Designation: D 3302 02a

Standard Test Method for

Total Moisture in Coal
1
This standard is issued under the xed designation D 3302; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the measurement of the total
moisture in coal as it exists at the site, at the time, and under
the conditions it is sampled. It is applicable to coals as mined,
processed, shipped, or used in normal commercial pursuits. It
is not applicable to coal-water slurries, sludges, or pulverized
products under 0.5-mm-diameter sieve size. It is applicable to
coals of all ranks within the recognized limitations imposed by
oxidation and decomposition characteristics of lower rank
coals. Because of its empirical nature, strict adherence to basic
principles and permissive procedures are required for valid
results (see Appendix X1). This complete standard is available
to producers, sellers, and consumers as a total moisture method
when other procedures or modications are not mutually
agreed on.
1.2 Since coal can vary from extremely wet (water-
saturated) to completely dry, special emphasis must be placed
on the sampling, sample preparation, and the moisture deter-
mination itself to ensure total reliability of measurement.
Therefore, this standard entails collection of the gross sample,
sample preparation, and the method of determination.
1.3 While it is recognized that such a standard may be
unwieldy for routine usage in commercial operations, it can
provide a common base for agreement in cases of dispute or
arbitration. The complete standard is referred to as the referee
method. Embodied in the standard is the commercial method
starting with the crushed and divided sample when the gross
sample is not too wet to crush and divide. See Test Methods
D 2961 and D 3173 for other moisture methods.
1.4 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
only.
1.5 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 121 Terminology of Coal and Coke
2
D 2013 Practice for Preparing Coal Samples for Analysis
2
D 2234 Practice for Collection of a Gross Sample of Coal
2
D 2961 Test Method for Single-Stage Total Moisture Less
than 15% in Coal Reduced to 2.36-mm (No. 8 Sieve)
Topsize
2
D 3173 Test Method for Moisture in the Analysis Sample of
Coal and Coke
2
D 5865 Test Method for Gross Caloric Value of Coal and
Coke
2
3. Terminology
3.1 DenitionsFor additional denitions of terms used in
this test method, refer to Terminology D 121.
3.2 Denitions of Terms Specic to This Standard:
3.2.1 air dryinga process of partial drying of a coal
sample to bring it to near equilibrium with the atmosphere in
the room in which further reduction/division of the sample is to
take place.
3.2.2 air-dry lossthe loss in weight, expressed as a
percent, resulting from each air-drying operation.
3.2.3 easily oxidized coalslow-rank coals such as subbi-
tuminous or lignitic coals.
3.2.4 equilibriumcondition reached in air drying when the
change in weight of the sample, under conditions of ambient
temperature and humidity, is no more than 0.1 %/h or 0.05 %/
1
2 h.
3.2.5 residual moisturethat moisture remaining in the
sample after air drying.
3.2.6 total moisturesee Terminology D 121.
4. Summary of Test Method (See Fig. 1)
4.1 This test method is based on the loss in weight of a coal
sample in an air atmosphere under rigidly controlled conditions
of temperature, time, and airow.
4.2 Alternative Methods:
4.2.1 Referee Method, which may be used in cases of
dispute or arbitration. The gross moisture sample is air dried to
1
This test method is under the jurisdiction of ASTM Committee D5 on Coal and
Coke and is the direct responsibility of Subcommittee D05.21 on Methods of
Analysis.
Current edition approved April 10, 2002. Published July 2002. Originally
published as D330274. Last previous edition D330200a
e1
.
2
Annual Book of ASTM Standards, Vol 05.06.
1
Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
equilibrate it with the atmosphere at each stage of division and
reduction. No air drying is necessary if the sample is already at
equilibrium with the atmosphere as indicated by stable weight.
4.2.2 Commercial Method, which may be used in routine
commercial practice or when the concerned parties agree upon
this method. The crushed and divided moisture sample is air
dried to equilibrate it with the atmosphere in which further
division and reduction are to occur.
4.2.3 Residual moisture determination is made in a heated
forced-air circulation oven under rigidly dened conditions.
4.3 Total moisture is calculated from loss (or gains) in air
drying and the residual moisture.
5. Signicance and Use
5.1 The collection and treatment of the sample as specied
for the referee method is intended for the express purpose of
determining the total moisture in coal. The standard is avail-
able to producers, sellers, and consumers as a method of
determination when other techniques or modications are not
mutually agreed upon.
