - Me
Y = b0 +
Â
3
b X
n =1 n n
Â
G. Pushpa et al. (2006)
Â
3
bn X n +
Â
Gujral and Brar (2003)
+
+
Â
3
b X2
n = 1 nm n
+
3
b X X
n < m nm n m
Factorial randomized block design Yi,j = µ + Ti + Bj + random error
Completely randomized design Yi,j = µ + Ti + random error
with factorial concept
BET = Brunauer-Emmett-Teller; GAB = Guggenheim-Anderson-deBoer; CB, CG, CO = Constants of BET, GAB and Oswin
model respectively; KG, KH, KO = Constants in GAB, Henderson and Oswin models, respectively; m = Moisture content;
mO,B , mO,G = Monolayer water content calculated by BET and GAB models respectively; nH, nO = Constants in Henderson
and Oswin models, respectively; aw = Water activity; Y = Dependent variable; b0= Fixed response at the central point of
the experiment; bn, bm, and bnm= Linear, quadratic, and cross product coefficients respectively; Yi,j = Dependent variable for
which X1 = i and X2 = j; X1 = Primary factor; X2 = Blocking factor; M = General location parameter; Ti = Effect for being
in treatment i; Bj = Effect for being in block j; MR = Moisture ratio; MO = Initial moisture content; Me = Final moisture
content; k = Drying constant; A = Shape factor; σ(t) = Stress over time t; ε0 = Initial strain; E1, E2 … = Elastic moduli; Ee =
Equilibrium elastic moduli; λ1, λ2 = Relaxation time; t = compression holding time; σe= Residual stress; σ0 = Initial relaxation
stress; and k1, k2 = Constant.
Tanmay Sarkar and Runu Chakraborty
86
Table 2: Comparison of different drying methods used in mango leather processing
Methods of drying
Sun drying
Key features
Energy extensive and most economical.
Climate dependent and time consuming.
Reference
Rameshwar (1979)
Hot-air drying
Process parameter like drying temperature and air flow rate can
be controlled.
Very low residual moisture level cannot be achieved.
A possibility of thermal damage is there for material with high
initial moisture content.
Microwave drying
Mir and Nath (1995)
Gujral et al (2013)
Gujral and khanna (2002)
Azeredo et al (2006)
Prasad et al (2002)
Parekha et al (2014)
Puspa et al (2006)
Fastest drying process and high energy density.
Rapid heat transfer along with inadequate homogeneity.
A possibility of dark spot generation and plasma expulsion.
Process parameters can easily be controlled. Uniform temperature Effah-Manu L (2013)
distribution can be achieved.
Depending on food commodity the wavelength of radiation is
selected.
In case of thin layer drying Far Infra-red radiation (3-1000 µm) is
better whereas Near Infra-red radiation (0.78-1.4 µm) is efficient
in drying of thick layers.
Infra-red drying (IR drying)
Vacuum drying
Comparatively less energy consuming process and environment Jaya and Das (2003)
friendly process.
Ideal for hygroscopic and heat sensitive material
using Eq. (1) (Motevali et al., 2011; Aghbashlo et al.,
2008; Koyuncu et al., 2007):
EtH = A × v × ρa × ∆T × t
(1)
where EtH is total energy consumed in each cycle of
drying (kWh), A = container area (m2), v = air flow
rate (m/s), ρa = density of air (kg/m3), t = time required
for drying, ∆T = temperature difference (°C) and Ca =
specific heat of air (kJ/kg °C).
As the specific heat of dry air is constant and it is
1.004 so Ca can be calculated from the Eq. (2) [63]
Ca = 1.004 + 1.88 w
(2)
where w is relative humidity and can be determined
from Eq. (3) (Aghabashlo et al., 2009)
w = 0.622 ¥
Pvs
P - Pvs
(3)
where P = air pressure (k Pa), P vs = saturated
vapour pressure (k Pa) and can be calculated from
psychrometric chart.
Energy Consumption by Infra-red Dryer
The total energy consumption of infrared dryer (EtI) is
the sum of cumulative energy intake by the infra-red
lamp (E1) and the centrifugal blower (E2) (Motevali et
al., 2011; Sirvastava et al., 1993).
E1 = K × t
(4)
where K = power of IR lamp and t = time required for
drying.
V3
16600
where V = velocity of air (m/s).
Therefore,
E2 =
(5)
EtI = E1 + E2
(6)
Energy Consumption in Microwave Dryer
The energy consumption in microwave dryer (EtM) can
be determined by using Eq. (7) (Ozkan et al., 2007)
EtM = G × t
(7)
in which, G = output power of microwave (kW) and t
= time required in drying.
Energy Consumption in Vacuum Dryer
The energy consumption of vacuum pump (E1) is
determined by using Eq. (8) (Ali et al., 2011).
Mango Leather Production: A Review
E1 = L × t
(8)
where L = power of pump (kW) and t = drying time.
Energy consumption of heaters (E2) can be calculated
by using Eq. (9).
