800 Users
800 Users
800 Users
USER'S MANUAL
Version 7.0
ZELTEX, Inc.
130 Western Maryland Parkway
Hagerstown, Maryland 21740
USA
Phone: 301-791-7080
Fax: 301-733-9398
E-mail: zeltex@zeltex.com
Website: www.zeltex.com
This manual provides you with all information needed to operate the Zeltex ZX-800.
1
TableofContents
WARNING.....................................................................................................................................................
PREPARATION.............................................................................................................................................
SAMPLE CUPS.............................................................................................................................................
VOLTAGE RING............................................................................................................................................
KEYPAD DESCRIPTION..............................................................................................................................
OPTIONAL PRINTER...................................................................................................................................
SELECTING A PRODUCT............................................................................................................................
EDITING A CALIBRATION...........................................................................................................................
TROUBLE-SHOOTING.................................................................................................................................
GLOSSARY...................................................................................................................................................
INDEX............................................................................................................................................................
2
WARNING
3
About the ZX-800
4
Preparation
After you have opened the carton take a moment to consider where to place the ZX-
800. While the ZX-800 has been designed to work flawlessly in the grain elevator
environment, there are a few things that must be considered before setting up the ZX-
800.
1. Electrical requirements
For best operation and reliability of the analysis the ZX-800 should have a clean
independent electrical line.
2. The ZX-800 should be placed on-line on a flat surface with enough room for
filling the sample cup with grain for analysis (and the optional printer if
purchased). Approximately three feet of counter space should be sufficient.
3. The ZX-800 should not be exposed to very wet conditions. Do not place on the
same counter with vibrating machinery. Do not place in direct sunlight.
4. The ZX-800 was preset for the voltage in your country. To check the voltage
setting, please look at the voltage ring on the back of the analyzer. There should
be a notch in the ring next to the voltage for your location. If the ring is set
incorrectly, turn the ring so the notch is toward the voltage for your country.
Incorrect voltage set-up can damage the ZX-800. See section VOLTAGE
RING, page 9 before changing voltage.
The ZX-800 is designed to be left on 24 hours a day, 365 days a year. While at rest the
ZX-800 Whole Grain Analyzer consumes about the same electricity as a standard 60
watt light bulb. If it cannot be left on, allow 60 minutes warm up time before running the
first sample.
5
Unpacking the ZX-800
Check that all items 1 through 4 are in the box. If any items are missing please contact
Zeltex immediately.
2. User's Manual
In addition, you may have purchased any of the following optional accessories:
The ZX-800 is mounted on an easy liftout tray. Grasp the handles and carefully lift the
analyzer from the box.
6
Appearance and Part Names
7
Sample Cups
The ZX-800 is shipped with a standard sample cup to be used with wheat and barley.
The soybean and corn sample cup is optional.
Do not place objects on the sample cup. It should not be placed on direct heat or
cleaned with harsh chemicals such as scouring powder.
16mm and below for smaller grains: 24mm for larger grains: corn, soybeans,
wheat, oats, canola, etc. etc.
8
Voltage Ring
The voltage in this illustration is set for 120 volts. If this is the correct voltage nothing
else needs to be done. To select another voltage, insert a flat screwdriver in the slot in
the center of the ring. The voltage selector will turn easily in either direction. Line up
the desired voltage with the notch. Incorrect voltage set-up can damage the ZX-
800.
9
Keypad Description
77 88 99 CAL
CAL
DISPLAY
DISPLAY OUTPUT
OUTPUT Contrast
TIME
44 55 66 <<
<< >>
>> TIME
DATE
DATE
11 22 33 CLEAR
CLEAR
AVG
AVG
Measure
Measure
00 ..
CM
CM
Key Name
b. AVG stands for average. This key will average the results of all previous
samples that have been measured since the AVG was last pushed.
NOTE: You must press the AVE key prior to running the samples you want to
average together. The screen will tell you the number of samples that are ready
for averaging (N=#).
c. TIME is used to set the time data output on the analyzer. This information is
sent to the (optional) printer to allow a time/date stamp on the printout.
d. OUTPUT allows you to decide if the RS232 port is being used for a printer or a
computer. Please be aware there are two different PC settings: PC1 and PC2.