5.2 The commercial method, which determines total mois-
ture content of the crushed and divided sample, is designated as
the method for total moisture for routine commercial practice.
6. Apparatus
6.1 Drying FloorAsmooth clean oor area in a room free
of contamination by dust or other material and that permits air
circulation without excessive heat or air currents. Conditions
for an air-drying oor should approach those established for
oven drying as much as possible.
6.2 Air-Drying OvenA device for passing slightly heated
air over the sample. The oven should be capable of maintaining
FIG. 1 Total Moisture Determination on Gross Sample, Special Moisture Subsample, or on Crushed and Divided Sample
D 3302 02a
2
a temperature of 10 to 15C (18 to 27F) above ambient
temperature with a maximum oven temperature of 40C
(104F) unless ambient temperature is above 40C (104F), in
which case ambient temperature shall be used. In the case of
easily oxidized coals, the temperature should not be more than
10C (18F) above ambient temperature. Air changes should be
at the rate of one to four per minute. A typical oven is shown
in Fig. 2.
6.3 Drying Pans:
6.3.1 Pans for Gross Sample, noncorroding, weight-stable
at temperature used, of sufficient size so that the sample can be
spread to a depth of not more than twice the diameter of the
largest particles if larger than 13 mm (0.5 in.) or not more than
25-mm (1.0-in.) depth for smaller coal, with pan sides about 50
to 75 mm (2 to 3 in.) high.
6.3.2 Pans for Crushed and Divided Sample, noncorroding,
weight-stable at temperature used, of sufficient size so that the
sample can be spread to a depth of not more than 25 mm (1.0
in.) with sides not more than 38 mm (1.5 in.) high.
6.4 Scale (Gross Sample)a scale of at least 45-kg (100-
lbs) capacity and sensitive to 23 g (0.05 lbs) in 45 kg (100 lbs).
6.5 Balance (Crushed Sample), sensitive to 0.1 g with a
capacity sufficient to weigh pan, sample, and container.
6.6 Laboratory Sample Containersheavy vapor-
impervious bags, properly sealed, or noncorroding cans such as
those with an airtight, friction top or screw top sealed with a
rubber gasket and pressure-sensitive tape for use in storage and
transport of the laboratory sample. Glass containers, sealed
with rubber gaskets, can be used, but care must be taken to
avoid breakage in transport.
6.7 Drying Oven (for residual moisture on 250-m (No. 60)
sieve by 0 sample)This oven is described in Test Method
D 3173 and can be of the form illustrated in Fig. 2 in Test
Method D 3173.
6.8 Analytical Balance, sensitive to 0.1 mg (for residual
moisture on 250-m (No. 60) by 0 sample).
6.9 Capsules, with covers, described in Test Method
D 3173.
7. Precautions
7.1 In collecting, handling, reducing, and dividing the gross
moisture sample, all operations shall be done rapidly and in as
few operations as possible, since moisture loss depends on
several factors other than total moisture content, such as time
required for crushing, atmospheric temperature and humidity,
and type of crushing equipment.
7.2 While awaiting preparation, the uncrushed gross mois-
ture sample shall be sealed in appropriate containers in order
that it be protected from moisture change as a result of
exposure to ambient air, rain, snow, wind, and sun, or contact
with absorbent materials.
7.3 If the gross sample requires air drying, then the initial
weight of the original gross moisture sample and container
shall be recorded, and the moisture loss or gain of sample and
containers shall be determined before the sample is reduced.
7.4 Whenever a distinct change of humidity occurs during
the course of preparation of an air-dried sample, the subsample
should be weighed and equilibrated with the new atmosphere
and the weight loss or gain used in the calculation of total
moisture content.
7.5 Whenever subsamples are stored or transported and
moisture condenses on the container, then the container and
subsample shall be weighed, equilibrated to the new atmo-
sphere by air drying, and the weight loss or gain shall be used
in the calculation of total moisture content.
7.6 Since most coals have a tendency to oxidize on exposure
to air, the air-drying procedure should not be prolonged past
the time necessary to bring the sample to equilibrium with the
temperature and humidity of the air in the room in which
further reduction and division are to be made. Easily oxidized
coals must not be air dried at a temperature exceeding 10C
above ambient temperature. In no case shall the air drying be
done at a temperature over 40C. Air drying of low-rank coals
should not exceed 18 h because of oxidation. In the case of
lignite, the goal of reaching equilibrium should be weighed
against the possibility of oxidation.
