INDUSTRIAL TRAINING REPORT

FOR

PIGMENT MANUFACTURNG

OF

PIGMENT INDIA PRIVATE LIMITED

Duration: 28/05/2017 12/06/2017

Submitted by: 1) Kheni Parth (140420105023)

2) Pipalva jay (140420105050)

Submitted To :

Sarvajanik college of Engineering and technology,

B.E 3rd year , Chemical Engineering

Guided by :
Rajesh Virani

2017

M/S PIGMENT INDIA

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PI/BE/CH/PAK/04/2017-18 26TH June,2017

TRAINING CERTIFICATE

TO WHOM SO EVER IT MAY CONCERN

This is to certify that, Mr. PARTH A. KHENI and Mr. JAY G.

PIPALVA,student of B.E. Chemical engineering(III year, 6th sem.),has attend
the company from 28th MAY-2017 to 12th JUNE-2017, for training in our
company M/S PIGMENT INDIA.

He was found to obedient, sincere, punctual, hardworking and intelligent.

We wish him GOOD LUCK for his future endevors.

Your truly,

For M/S PIGMENT INDIA

PARTNER
RAJESH VIRANI

M/S PIGMENT INDIA

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 ACKNOWLEDGEMENT

Experience is the best guide. I was lucky enough to have take visit for ten day
at m/s pigment india. It provided me the best opportunity to learn things first
hand. It enables me to apply the theoretical knowledge and experience the
results..

It is very necessary to have a guide when you are a fresher in the corporate world
because that helps us in finding our way our goals easily.

I would like to express my sincere thanks to all the M/S PIGMENT

INDIA. without their support, this project would not have been a success.

I would also like to acknowledge and appreciate the guidance given to me by

Mr. Srujal Rana Faculty Members of Sarvajanik college of engineering and
technology.

M/S PIGMENT INDIA

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 INDEX

1. COMPANY PROFILE
2. ABOUT COMPANY
3. ENVIRONMENT AND SAFETY
4. PRODUCT PROFILE
5. TECHNICAL DATA FOR PATHALOCYANINE PIGMRNT
ALPHA BLUE
6. MANUFACTURING OF PATHALOCYANINE ALPHA BLUE
7. PROCESS FLOW CHART FOR ALPHA BLUE
8. TECHNICAL DATA FOR PATHALOCYANINE PIGMRNT BETA
BLUE
9. MANUFACTURING OF PATHALOCYANINE BETA BLUE
10.PROCESS FLOW CHART FOR BETA BLUE
11.APPLICATION
12.CONCLUTION
13.REFERANCE

M/S PIGMENT INDIA

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 COMPANY PROFILE

COMPANY NAME : M/S PIGMENT INDIA

YEAR
: 1988
ESTABLISHED
INDUSTRY
: PIGMENTS, PLASTICS,PAINT,INK
FOCUS
: PLOT NO C-1/7013 GIDC , IND. ESTATE,
ADDRESS
ANKLESHWAR -2 ( GUJARAT ) INDIA
PHONE NO : 02646 221754/329919
FAX NO. : 02646 239670
MOBILE : 9824011670
E-MAIL : info@pigmentindia.com
WEBSITE : www.pigmentindia.com
CONTACT
: MR. RAJESH VIRANI
PERSON
R & D STAFF : 11-20
: PHTHALOCYANINE PIGMENTS
PRODUCT
C.I. NO : 74160
COLOUR INDEX : PIGMENT BLUE 15:0, 15:1, and 15:3, 15:4
NAME
QUANTITY : 500 MT Per Annum

M/S PIGMENT INDIA

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 ABOUT COMPANY

PIGMENT INDIA was formed in 1988 as a part of our group of companies,

which consist of another two officiates M/s, Shree Ram Dye Chem. Industries
and M/s. Colours India. at Ankleshwar Industrial Estate in GUJARAT STATE
OF INDIA.

Company are very proud with the achievement made in last 18 years and
having a hard working aggressive team that is well connected with market
requirement allowed us to enter new areas with a wide range of products.

Thanks to our team work, which provide professional handling in dealing with
the agencies in hand our team of 5 sales engineers, supported by 10
administration and finance team are well connected and widely covers the
market in the areas of interest to us.

PIGMENT INDIA is well established company in India renowned for its

representation of well known Indian companies for the supply of pigment
powder suitable for all type of PAINTS, INKS, PLASTICS, RUBBER,
TEXTTILE EMULSION AND MASTER BATCHES etc.

Over the years company have established and developed a close working
relationship with all our clients within the India and solid business relationship
with your company for the mutual benefits of our both parties.