The ZX-800 must be set to PC2 to communicate with the optional calibration
software. Press 2 to select PC2. Press 0 for optional printer.
The ZX-800 must be set to PC1 to communicate with the Z800 Instrument Edit
Program. Press 1 to select PC1.
f. When you press the CAL key, the following screen will appear:
CALI B RATI O N S
1: Select Product
2: Print Index
3: Time Stamp
AutoBIAS [if equipped]
8: Positions
Exit
g. << >> These are used within the calibration menu to move from point to point
when entering constants or other information, depending on the arrow
pressed.
11
h. Are used within the menus to move up or down to highlight and select an
item.
j. Enter key is used to save all information and to exit most programs.
k. 09 Number keys are used for entering data into the ZX-800. If the data is
negative use the "" key under the 3.
12
Optional Printer
If you did not purchase option A: Printer, please skip to page 16: Using the ZX-800 for
the First Time.
The ZX-800 optional printer weighs 950g. The external dimensions are 162mm x
240mm x 58.5mm. Printing method is thermal serial dot, speed 37.5 cps. You can
expect flawless printing results in temperature 0 o to 40o; humidity 30% (relative
humidity) RH to 80% RH. The printhead must be at the extreme left before you turn off
the printer.
The ZX-800 optional printer uses thermal paper, width 112mm, outer diameter 48mm,
roll length approximately 28m. The thermal paper used is compatible with Seiko
TP411-28CL or can be purchased from Zeltex. Non-thermal paper will not work in the
printer.
Interface Specifications are: Data input: Eight-bit parallel, handshake STROBE, BUSY,
and ACK.
13
Printer Operation Panel
5 ON LINE 3
FEED 2
4 POWER ON/OFF 1
1. Power Switch Slide the power switch to turn the power on or off
2. Paper Feed Switch When the printer is off-line, paper is fed while the paper
feed switch is pressed.
3. On-line Switch Press the on-line switch to turn the printer on-line or off- line.
Set the printer on-line to print from the computer.
Set the printer off-line to feed paper with the paper feed
switch or to stop printing. You can not input any data or
control codes.
5. On-line lamp When the printer is on-line, the on-line lamp lights. The light
flashes when data remains in the buffer memory when the
printer is off-line.
6. Off-line Lamp When the printer is off-line, the off-line lamp lights. if the
paper is not set or has run out, the lamp flashes. When an
error occurs, both the on-line and off-line lamps light.
1. Open the front of the paper holder, Using your thumb, pull paper holder cover
towards back of the printer (Unlock it).
4. Cut an angle on both sides of the paper so it comes to a point before inserting.
Place the roll in the printer so the paper unrolls toward the back of the printer.
14
5. Push the top of the paper into inlet and feed it by hand until you can see the tip
of paper from paper cutter.
6. Keep pressing the paper feed switch until the paper feeds straight and smoothly.
The off lamp will stop flashing when paper is inserted correctly.
See Trouble-Shooting (page 31) if your printer does not work correctly.
15
Using the ZX-800 for the First Time
1) Please check the voltage on the voltage ring on the back of the ZX-800.
Make sure it is set for the correct voltage for your area.
2) After checking the voltage, plug the AC cord into the back of the analyzer
and then into a voltage regulator/surge suppressor.
3) Turn on the power switch. The ZX-800 should boot up to the primary
menu.
5) If you ordered the instrument with the optional AutoBIAS feature, it will ask
you to run the AutoBIAS sample before reading other samples. Follow the
directions on Running the AutoBIAS Sample on page 17.
6) Measure ten (10) samples with the ZX-800 that have been analyzed by
your lab. Measure the samples using the directions on page 19 for
Analyzing a Grain Sample. Write the analysis in the chart provided and
fax the page or call Zeltex.
FAX 301-733-9398
PHONE in the USA, 800-732-1950
outside the USA, 301-791-7080
16
Running the AutoBIAS Sample
When you turn the instrument on each day, it will require you to run an AutoBIAS
sample in each product you use.* The autobias feature uses the latest NIR technology
to prevent the ZX-800 from drifting out of calibration.