7.7 Protect crushed, divided, pulverized, or pulverizing
samples from atmospheric changes affecting surface moisture
or otherwise affecting sample integrity.
7.7.1 Procedures useful in maintaining uniform temperature
and humidity conditions and minimum airow in moisture FIG. 2 Air-Drying Oven
D 3302 02a
3
determination and sample preparation area include the follow-
ing: (1) closed dust control system, recycling ltered air; (2)
hood over dust-producing equipment to minimize airow
required to remove dust; and (3) pulling makeup air from
within the building to replace exhausted air or using tempered
or conditioned makeup air.
7.7.2 Avoid heatup of pulverizer by: (1) using pulverizer
large enough to process sample quickly and (2) allowing time
for pulverizer to come to room temperature before reuse.
8. Sampling
8.1 The principles, terms, organization, and collection as set
forth in Practice D 2234 shall apply to the collection of the
total moisture sample. Particular attention is directed to Section
8. The increments as established in Table 2 of Practice D 2234
for mechanically cleaned coal are deemed adequate for general
purpose sampling for total moisture.
9. Procedure
9.1 Air-Drying Loss on Gross SampleReferee Method:
9.1.1 Procedure A, Drying FloorThis procedure is par-
ticularly applicable if the gross moisture sample is too large an
amount to ship reasonably or is too wet to handle or ship
without loss of moisture.
9.1.1.1 Weigh and record the weight of the gross moisture
sample. Spread the sample on the drying oor to a depth of not
more than twice the top size of the coal. Mix or stir the coal
from time to time, being careful not to lose any of the coal
particles. Continue the air drying and mixing until the surface
of the sample appears dry. Weigh the entire sample and
redistribute over the oor for additional drying. Continue the
drying and stirring, weighing at 1- to 2-h intervals until the
weight loss of the total sample becomes no more than 0.1 %/h
(Note 1). Record the weight of the air dry sample. Avoid excess
drying.
NOTE 1If the sample surface appears dry, and the time required for
reduction and division is well established, air drying can be stopped when
the weight loss is less than 0.1 % per twice the required time for
processing. Example: If reduction and division of the sample is expected
to require 20 min, the air-drying procedure can be stopped when the rate
of moisture loss is less than 0.1 %/40 min. If this procedure is used, a
second air drying is required to establish the 0.1 %/h rate before the nal
preparation of the laboratory sample.
9.1.1.2 Proceed with sample reduction and division in
accordance with Method D 2013, Section 9.3.3 or 9.3.4,
observing precautions of Method D 2013, Section 7. Use
enclosed equipment where possible to minimize moisture
change.
9.1.2 Procedure B, Air Drying Oven:
9.1.2.1 Distribute the gross moisture sample over the re-
quired number of tared pans. Weigh each pan with sample as it
is lled from the gross sample. Place in an air-drying oven that
has been adjusted to maintain temperature no more than 10C
(18F) above ambient temperature for easily oxidized coals or
no more than 15C (27F) above ambient temperature for other
coals (oven temperature not to exceed 40C). Ambient air may
be used with no heating. Maintain air circulation through the
oven at a rate of at least one air exchange per minute, but in no
case should it be sufficiently high to blow ne particles from
the pans. Gently stir the sample from time to time to ensure
uniform drying throughout the sample. Continue drying with
intermittent stirring until the coal surfaces appear to be dry.
Remove from oven, weigh, and record the weight. Return the
pans with sample to the oven and continue the operation.
Calculate the percent weight loss. Repeat the drying and
weighing process at 1- to 2-h intervals until the weight loss is
less than 0.1 %/h (Note 1). Allow the sample to reach equilib-
rium with ambient temperature and humidity before the nal
air dry weight is recorded. Avoid excess drying.
9.1.2.2 Proceed with sample reduction and division in
accordance with Method D 2013, Section 9.3.3 or 9.3.4,
observing precautions of Method D 2013, Section 7. Use
enclosed equipment where possible to minimize moisture
change.
9.2 Air-Drying Loss on Crushed and Divided Coal Sample,
Referee and Commercial Method:
9.2.1 Proceed with determination of air-drying losses (or
gains) without unnecessary delay under either of the following
conditions:
9.2.1.1 When the air-drying loss has been determined on the
gross sample and it has been crushed and divided in accordance
with 9.1.1.2 or 9.1.2.2.