E2 = Q × I cos θ × t
(9)
where Q = voltage (V), I = electrical current (amp),
t = time required to drying, θ = phase angle between
current and voltage sine wave. Therefore, the total
energy consumption in vacuum drying (EtV) is derived
from Eq. (10):
EtV = E1 + E2
(10)
Physicochemical Analysis
A series of physicochemical analysis has been done by
researchers to determine the effect of formulation and
processing technology on quality of mango leather.
The compositional view of mango leather found by
researchers is listed in Table 3.
Equilibrium Relative Humidity (ERH) and Water
Activity (aw)
Five grams of accurately weighed mango bars are
taken in pre-weighed, dried petri dishes and placed
at desiccators, maintained at room temperature (25 ±
2 °C) (Prasad et al., 2002). The samples have been
allowed to equilibrate to constant weights; thereafter
the moisture content of samples at different relative
humidity has been measured by vacuum oven method
(Ranganna, 1986). aw has been determined by using
following equation:
aw =
ERH
100
Proximate Analysis
Researchers have analysed the moisture content, crude
protein, fat, crude fibre, carbohydrate and ash content
of mango leather according to AOAC methods (EffahManu, 2013; AOAC, 1990). The acidity, reducing and
total sugars of samples have been analysed by Lane and
Eynon method (Effah-Manu, 2013; Ranganna, 1986).
Determination of Total Soluble Solids (°Brix)
Effah-Manu et al. (2013) have determined the
total soluble solids using the analogue hand-held
refractometer. To calibrate the instrument distilled
water and test solution of known sucrose concentration
have been used. All the readings have been taken in
duplicates and averaged before analysis of results.
87
Determination of Vitamin C (Total Ascorbic Acid)
Content
Effah-Manu et al. (2013) have used the following
procedure to determine the vitamin C in mango
leather. 10 ml of sample extract was poured in a
100 ml volumetric flask and the volume made up
by 0.4% oxalic acid solution. After filtration of this
solution through Whatman No. 4 filter paper, 10 ml
of the filtrate has been pipetted into a conical flask
and 15 ml of 0.4% oxalic acid solution added to it.
The solution has been titrated against 0.04% aqueous
sodium dichlorophenolindophenol solution; end point
has been detected on appearance of first pink shade.
0.01 N sodium thiosulfate along with potassium iodide
(50%) and 1 N HCl has been used to standardize sodium
dichlorophenolindophenol solution using starch as
indicator. The amount of total ascorbic acid has been
determined through the following equation (Sharma et
al., 2016):
ˆ 0.5 mg
Ê
V
mg
=
¥ 2
Ascorbic Acid Á
˜
V1
15 ml
Ë 100 g sample ¯
¥
100 ml
¥ 100
weight of sample
Total Carotenes
Prasad (2009) underwent through the following method
to estimate total carotenes in mango leather. 100 mg
of leather has been added with 10 ml of 80% acetone
and grinded well in mortar-pestle. After centrifugation
of the mixture at 3000 rpm for 10 min the supernatant
has been taken and the volume is made up to 10 ml.
The optical density values have been studied at 480 nm
in ultra violet spectra. The following equation has been
used to calculate the amount of carotenoids in mango
leather (Harbone, 1973).
Amount of carotenoids in 100 mg leather
4 × optical density × total volume of sample (10 ml)
=
wright of leaather (100 mg)
Texture Analysis
Florina Danalache et al. (2014) have carried out texture
analysis of mango bar in order to mimic the human
biting action. They employ method used by texture
analyser equipped with 50N load cess (Mandala et al.,
2007). By using an aluminium plunger with 60 mm
diameter a double compression cycle test has been
performed, with a time gap of 5 s between the two
compression cycles. To avoid friction a thin layer of
paraffin oil has been applied between plates and the
testing sample in order to avoid friction. Hardness has
88
Table 3: Mango leather composition
TSS
(°B)
Moisture ERH
(%)
(%)
15.0 ± 1.60
Crude
protein (%)
2.25 ± 0.92
Crude fat Crude fibre
Ash (%)
Carbohydrate
(%)
(%)
(%)
0.55 ± 0.03 2.82 ± 0.04 2.06 ± 0.25 77.32 ± 0.62
65.57
15.21
2.0
2.0
Vitamin C
(mg/100 g)
17.49 ± 2.11
Carotene
(mg/100 g)
Effah-Manu
et al. (2013)
25.93
65.94
17.2
0.621
10.0
10.0
75-80
45.16
10.0-15.0
0.667-0.529
13.2
22.9
11.17 –
17.94
2.0
69
0.3
2.0
82.5
12.2
61.40-7150
0.46 – 0.72
Reference
Parekha et al.
(2014)
Prasad et al.
(2002)
Azeredo et
al. (2006)
Gujral et al.
(2002)
Gujral and
Brar (2003)
Pushpa et al.
(2006)
Prasad
(2009)
Mir and Nath
(1995)
Dina et al.
(2015)
Tanmay Sarkar and Runu Chakraborty
81.24
Water
activity
0.61 ± 3.8a
Mango Leather Production: A Review
been measured as the maximum force during the first
compression cycle. Springiness is the ratio of the second
and first compression distances. Cohesiveness has been
defined as the ratio of the positive force area during the
second and first cycle of compression.