Insert the AutoBIAS sample provided with your instrument. The instrument will read the
sample, just like a regular sample, and adjust the bias accordingly. (See also
Analyzing a Grain Sample on page 19.) Write down the amount of the bias adjustment
for each constituent on a photocopy of the following chart. (You can select to run an
AutoBIAS at any time, in addition to the daily prompt. On the ZX-800, make sure you
are in the product for the bias you want to adjust. Press CAL on the instruments
keypad. Select AutoBIAS from the Calibrations menu.)
* If you are unable to run the AutoBIAS sample for some reason, you can escape the daily prompt by pressing 8 8 1 . Do not
make a habit of ignoring the prompt, however. If you have lost the AutoBIAS sample, contact Zeltex for a replacement.
You are now ready to begin reading samples in the adjusted product!
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17
FAX TO Zeltex, Inc. at 1-301-733-9398
COUNTRY__________________________________________________________
FAX: _______________________________________________________________
Enter ten (10) samples that have been analyzed by your lab in the analyzed sample
row. In the second row, enter the ZX-800s readings of those samples. Fax to Zeltex for
advice concerning any needed adjustments.
18
Analyzing a Grain Sample
1. Turn power switch on. The ZX-800 must be on for a minimum of one hour before
measurement. The product the ZX-800 is measuring will show on the display.
NOTE: The ZX-800 should be left on at all times. It requires a minimum of
1 hour for warm-up if it has been turned off.
2. If the grain you are analyzing is not displayed, you need to change products
(see Selecting a Product, page 20).
3. Choose the correct cup for your product. See page 8, Sample Cups.
4. Load sample holder with grain and tap gently twice on table top or counter or
load the cup and place it on the optional shaker. Shake for approximately 30
seconds.
6. Close hood.
7. Press Measure.
8. In approximately 30 seconds (may take a little longer with some samples), the
analysis of the grain will be displayed.
10. If the optional printer is attached, you will get a printout of all constituents.
19
Selecting a Product
1. Press CAL.
The ZX-800 has been carefully calibrated at the factory; however, it is sometimes
necessary to adjust the bias or slope. These corrections can help fine tune the
instrument.
2) Slope Adjustment (changes the angle of prediction line to agree with the new lab
results).
The ZX-800, permits bias and slope correction, and allows full custom calibration, using
the optional calibration software and RS232 cable.
20
* Example of an outlier data point which must not be used when performing a K(0) or slope adjustment
21
Adjusting the Slope & Bias
Keep in mind: You should plot all data prior to doing a slope and bias
adjustment to verify that the data you are working with is correct.
Protein should always be done on an As-Is basis. NEVER do an
adjustment on a constant moisture basis.
The ZX-800 has been designed to meet NTEP requirements of
logging all changes. You must enter yes to when asked in order
to keep your log entries up to date.
To adjust the Slope and bias you need to access the Calibration Mode. To get into the
Calibration Mode you must:
1) Press the CAL key. The ZX-800 will show the following screen.
CALIBRATIONS
1: Select Product
2: Print Index
3: Time Stamp
AutoBIAS [if equipped]
8: Positions
Exit
2) Press CLEAR 9 9 1.
EDIT CALIBRATION
1: Duplicate Cal
2: Edit Contents
3: Add Cal
4: Delete Cal
5: Print Status
1: Group
2: Product Name
3: Cal Name
4: Unit
5: Unit Temp
EDIT CONTENTS
6: Sample Temp
7: Constants
8: Data Limits
9: Slope & Bias
SELECT CAL
1: CAL 1 2: CAL 2
3: CAL 3 4: CAL 4
9) Press the constituent you want to adjust. (CAL1 is PROTEIN and CAL2 is
MOISTURE ON CALIBRATIONS FROM ZELTEX.)
23
10) The following screen is displayed:
+000.00
Type in the adjustment you have received from either Zeltex or the adjustment
from your calculations. Please make sure the bias and slope displayed are
correct. The screen will first display +000.00. Use the arrow keys to highlight
what you want to change using the keypad to enter new numbers or symbols
Pay particular attention to the decimal point and whether the
number is + or .
NEW KO
1.2345E 1
NEW SLOPE
1.000E 0
13) If the bias and slope are not correct, press CLEAR to cancel.