9.2.1.2 When the gross sample is not too wet to crush and
has been crushed and divided to 4.75-mm (No. 4) or 2.36-mm
(No. 8) top sieve size.
9.2.2 The minimum weight of the crushed and divided
sample is specied in Method D 2013, Table 1. The sample
must remain in an airtight container with minimum unused
volume until testing is started. Preparation of top-sieve size
2.36-mm (No. 8) by 0 samples described in the following
method, but 4.75-mm (No. 4) by 0 or 850-m (No. 20) by 0
samples can be air dried by this method as stages in the
determination of total moisture, using appropriate quantities.
9.2.3 Weigh and record the tare weight of the air-drying pan
or pans. Quickly empty the sample from its airtight container
into the tared pan or pans and weigh with container (Note 2),
recording to the nearest 0.1 g. Spread the sample evenly to a
depth of no more than 25 mm (1.0 in.), preferably less for
shorter drying time. Place both the pan containing the sample
and emptied sample container in the air-drying oven that has
been adjusted to maintain temperature no more than 10C
(18F) above ambient temperature for easily oxidized coals or
no more than 15C (27F) above ambient temperature for other
coals. Ambient air can be used with no heating. Air changes in
the oven must be at the rate of one to four per minute. (The
sample may be stirred gently from time to time to promote
uniform and quicker drying.) Continue drying until the coal
surfaces appear to be dry. Remove the pan and container from
the oven and weigh together. Carefully transfer residual coal
from the dried sample container to the sample in the pan.
Weigh the empty container and subtract its weight from the
combined weight of pan, sample, and container recorded both
before and after the rst air-drying period. Calculate the
percent weight loss of the sample. Return the pan or pans with
sample to the oven and continue drying. Weigh at 1- to 2-h
intervals until the weight loss drops to a level near the 0.1 %/h
target (about 0.2 to 0.3 %/h). Complete the air drying at
D 3302 02a
4
ambient temperature, allowing the sample to reach equilibrium
(0.1 % loss per hour or 0.05 % loss per half hour) with both
ambient temperature and humidity before the nal air-dry
weight is recorded (Note 3). When this point is reached, record
the nal air-dry weight. Calculate the percent air-drying loss.
Strictly observe the cautions of Section 7.
NOTE 2If the moisture determination is to be made without delay in
the immediate vicinity of sample preparation, the sample need not be
placed in a container, but can be weighed directly in a tared drying pan.
NOTE 3This nal air-drying phase may be accomplished by leaving
the sample in the oven, cutting off the heat, but continuing the air
circulation at ambient temperature, or the sample may be removed from
the oven for the ambient temperature-drying phase. Required time is
reduced by using a heater timer adjusted to cut off the heat 2 h or more
before the sample is to be weighed nally, leaving the circulating fan
running. This makes overnight drying more practical and reliable. (The
time required after the drying at elevated temperature to bring the weight
loss rate to 0.1 %/h at ambient temperature may be as much as 1
1
2 to 3 h,
perhaps more.)
9.3 Residual Moisture on Prepared Sample:
9.3.1 The procedure for determining the residual moisture
on the air-dried sample is dependent on the top size to which
the air-dried sample is crushed or pulverized. Procedure A is
used on samples prepared to a top sieve size of 250 m (No.
60) U.S.A Standard. Procedure B is used on samples prepared
to a top sieve size of 850 m (No. 20) U.S.A Standard.
9.3.2 Procedure A, Top Sieve Size 250 m (No. 60) U.S.A
Standard:
9.3.2.1 Immediately after obtaining the nal air-dry weight
on the 2.36-mm (No. 8) sieve size sample, prepare the 250-m
(No. 60) sieve size sample in accordance with Method D 2013,
Sections 9.3.3.6 and 9.3.3.8, placing the sample in a tightly
sealed container.
9.3.2.2 The 250-m (No. 60) sieve size sample for residual
moisture determination shall have a minimum weight of 50 g.
9.3.2.3 Determine residual moisture on the 250-m (No. 60)
sieve size sample without prolonged delay after its preparation
to avoid unmeasured moisture change and oxidation, especially
for low-rank, easily oxidized coals.
NOTE 4Oxidation after sampling of susceptible low-rank coal or
lignite may result in a reduction of the caloric value. Unnecessary
exposure of the sample to air from the time of sampling or delay in
analysis shall be avoided.
