Tarea 2 de Op III

D1.
A continuous, steady-state distillation column with a total condenser and a part

separating methanol from water at one atmosphere (see Table 2-7 for data). The fee
kmol/h. The feed is 55 mol% methanol and 45 mol% water. We desire a distillate pro
90 mol% methanol and a bottoms product that is 5 mol% methanol. Assume CMO.
a. If the external reflux ratio L/D = 1.25 plot the top operating line.
b. If the boilup ratio /B = 2.0 plot the bottom operating line.
c. Step off stages starting at the bottom with the partial reboiler. Use the optimum f
Report the optimum feed stage and the total number of stages.
d. Plot the feed line. Calculate its slope. Calculate q. What type of feed is this?
componente
metanol
agua
D
B
Z
55 52.9411765 2.05882353
45 5.88235294 39.1176471
100 58.8235294 41.1764706
XD
0.55
0.45
0.9
0.1
A)
Ln/D = R
1.25
XD
XB
0.9
0.9
0.9
0
1.2
0.55
0.55
0.55
0
0.8
0.05
0.05
0.05
0
0.6
0.4
0.2
LOR
LOR
B)
m
b
0.55555556
X
Y
0.9
0
Lm/B
B
Lm
Vm
b
2
X
LOS
0.9
0.4
2
41.1764706
82.3529412
41.1764706
m
LOS
0.4
-0.05
0 0.1 0.2
-0.2
1.2
1
0.8
0.6
0.4
0.2
Y
0.05
-1.66533453693773E-016
0.05
-1.66533453693773E-016
0 0.1 0.2
-0.2
0.4
0.2
0.5
-1.66533453693773E-016
0.95
0 0.1 0.2
-0.2
C)
LOR
LOS
interseccion
LOA
D)
X
Y
0.55
0.55
0.31153846 0.57307692
m
b
-0.09677419 0.60322581
LOA
LOA
=_ X + _
=/(1)X - /(1)
m= Pendiente
q/(q-1)
q=
q= <0-1>
N
x
0.9
0.9
0.31153846 0.57307692
0.05
0.05
0.31153846 0.57307692
0.55
0.55
0.31153846 0.57307692
LOS
0.4
-0.05
X
Y
0.31153846 0.57307692
X
LOR
m
b
0.55555556
2
-0.09677419
-0.09677419
0.08823529
Parcialmente vaporizada
8.82 `Liquido
91.2% Vapor
cambio
0.9
0.76
0.76
0.6
0.6
0.4
0.4
0.25
0.25
0.12
0.12
0.04
0.04
otal condenser and a partial reboiler is

Table 2-7 for data). The feed rate is 100
er. We desire a distillate product that is
methanol. Assume CMO.
ating line.
eboiler. Use the optimum feed stage.
t type of feed is this?
XB
0.05
0.95
1.2
1
XY
0.8
X=Y
0.6
XD
0.4
0.2
LOR
XB
33453693773E-016
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
-0.2
1.2
1
XY
0.8
X=Y
0.6
XD
Z
0.4
XB
0.2
LOS
3453693773E-016
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
-0.2
0.4
0.2
LOS
XB
3453693773E-016
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
-0.2
1.2
y
0.9
0.9
0.82222222
0.82222222
0.73333333
0.73333333
0.62222222
0.62222222
0.45
0.45
0.19
0.19
0.03
1
0.8
0.6
0.4
0.2
-1.66533453693773E-016
-0.2
0 0.10.20.30.40.50.60.70.80.9 1
n de etapas
etapa optima
6
3
y
0
0.02
0.04
0.06
0.08
0.1
0.15
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
0.95
1
volatilidad
0
0.134
0.23
0.305
0.365
0.418
0.517
0.579
0.665
0.729
0.779
0.825
0.87
0.915
0.958
0.979
1
7.58198614
7.16883117
6.87529976
6.61023622
6.46391753
6.06556246
5.50118765
4.6318408
4.03505535
3.52488688
3.14285714
2.86813187
2.69117647
2.53439153
2.45363409
no cte
0 0.10.20.30.40.50.60.70.80.9 1
XY
X=Y
XD
Z
XB
LOR
LOS
LOA
Column K
N
a. A distillation column with a total condenser is separating acetone from etha