14) If the bias and slope are correct, press the key again. "Busy" will appear on
the screen the ZX-800 will store the data the bias is adjusted.
24
Editing a Calibration
A calibration can be edited either with the aid of a computer and the ZX-800 Instrument
Edit program or manually. Editing can affect the accuracy and predictability of the ZX-
800, therefore you should not edit a calibration until you have read and understood this
manual fully. If you have any questions at all please contact Zeltex at 800-732-1950 or
(USA) 301-791-7080 or fax (USA) 301-733-9398, Monday through Friday, Eastern
Standard Time 7:30 am to 4:30 pm.
1. Press CAL.
2. Press CLEAR 9 9 1.
EDIT CALIBRATION
1: DUPLICATE CAL
2: EDIT CONTENTS
3: ADD CAL
4: DELETE CAL
5: PRINT STATUS
1: Duplicate Cal - Allows the user to duplicate into another product an existing
calibration. This key will duplicate the group, file name and all energy settings
into another product number. This is used for creating backups to the master
calibrations.
2: Edit Contents - This open a sub-menu if you press 2 the following menu
appears.
EDIT CONTENTS
1: GROUP
2: PRODUCT NAME
3: CAL NAME
4: UNIT
5: UNIT TEMP
25
6: SAMPLE TEMP
7: CONSTANTS
8: DATA LIMIT
9: SLOPE & BIAS
NOTE: You have to press to see the second half of this menu.
Each of these items allow you to adjust the criteria that are used to measure that
product you have currently selected.
1: Group - There are four different groups in the unit. The group name has
no meaning for the type of product that is actually run. These groups are
settings of energy. You are able to have four different energy settings for
different products within the ZX-800. These are preset at the factory and
cannot be adjusted in the field.
3: Cal Name - You can set 1 through 4 for different constituent names. This
will include any name you want: protein, moisture, oil, fat, etc. You enter
the information by highlighting the correct letter and pressing Select until
the whole name is entered. Highlight "END" and press Select.
4: Unit - It is recommended you put in the percent sign so the readout will
say for example 14.1% instead of just 14.1. You can also enter Parts per
million or any other notation you would prefer.
26
6: Sample Temperature - The ZX-800 was calibrated at this range of sample
temperatures. Zeltex recommends during calibration a range of -20C to
+50C. This is a very wide temperature range and can be done on the ZX-
800. Please note if the sample is either colder or hotter than the
temperature range to which it is set, an error warning, SAMPLE
TEMPERATURE OUT OF RANGE, will be displayed.
8: Data Limits - The calibration range. The high value and low value for each
constituent during calibration. These limits have been set in the ZX-800
for each product. If your reading exceeds the high or low limit, the ZX-800
will display "Warning, too high or too low."
9: SLOPE & BIAS - Allows you to do a slope & bias adjustment automatically
in the unit. NOTE: Any work in this mode must be time/date stamped for
memory and can affect the accuracy of the ZX-800. See page 22,
Adjusting the Slope & Bias.
Once you have completed work in the Edit Constants, press and return to the Edit
Calibration Menu.
3: Add Calibration - If you want to add a calibration select the Group. Define the
product name and all items for adding a brand new calibration. At the end the
ZX-800 will ask you if you want to save it. Make sure you do not save it over an
existing calibration, thus wiping out the existing calibration. Once you have
completed a calibration press exit to return.
4: Delete Calibration - If the product that has been calibrated is no longer going to
be tested you can delete the old calibration. However, once you have deleted it
all information is lost from the ZX-800. It is always best to keep the calibration
unless you have run out of room on the ZX-800.
Note: For more details on groupings and setting up calibrations, consult your
Calibration Manual. This manual has more information on how to adjust groups and so
forth.
5: Print Status - Prints the status of the calibration that is currently activated. This
includes all K values, ranges and other information. Print Status requires a
printer and will lock up the ZX-800 if a printer is not attached.
27
28
Entering a New Calibration
1) Press CAL.
4) Pick the group name that has the energies that are correct for the product you
are using. If you have any questions, contact Zeltex immediately and we can
tell you which group to use.
6) Once product name has been entered you must enter the constituent names.
The constituent names are referred to as CAL 1 - CAL 4 (Protein, Moisture, etc.)