9.3.2.4 Mix sample thoroughly with mixing wheel or oth-
erwise before extracting portions.
9.3.2.5 (This procedure, as well as an acceptable alternative,
may be found in Test Method D 3173.) Heat an empty capsule
under the conditions at which the sample is to be dried, place
the cover on the capsule, cool over a desiccant for 15 to 30 min,
and weigh. Dip out with a spoon or spatule from the sample
approximately 1 g of the sample. Put this quickly into the
capsule, close, and weigh at once to 60.1 mg. Place the
uncovered capsule in a preheated oven (107 6 3C) through
which passes a current of air that has been dried by a suitable
desiccant such as Drierite or magnesium perchlorate or other
efficient air-drying procedure. Close the oven at once and heat
for 1 h. Open the oven, remove and cover the capsule quickly,
cool in a desiccator over desiccant, and weigh as soon as
cooled to ambient temperature.
NOTE 5The residual moisture content in analytical samples can
change when the samples are exposed to an atmosphere in which the
relative humidity differs from that prevailing during sample preparation.
Consequently, for tests of certain properties (such as caloric value, see
Test Method D 5865, Section 12.3), in which a small error may have
signicant economic impact, it is advisable to measure residual moisutre
at the same time the economically signicant property is determined.
9.3.3 Procedure B, Top Sieve Size 850 m (No. 20) U.S.A
Standard:
9.3.3.1 Immediately after obtaining the nal air-dry weight
on the 2.36-mm (No. 8) sieve size sample, reduce the sample
to pass 95 % through an 850-m (No. 20) sieve using suitable
crushing equipment. Divide by riffling, using the small en-
closed riffle, to not less than 250 g. Quickly place in a tightly
sealed container. (For small riffle, see Method D 2013, Fig. 3.)
9.3.3.2 Thoroughly mix before extracting portions for re-
sidual moisture determination.
9.3.3.3 Proceed as in 9.3.2.5, except that the quantity
weighed into the capsule shall be approximately 5 g and the
drying time shall be 1
1
2 h.
10. Calculation
10.1 Calculate the percent total moisture, M, as follows
when one stage of air drying has been used:
M 5 @R ~100 2 ADL!/100# 1 ADL (1)
where:
M = total moisture, weight %;
ADL = air dry loss, weight %; and
R = residual moisture, weight %.
10.1.1 Calculate percent air-dry loss, ADL, as follows:
ADL 5 ~L/G! 3 100 (2)
where:
ADL = air-dry loss, weight %;
L = loss in weight in air drying, g; and;
G = weight of gross sample, g.
10.1.2 Calculate percent residual moisture, R, as follows:
R 5 @~W 2 H!/W# 3 100 (3)
where:
W = weight of sample used, g and
H = weight of sample after heating, g.
10.2 Calculate the percent total moisture, M, as follows
when two stages of air drying have been used (on uncrushed
gross sample and on crushed and divided laboratory sample or
on crushed and divided samples from two stages of crushing,
for instance, to the 4.75- and 2.36-mm (Nos. 4 and 8) top sieve
sizes):
M8 5 @R ~100 2 ADL8!/100# 1 ADL8 (4)
M 5 @M8 ~100 2 ADL!/100# 1 ADL (5)
where:
M = total moisture;
M8 = moisture in crushed and divided laboratory
sample;
ADL = air-dry loss, uncrushed gross sample or rst-stage
crushed and divided sample;
ADL8 = air-dry loss, laboratory sample; and
D 3302 02a
5
R = residual moisture.
10.2.1 Calculate air-dry losses ADL and ADL8 as for ADL in
10.1.1.
10.2.2 Calculate percent residual moisture, R, as in 10.1.2.
11. Precision and Bias
3
11.1 PrecisionThe relative precision of this test method
for the determination of total moisture covers the concentration
range from 1.6 to 7.9 % for bituminous coals and 12.4 to
31.2 % for subbituminous and lignitic coals. The repeatability
and reproducibility intervals given below apply only to coals
without free (surface) moisture in the gross sample before
preparation of No. 8 (2.36-mm) sieve-size subsamples. When
duplicate No. 8 (2.36-mm) sieve-size subsamples are air dried,
reduced to No. 60 (250-mm) sieve size, and their residual
moistures determined, the following repeatability and repro-
ducibility intervals apply to the resulting total moisture values.