concentration of xD = 0.90 mole fraction acetone is desired. Since CMO is valid
constant. If L/V is equal to 0.8, find the composition of the liquid leaving the fif
the total condenser.
b. A distillation column separating acetone and ethanol has a partial reboiler th
equilibrium contact. If the bottoms composition is xB = 0.13 mole fraction acet
boilup ratio /B = 1.0, find the vapor composition leaving the second stage abov
reboiler.
c. The distillation column in parts a and b is separating acetone from ethanol a
= 0.13, L/V = 0.8, and /B = 1.0. If the feed composition is z = 0.3 (all concentr
fraction of more volatile component), find the optimum feed plate location, tot
stages, and required q value of the feed. Equilibrium data for acetone and etha
(Perry et al., 1963, pp. 134) are
A)
DATOS:
Ln/Vn=
q (liquido)=
entonces R/(R+1)=
R=
componente
acetona
etanol
0.8
1
0.8
4
F
F
60
40
100
100
58
XD
0.9
0.9
0.9
0
0.6
0.6
0.6
0
LOR
0.1428571429 0.14285714
0.1428571429
0
LOS
XB
ETAPAS
1
2
3
42
LOR
LOS
LOA
0.582
-0.582
0.6456
0.6456
0.9
0.85
0.85
0.79
0.79
0.72
0.9
0.9
0.86
0.86
0.812
0.812
N
1.2
0.8
0.6
0.72
0.63
0.63
0.52
0.52
0.36
0.36
0.18
0.18
0.07
0.07
4
5
6
7
8
0.8
0.756
0.756
0.684
0.684
0.57462069 CAMBIO
0.57462069
0.39144828
0.39144828
0.18537931
0.18537931
0.05944828
0.6
0.4
0.2
0
0
0.1
Entonces el % de liquido en la 5 etapa es de 0.

B)
b. A distillation column separating acetone and ethanol has a

equilibrium contact. If the bottoms composition is xB = 0.13 m
boilup ratio /B = 1.0, find the vapor composition leaving the s
reboiler.
DATOS:
Vm/B=
q=
1
1.1
D
100
m
LOR
LOS
X
27.8
b
0.5530546624 0.27974277
2
-0.13
Y
0.2831777778 0.43635556
componente
acetona
etanol
20
80
100
72.2
1.1
XD
XB
ETAPA
N
1
2
3
0.6258992806
0.42
0.42
0.28
0.28
0.21
0.62589928
0.62589928
0.51202572
0.51202572
0.43459807
0.43459807
1.2
0.8
0.6
0.8
0.21
0.12
0.12
0.29 CAMBIO
0.29
0.11
0.6
0.4
Entonces el % de vapor en la 2 etapa es de 0.512

0.2
0
0
0.1
0.2
0.3
C)
c. The distillation column in parts a and b is separating aceton

= 0.13, L/V = 0.8, and /B = 1.0. If the feed composition is z =
fraction of more volatile component), find the optimum feed p
stages, and required q value of the feed. Equilibrium data for
(Perry et al., 1963, pp. 134) are
DATOS:
Ln/Vn=
entonces R/(R+1)=
R=
Vm/B=
0.8
0.8
4
1
componente
acetona
etanol
m
LOR
LOS
0.18
-0.13
Y
0.2583333333
30
70
100
D
100 22.0779220779
b
0.8
2
XD
Z
0.3866666667
XB
ETAPA
N
1
2
0.9
0.86
0.86
0.809
0.809
0.9
0.9
0.868
0.868
0.8272
1.2
0.8
0.6
3
4
5
6
7
8
9
0.74
0.74
0.66
0.66
0.56
0.56
0.44
0.44
0.31
0.31
0.21
0.21
0.12
0.12
0.8272
0.772
0.772
0.708
0.708
0.628
0.628
0.532
0.532
0.428
0.428
0.29 CAMBIO
0.29
0.11
0.8
0.6
0.4
0.2
0
0
0.1
0.2
0.3
0.4
Posee 9 etapas
La alimentacion se encuentra
ting acetone from ethanol. A distillate