Company hope this will meets to your interest and we assure you of our
excellent quality product and prompt delivery in attractive packing, also
company add up that they can cater your need for any other organic pigments
from our group industries.

M/S PIGMENT INDIA

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 ENVIRONMENT AND SAFTEY

The layout of plant at Pigment India is designed to facilitate a completely clean

& pollution free working environment. Special safety codes are deployed &
necessary safety equipments are used in the plant to mark us a normal practice.

The organization is committed to accompany with all relevant environmental

legislation & products on the environment in accordance with the standards
and ISO-14001 by accredited with ISO-14001certification. We also take care of
health of the workers & employees working in our plant. Read & understand the
respective MATERIAL SAFTEY DATA SHEET (MSDS) before handling.

M/S PIGMENT INDIA

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 PRODUCTS

Pigmnet india is one of the major produc is phthalocyanine pigments. It has two
production units at ankleswer. PIGMENT INDIA is well established company
in India renowned for its representation of well known Indian companies for the
supply of pigment powder suitable for all type of PAINTS, INKS, PLASTICS,
RUBBER, TEXTTILE EMULSION AND MASTER BATCHES etc.

Main prodect of company:

Phthalocyanine alpha blue

Phthalocyanine beta blue

Phthalocyanine alpha blue products divided in 3 step:

Milling
Acid process
Pigmentation Process

Phthalocyanine alpha blue products divided in 2 step:

Milling
Pigmentation Process

M/S PIGMENT INDIA

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TECHNICAL DATA FOR PATHALOCYANINE
PIGMRNT ALPHA BLUE:

TECHNICAL DATA :

(1) PRODUCT NAME PHTHALOCYANINE PIGMENT ALPHA

BLUE
(2) CHEMICAL CLASS PIGMENT BLUE 15:1
(3) SUBSTANCE COPPER PHTHALOCYANINE
(4) MOLECULAR WEIGHT 576.08
(5) C.I. NUMBER 74160
(6) CAS NUMBER 147-14-8
(7) BULK DENSITY 0.35 to 0.45 GM/CC.
(8) ODOUR ODOURLESS
(9) PHYSICAL APPEARANCE BLUE POWDER
(10) COLOUR SHADE Masstone Tint

(11) SOLUBILITY IN WATER INSOLUBLE

(12) SPECIFIC GRAVITY(20 C) 1.4 to 1.6
(13) PH OF 10% Aq. SOL NEUTRAL
(14) HEAT STABILITY STABLE AT 280C FOR 10 MINUTTES
(15) HAZARDOUS NATURE NON HAZARDUS
(16) MOISTURE CONTENT 0.5% MAX.
(17) GREET CONTENT 260 ppm MAX.
(18) OIL 35 to 40
ABSORPTION(ML/100GM)
(19) SOLVENT STABILTY EXCELLENT
(20) LIGHT FASTNESS OUTSTANDING
(21) CHEMICAL RESISTANCE EXCELLENT

M/S PIGMENT INDIA

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MANUFACTURIN
MANUFACTURING OF
PATHALOCYANINE
ATHALOCYANINE ALPHA BLUE:
Stage 1 (Milling) :
Charge CPC (98 % ) in ball mill of capacity 10,000 liter. Mill the contents
for 24 Hrs. After grinding discharge the milled blue for stage 2.

Stage 2 (Acid process) :

Take sulphuric acid (98 %) in a reaction vessel. Then slowly charge
Copper Phthalocyanine crude.
Maintaining temperature just below 85 deg C . So as to dissolve it to
completely.
The mass is stirred further for 22-3 hrs. at 60 deg C and then cooled to room
temp. by external circulation of water in jacket.
Recycled water is then introduced as a thin spray into the vessel slowly,
taking care to maintain the temp. below 60 deg C.
The CPC separate out in the required form and is filtered off.
After filtration process whatever mother liquor generated that contains
approximate 20 % of sulphuric acid. We are using that liquor (H2SO4) into
the manufacture of CPC blue.

Stage 2 (Pigmentation Process) :

The CPC cake is charged in another vessel and washed with water and
stirred with fresh water.
The aqueous slurry is neutralized to pH 8 to 8.5 using ammonia solution
and caustic lye and stirred with emulsifier at 60 - 90 deg C for 2 Hrs.
The above slurry is filtered and the cake is washed with large amount of
fresh water.
The wet cake is dried and pulverized to obtain CPC Alpha Blue.
The aqueous filtrate goes to ETP.