Colour Measurement
The mango leather has been positioned underneath the
optical sensor of Hunter Lab Calorimeter; the readings
for mean value of L, a and b were considered from three
measurements performed on each sample in terms of
defining the colour of samples. Before initialization of
experiment the colorimeter has been standardized by
using standard white and black tiles (Effah-Manu et al.,
2013; Pushpa et al., 2006). Table 4 represents the L, a
and b values studied by researchers.
Sensory Analysis
Most of the researchers employ nine-point Hedonic
scale to evaluate mango leather samples for flavour,
colour and texture where the sensory panel consisted of
20 trained members. (Prasad et al., 2002; Effah-Manu
et al., 2013; Azeredo et al., 2006; Gujral et al., 2013;
Pushpa et al., 2006; Prasad, 2009; Dina et al., 2015).
A preference–ranking test (ISO 8587:2006) has been
performed by Florina Danalache et al. (2014). As texture
is the determining factor in developing food products
like bars, they have been considered only one sensory
parameter that is the overall texture and each panellist
had been requested to assess that particular attribute of
samples by preference. According to ISO 8587:2006
the sensory evaluation of mango bars has been carried
out in a sensory room with six analysis boxes. The 63
panellists aged between 20-65 years old and regular
consumers of mango fruit have been chosen. The
five different mango bars have been presented to the
panellists in random order and labelled with randomly
generated code of three digits at room temperature
(20-22°C). The panellists rank the five samples in
order of their preference: (1) the least, (2) slightly,
(3) moderately, (4) neither like nor dislike and (5) the
89
most preferred texture (Meilgaard et al., 1999). The
panellists have been asked to validate their choices and
the justifications have been used to determine whether
each sample was significantly preferred over the others.
Packaging and Storage
As mango leather is a ready to eat food so food
containment can be achieved best by food packaging.
This is the best way to control and protect the food
against physical, chemical, biological and environmental
deterioration. Therefore packaging and storage of
mango leather is one of the prime factors with respect
to food safety as well as for marketing.
Rectangular pieces of mango bars have been packed
in polyethylene bags and stored at room temperature for
six months. The chemical and organoleptic assessment
of mango bars during the storage period of 0, 1, 2, 3,
4, 5 and 6 months show progressively decline of taste
score with storage period (Parekha et al., 2014). Up to
six months of time mango leathers are consumable. The
similar kind of result is also found by other researchers
(Narayana et al., 2003).
In some case Al foil rolled mango leather is packed in
cellophane film (Effah-Manu et al., 2013). In some other
cases polyethylene pouch as packaging material and at
room temperature storage is used (Gujral and Khanna,
2002; Gujral et al., 2013; Gujral and Brar, 2003). The
use of poly propylene (PP) pouches as packaging
material and refrigerated storage at 11±1°C temperature
is also found in some studies (Prasad, 2009).
The microbiological safety of mango leather
on storage at 25°C for six months packaged in
polypropylene buckets with lids has been studied by
Azeredo et al. (2006). It has been found that mesophyllic
aerobes remained less than 10 colony forming unit
(CFU)/g, yeasts and mould count is less than 100 CFU/g
throughout the storage period of six months. It has been
concluded that the product is microbiologically safe
for the storage period considered as there is no proof
of presence of Salmonella and most probable numbers
Table 4: Colour values for mango leather
Cultivar
Keitt
Tommy Atkins
Safaida
Langra
Alphanso
L
59.01 ± 0.56
52.97
44.499
35.08
52.487
a
14.08 ± 0.10
8.12
10.104
12.33
9.849
b
47.77 ± 0.35
42.18
29.493
22.74
20.947
Reference
Effah-Manu et al. (2013)
Azeredo et al. (2006)
Gujral and Khanna (2002)
Gujral and Brar (2003)
Pushpa et al. (2006)
Tanmay Sarkar and Runu Chakraborty
90
(MPN) of all coliforms (including E. coli) have been
found to be lower than three organisms/gram.
Polyethylene pouch, wax paper and aluminium
foil have also been used for packaging of mango bar
purchased from market for two months of storage.
During storage heavy load of Enterobacters and some
other bacteria indicating spoilage have been found
(Singh et al., 2003).
Conclusion
The “King of fruit” mango is not only superior with
respect to sensory attributes but also has medicinal
activity. But as it has high moisture content it is
perishable in nature. Thus processing and preservation is
required. Among the processed mango products mango
leather is relished most. Texture and other sensory
qualities of mango leather can vary with different
formulations used and different drying techniques
employed. These changes of qualities can be determined
by a series of physicochemical analysis. The drying
techniques used for mango leather preparation include
sun drying, hot air drying, microwave drying, IR drying
and vacuum drying. The total energy consumption of
these dryers is investigated by researchers. There is
lack of research in the field of process optimisation for
mango leather production to get superior textural and
nutritional quality. A vivid research is required in the
area of packaging and storage of mango leather.
Acknowledgements
The authors wish to acknowledge UGC for financial
assistance, and members of Department of Food
Technology and Biochemical Engineering, Jadavpur
University for their support.
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