sired. Since CMO is valid, L/V =
he liquid leaving the fifth stage below
X
0
0.1
0.15
0.2
0.25
0.3
0.35
0.4
0.5
0.6
0.7
0.8
0.9
1
has a partial reboiler that acts as an

0.13 mole fraction acetone and the
g the second stage above the partial
acetone from ethanol and has xD = 0.9, xB

is z = 0.3 (all concentrations are mole
feed plate location, total number of
ta for acetone and ethanol at 1 atm
B
54
4
58
Z (supu)
6
36
42
Ln
1
1.2
1
0.8
0.6
0.4
0.2
0
0
0.1
0.2
0.3
0.4
0.5
XB
0.9 0.14285714
0.1 0.85714286
0.6
0.4
Vn
232
Vm
Lm
290
290
332
1.2
0.8
0.18
1.14482759 -0.02068966
0.9
0.582
XD
Y
0
0.262
0.348
0.417
0.478
0.524
0.566
0.605
0.674
0.739
0.802
0.865
0.929
1
0.9
0.6456
1
0.8
0.6
0.14285714 0.14285714
0.582
0.6456
0.6
0.582
0.6
0.6456
0.4
0.2
0
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.2
1
X-Y
0.8
X=Y
XD
0.6
Z
XB
1
X-Y
X=Y
0.8
XD
Z
0.6
XB
LOR
LOS
0.4
LOA
N
0.2
0
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
en la 5 etapa es de 0.52
tone and ethanol has a partial reboiler that acts as an

mposition is xB = 0.13 mole fraction acetone and the
mposition leaving the second stage above the partial
B
17.4
10.4
27.8
Ln
Z (supu)
2.6
69.6
72.2
Vn
XD
0.2
0.8
Vm
XB
0.63
0.37
0.13
0.87
Lm
34.4
62.2
72.2
144.4
0.63
0.63
0.63
0
LOR
0.63
0.63
0.28317778 0.43635556
0.2
0.2
0.2
0
LOS
0.13
0.13
0.28317778 0.43635556
0.13
0.13
0.13
0
LOA
0.2
0.2
0.28317778 0.43635556
X-Y
X=Y
XD
Z
XB
LOR
1
X-Y
X=Y
XD
Z
XB
LOR
LOS
LOA
N
0
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
d b is separating acetone from ethanol and has xD = 0.9, xB

feed composition is z = 0.3 (all concentrations are mole
find the optimum feed plate location, total number of
ed. Equilibrium data for acetone and ethanol at 1 atm
D
B
Z
19.8701299 10.1298701
2.20779221 67.7922078
22.0779221 77.9220779
B
R
77.9220779
XD
0.3
0.7
XB
0.9
0.1
0.13
0.87
Ln
Vn
Vm
Lm
4 88.3116883 110.38961 77.9220779 155.844156
0.9
0.9
0.9
0
LOR
0.9
0.9
0.25833333 0.38666667
0.3
0.3
0.3
0
LOS
0.13
0.13
0.25833333 0.38666667
0.13
0.13
0.13
0
LOA
0.3
0.3
0.25833333 0.38666667
X-Y
X=Y
XD
Z
XB
LOA
X-Y
X=Y
XD
Z
XB
LOR
LOS
LOA
N
0.1
0.2
0.3
0.4
0.5
0.6
mentacion se encuentra el la 8 etapa
0.7
0.8
0.9
=_ X + _
=/(1)X - /(1)
q/(q-1)
q
1.2
1
0.8
X-Y
0.6
X=Y
0.4
0.2
0
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
X-Y
X=Y
XD
Z
XB
LOR
LOS
LOA
0.6
0.7
0.8
0.9
X-Y
X=Y
XD
Z
XB
0.8
0.9
a. Una columna de destilacin con un