M/S PIGMENT INDIA

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Process flow chart for alpha blue

BALL MILL
Crude CPC Blue + Steel Balls

REACTION IN MS VESSEL
CPC Blue + Sulphuric Acid

DROWNING VESSEL
Water

FILTER PRESS
Filter Pump,water

PIGMENTATION VESSEL
MS VESSEL,TLS,Caustic Lye,Water

Drying in SFD
Dry Powder

Classifier
Fine mesh powder

Blending
Mixing of different batches

Packing
HPDE Bags

Dispatch

M/S PIGMENT INDIA

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TECHNICAL DATA FOR PATHALOCYANINE
PIGMRNT BETA BLUE:
TECHNICAL DATA :

(1) PRODUCT NAME PHTHALOCYANINE PIGMENT

BETA BLUE
(2) CHEMICAL CLASS PIGMENT BLUE 15:4
(3) SUBSTANCE COPPER PHTHALOCYANINE

(4) MOLECULAR WEIGHT 576.08

(5) C.I. NUMBER 74160.4
(6) CAS NUMBER 147-14-8
(7) BULK DENSITY 0.35-.45 GM/CC
(8) ODOUR ODOURLESS
(9) COLOUR SHADE Masstone Tint

(10) PHYSICAL BLUE POWDER

APPEARANCE
(11) SOLUBILITY IN INSOLUBLE
WATER
(12) SPECIFIC GRAVITY(20 1.58-1.77
C)
(13) PH OF 10% Aq. SOL NEUTRAL
(14) HEAT STABILITY STABLE AT 280C FOR
10MINUTES
(15) HAZARDOUS NATURE NON HAZARDUS
(16) MOISTURE CONTENT 0.5% MAX
(17) GREET CONTENT 200 ppm MAX
(18) OIL 30-60
ABSORPTION(ML/100GM)
(19) SOLVENT STABILTY EXCELLENT
(20) LIGHTFASTNESS OUTSTANDING
(21) CHEMICAL EXCELLENT
RESISTANCE
(22) PARTICLE SHAPE ROAD LIKE MONOCLINIC
(23) MEAN PARTICLE SIZE 0.04 TO 0.06 MM
(24) SPECIFIC SURFACE 30 TO 70 M(2/GM)
AREA

M/S PIGMENT INDIA

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MANUFACTURING OF
PATHALOCYANINE BETA BLUE:

Stage 1 (Milling) :
Charge CPC (98 % ) in ball mill of capacity 10,000 liter. Mill
the contents for 24 Hrs. After grinding discharge the milled blue
for stage 2. (Pigmentation)

Stage 2 (Pigmentation) :
Charge above milled blue into MS vessel, contains caustic water
, Surfactants and solvent. Reflux whole mass under stirring for 2
Hrs.
Then recover the solvent. Filter the pigmented mass through
filter press, wash with water till neutral pH. Dry the pressed cake
in spin flash dryer at the rate of 150 Kg/Hr.

M/S PIGMENT INDIA

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Process flow chart for beta blue:

BALL MILL
Crude CPC Blue + Steel Balls

PIGMENTATION VESSEL
Grind Powder + NBA Solvent

FILTER PRESS
Wet Cake

SFD
Drying

CLASSIFIER
Fine Mesh Powder

BLENDER
Mix Different Batches

PACKING
HPDE Bags

DISPATCH

M/S PIGMENT INDIA

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 APPLICATION
All our Pigment Product is mainly suitable for following
application.

Printing Ink.
1 Gravure Printing
2 Tin Printing Ink.
3 Web Offset Inks.
4 Heat Set Ink.
5 Cold Set Ink.
6 Water Base Flexo Inks.
7 Nitro Cellulose Ink.
8 Poly Amino Ink.
9 Vinyl Ink.

Paint
1 Alkyed Paint
2 Water Base Paint.
3 Decorative Paint.
4 Automotive Paint.
5 Staving Paint.
6 Industrial Paint.
7 Dry Colors.

Plastics
1 Polythene Plastics.
2 Polystyrene Plastics
3 PVC Plastics
4 H.D.P.E./L.D.P.E./P.P.
5 Master Batches

M/S PIGMENT INDIA

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Rubber
1 Eva Rubber
2 Natural Rubber.

Textile
1 Water Base Textile Emulsions

Detergent
1 Dry Dispersion
2 Soap ,Washing Powder

M/S PIGMENT INDIA

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 CONCLUTION

The vocational training provided is essential step towards making the future
engineer familiar with the practical aspect of their field. During the training
period the trainee is exposed to the work of the company. And also the
training give opportunity to relate the theoretical knowledge with practical
operation.

During training I was made familiar with the various operations, equipment
and their function and the safety measure of individual working units. I made
these humble efforts to put up in words some information ,in brief, about the
operation of the plant that I could gather during training.

M/S PIGMENT INDIA

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 REFERANCE

1) www.pigmentindia.com

M/S PIGMENT INDIA

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