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Solid phase extraction of trans-resveratrol from wines for HPLC analysis

Z Lebensm Unters Forsch. 1993 Jun;196(6):522-5. doi: 10.1007/BF01201331.

Abstract

Some recent studies have put forward the hypothesis that the presence of trans-resveratrol (trans-3,5,4'-trihydroxystilbene) in red wine may be related to some of its therapeutic properties. A fundamental step in view of this evaluation is the development of a method for the quick, accurate and precise analysis of this compound. Sample enrichment and purification can be obtained by solid-phase extraction using reverse-phase C18 cartridges. HPLC analysis carried out by means of a photodiode-array detector, with an internal standard method, allows the detection of up to 10 micrograms/L in wine, with a linear range between 0.6 and 300 ng injected and a precision of 3.3%. The results of the first analyses show that the concentrations of trans-resveratrol in wines might be much higher than so far reported in the literature.

MeSH terms

  • Cardiovascular Diseases / prevention & control*
  • Chromatography, High Pressure Liquid
  • Humans
  • Italy
  • Resveratrol
  • Spectrophotometry, Ultraviolet
  • Stilbenes / analysis
  • Stilbenes / isolation & purification*
  • Wine / analysis*

Substances

  • Stilbenes
  • Resveratrol