7) After you have entered the Cal name you must enter the units in which the
constituent is measured to be displayed with the results. Most users use the %
sign.
8) Once you have entered the first constituent name and units you must continue
through all 4 CAL names. If no name is needed, enter END and exit out of each
one. Note: If you hold the key, you will get to END quickly.
11) Once all 4 constituent names and units are entered, the ZX-800 will ask you for
the unit temperature limits. This is the limit for the ambient temperature used in
the calibration. Zeltex recommends you calibrate between 10C and 45C by
chilling and warming the instrument with ice packs and heating pads during
calibration.
12) Once the temperature limits have been entered for ambient, sample temperature
limits must also be entered. This is the limits of the sample temperatures you
used during calibration. The ZX-800 is able to read as high as 60C and as low
as -20C. Enter the highest and lowest sample temperatures used during the
calibration. Note: If you are using a negative temperature, you must use the
"" (negative key) prior to entering in the temperature.
29
13) The ZX-800 will now ask you for the constants. The constants are entered in
scientific notation. They must be typed in correctly: Double-check them to
make sure they are correct.
14) After the constants are entered, the ZX-800 will ask for upper and lower data
limits. This is the range of the calibration. The Histogram Program will tell you
the data limits of the calibration.
16) After all the data has been entered for a new calibration the ZX-800 will ask you
for the destination. BE CAREFUL. DO NOT WRITE OVER AN EXISTING
CALIBRATION. Scroll to a vacant product and press .
18) Press again and you are ready to analyze the product.
The ZX-800 has a number of warnings to tell you if an analysis is out of specification.
These include the following:
30
Trouble-Shooting
6. Contact Zeltex.
The ZX-800 does not 1. Do you have the optional software and
communicate with the IBM RS232 cable?
computer.
2. In the Options menu, make sure the ZX-800
is set for PC2 for the Calibration Software or
PC1 for ZX-800 Instrument Edit.
7. Contact Zeltex.
31
SYMPTOM POSSIBLE SOLUTIONS
Poor repeatability 1. Make sure the cup is full to the top.
4. Contact Zeltex.
Poor accuracy/Bad readings 1. Are you in the correct product for the grain
you are using?
5. Contact Zeltex.
Display is blank. 1. Check the contrast knob, turn it to the left if
the display is all white and to the right if the
display is all blue.
3. Contact Zeltex.
Grain has spilled inside the ZX- 1. Slide the grain catch tray out from under the
800. ZX-800.
2. Contact Zeltex.
Printer problems Power lamp is off:
a. Turn on power switch.
b. Is the AC adapter connected correctly?
c. Is the battery recharged?
33
Glossary
application - the type of product the user is analyzing for a certain constituent(s)
bias - the average overall shift of the regression curve from the ideal laboratory
regression curve
constants - numbers that relate to the influence of each wavelength use in the
statistical calibration of the customers product
IR - abbreviation of infrared
light absorption - the amount of light energy absorbed by various constituents in the
product being measured
OD - optical data expressed in terms of voltage values for each wavelength used in a
Zeltex analyzer
sensor - a device used in Zeltex analyzers that converts light energy to electrical
signals for processing optical data
transmittance - the ease with which light or other forms of energy can pass through a
sample being tested
BLY - Barley
CRN - Corn
SOY - Soybean
SML - Soymeal
35
Index
A R
absorption, 34 range, 34, 35
AC adapter, 13, 33 regression, 34, 35
ambient temperature, 29 repeatability, 11, 32
application, 34 RS232, 6, 10, 20, 31
As-Is, 4, 10, 11, 18, 19
AutoBIAS, 1, 6, 16, 34
AVG, 10 S
Slope, 20, 22, 23, 27
B SML, 35
SOY, 35
bias, 34 SRW, 35
BLY, 35 stamp, 10, 11, 26
SWW, 35
C
T
calibration, 34
constant moisture, 10, 22 Too Dark, 30
constituent, 34 Too Light, 30
CRN, 35 Trouble-Shooting, 31
curve, 34
V
G
voltage ring, 5, 16
grain catch tray, 32
H
HRS, 35
HRW, 35
L
lab, 34
Loading, 14
P
Paper, 14, 33
36