11.1.1 RepeatabilityThe difference in absolute value be-
tween two consecutive test results, carried out on duplicate
subsamples in the same laboratory, by the same operator using
the same apparatus, should not exceed the repeatability interval
for more than 5 % of such paired values (95 % condence
level). When such a difference is found to exceed the repeat-
ability, there is reason to question one or more of the test
results. The repeatability interval for this test method is:
Bituminous 0.14 %
Subbituminous and lignite 0.42 %
11.1.2 ReproducibilityThe difference in absolute value of
replicate determinations, carried out in different laboratories,
on representative samples, should not exceed the reproducibil-
ity interval for more than 5 % of such paired values (95 %
condence level). When such a difference is found to exceed
the reproducibility interval, there is reason to question one or
more of the test results. The reproducibility interval for this test
method is:
Bituminous 0.62 %
Subbituminous and lignite 0.70 %
11.2 BiasSee Appendix X1 on accuracy of determination
of moisture in coal.
11.2.1 Since there is no acceptable reference materials for
determining the bias for this test method, no statement on bias
is being made.
12. Keywords
12.1 air-drying; air-drying loss; coal; residual moisture;
total moisture
APPENDIX
(Nonmandatory Information)
X1. ACCURACY OF DETERMINATION OF MOISTURE IN COAL
X1.1 The accurate determination of moisture in coal of
various ranks has long been a subject of discussion and
investigation. As has been pointed out in the referenced
investigations, one of the major difficulties in assigning abso-
lute merit to a particular procedure is the multiplicity of
conditions under which water exists in coals and the difficulties
involved in obtaining sharp separation and distinction among
these conditions.
X1.2 As stated by Gauger (1), Water recoverable from
coal is obtained from the following sources: (1) decomposition
of organic molecules (sometimes called combined water), (2)
surface-adsorbed water, (3) capillary-condensed water, (4)
dissolved water, and (5) water of hydration of inorganic
constituents of the coal.
X1.3 Brown (2) further refers to ( 1) Free or adherent
moisture (essentially surface adsorbed) possessing the physical
properties of ordinary water, (2) physically bound or inherent
moisture of vapor pressure lowered by the small diameter of
the pores of the coal structure in which it is absorbed, and (3)
chemically bound water of hydration or combined water.
X1.4 It becomes apparent, then, that total moisture in
principle represents a measurement of all of the water not
chemically combined.
X1.5 Traditionally, thermal treatment has provided the most
commonly used basis for attempting to separate the nonchemi-
cally bound water from coal, and the measurement is normally
made by weight loss. The absolute separation of adsorbed
moisture without loss of a portion of chemically bound water
is most difficult, if not impossible. The separation is particu-
larly difficult in geologically younger coals of lower rank.
Investigators (3,4,5) have shown that the amount of water
extracted is a function of both temperature and time. The
problem is further compounded by the susceptibility of certain
coals to oxidation.
X1.6 Because of such problems, investigators have pro-
posed a number of schemes to satisfy their particular objectives
in the measurement of water associated with coal.
These include:
X1.6.1 Heating in air at varying temperatures and for
varying time intervals.
X1.6.2 Heating in inert atmospheres (nitrogen, helium,
argon, and so forth).
X1.6.3 Separation of water by distillation with benzene,
toluene, xylene, kerosine, and so forth.
X1.6.4 Measurement of water by such chemical methods as
Karl Fischer titrations.
3
Supporting data are available from ASTM Headquarters. Request RR D05-
1015.
D 3302 02a
6
REFERENCES
(1) Gauger, A. W., Condition of Water in Coals of Various Ranks,Trans-
actions of the TAIMA, Vol 101, 1932, pp. 148164.
(2) Brown, G. M., The Determination of Moisture in Coals, National Gas
Bulletin, Australia, Vol 17, 1953, pp. 1421.
(3) Goodman, J. B., Gomez, M., and Parry, V. F., Determination of
Moisture in Low-Rank Coals, Bureau of Mines, R.I. 4969, 1953, p.
20.
(4) Barghoorn, E. S., and Spackman, W., Geological and Botanical Study
of the Brandon Lignite and its Signicance on Coal Petrography,E-
conomic Geological, Vol 45, No. 4, 1950, pp. 344357.
(5) Hoeppner, J. J., Fowkes, W. W., and McMurtrie, R., Removal of
Moisture from Lignite in Inert Gas Atmospheres,Bureau of Mines,
R.I. 5215, 1956.
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