destilado
concentracin de xD = 0,90 fraccin
constante. Si L / V es igual a 0,8, enco
debajo
el condensador total.
b. Una columna de destilacin que se
acta como una
contactos de equilibrio. Si la composi
relacin boilup / B = 1,0, encontrar la
de la parcial
rehervidor.
c. La columna de destilacin en las pa
0,9, xB
= 0,13, L / V = 0,8, y / B = 1,0. Si la c
concentraciones son mol
fraccin del componente ms voltil)
nmero total de
etapas y requiere valor q de la alimen
(Perry et al., 1963, pp. 13-4) son
X-Y
X=Y
XD
Z
XB
LOR
LOS
LOA
N
0.9
1.2
1
X-Y
0.8
X=Y
XD
Z
0.6
XB
LOR
0.4
LOS
LOA
0.2
0
0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.2
1
X-Y
0.8
X=Y
XD
Z
0.6
XB
LOR
0.4
LOS
LOA
0.2
0
0
pendiente
interseccion
-2.08
0.924
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
_ X + _
/(1)X - /(1)
-2.08
0.67532468
olumna de destilacin con un condensador total se separa acetona a partir de etanol. Un

o
acin de xD = 0,90 fraccin molar de acetona se desea. Desde OCM es vlida, L / V =
e. Si L / V es igual a 0,8, encontrar la composicin del lquido que sale de la quinta etapa
nsador total.
olumna de destilacin que separa la acetona y el etanol tiene un rehervidor parcial que
mo una
s de equilibrio. Si la composicin de los fondos es xB = 0,13 moles fraccin acetona y la
boilup / B = 1,0, encontrar la composicin del vapor dejando la segunda etapa por encima
cial
or.
umna de destilacin en las partes A y B es separar acetona a partir de etanol y tiene xD =
L / V = 0,8, y / B = 1,0. Si la composicin de la alimentacin es z = 0.3 (todas las

aciones son mol
del componente ms voltil), encontrar la ubicacin de la placa de alimentacin ptima, el
total de
requiere valor q de la alimentacin. Datos de equilibrio de acetona y etanol a 1 atm
al., 1963, pp. 13-4) son
X-Y
X=Y
XD
Z
XB
LOR
LOS
LOA
.8
X-Y
X=Y
XD
Z
XB
LOR
LOS
LOA
0.9
r de etanol. Un
lida, L / V =
a quinta etapa
or parcial que
n acetona y la
tapa por encima
nol y tiene xD =
das las
tacin ptima, el
ol a 1 atm

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D1.

A continuous, steady-state distillation column with a total condenser and a part

otal condenser and a partial reboiler is

eboiler. Use the optimum feed stage.

t type of feed is this?

a. A distillation column with a total condenser is separating acetone from etha

Entonces el % de liquido en la 5 etapa es de 0.

b. A distillation column separating acetone and ethanol has a

Entonces el % de vapor en la 2 etapa es de 0.512

c. The distillation column in parts a and b is separating aceton

ting acetone from ethanol. A distillate

has a partial reboiler that acts as an

acetone from ethanol and has xD = 0.9, xB

tone and ethanol has a partial reboiler that acts as an

d b is separating acetone from ethanol and has xD = 0.9, xB

mentacion se encuentra el la 8 etapa

a. Una columna de destilacin con un

olumna de destilacin con un condensador total se separa acetona a partir de etanol. Un

L / V = 0,8, y / B = 1,0. Si la composicin de la alimentacin es z = 0.3 (todas las

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