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    Amines & Derivatives Plant: 17A Marlen Drive W Hamilton, NJ 08691 W USA Tel: (609) 586-8004 W Fax: (609) 586-0002

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    irsanti dewi
    This document summarizes an amines and derivatives plant that produces methyl amines, higher amines, dimethyl formamide, dimethyl aminoethanol, and choline chloride. The plant consists of six main units and was constructed in 1974 with major upgrades. It produces various chemical products for total capacities of 46,000 metric tons annually of methyl amines, 24,000 metric tons of dimethyl formamide, and smaller capacities of other products. Contact information is provided for sales representatives.

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    Amines & Derivatives Plant: 17A Marlen Drive W Hamilton, NJ 08691 W USA Tel: (609) 586-8004 W Fax: (609) 586-0002

    Uploaded by

    irsanti dewi
    90 views22 pages
    This document summarizes an amines and derivatives plant that produces methyl amines, higher amines, dimethyl formamide, dimethyl aminoethanol, and choline chloride. The plant consists of six main units and was constructed in 1974 with major upgrades. It produces various chemical products for total capacities of 46,000 metric tons annually of methyl amines, 24,000 metric tons of dimethyl formamide, and smaller capacities of other products. Contact information is provided for sales representatives.

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    pelajari saja

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    amines

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    This document summarizes an amines and derivatives plant that produces methyl amines, higher amines, dimethyl formamide, dimethyl aminoethanol, and choline chloride. The plant consists of six main units and was constructed in 1974 with major upgrades. It produces various chemical products for total capacities of 46,000 metric tons annually of methyl amines, 24,000 metric tons of dimethyl formamide, and smaller capacities of other products. Contact information is provided for sales representatives.

    Copyright:

    © All Rights Reserved
    Download as PPS, PDF, TXT or read online from Scribd
    Download as pps, pdf, or txt
    90 views22 pages

    Amines & Derivatives Plant: 17A Marlen Drive W Hamilton, NJ 08691 W USA Tel: (609) 586-8004 W Fax: (609) 586-0002

    Uploaded by

    irsanti dewi
    This document summarizes an amines and derivatives plant that produces methyl amines, higher amines, dimethyl formamide, dimethyl aminoethanol, and choline chloride. The plant consists of six main units and was constructed in 1974 with major upgrades. It produces various chemical products for total capacities of 46,000 metric tons annually of methyl amines, 24,000 metric tons of dimethyl formamide, and smaller capacities of other products. Contact information is provided for sales representatives.

    Copyright:

    © All Rights Reserved
    Download as PPS, PDF, TXT or read online from Scribd
    Download as pps, pdf, or txt
    of 22

    Amines &

    Derivatives Plant

    Please click on
    our logo or any
    link in this
    presentation to be
    redirected to our
    website & email.
    Thank You!

    17A Marlen Drive w Hamilton, NJ 08691 w USA


    Tel: (609) 586-8004 w Fax: (609) 586-0002
    www.ippe.com
    Introduction
     Highly integrated facility producing Methyl Amines for use in
    Higher Amines and Amine Derivatives
     Facility was constructed in 1974 with major upgrades in 1990
    and 2000
     Facility consists of six units:
    • Oil and Gas (CO/H2 Production) Unit
    • Methyl Amines (MMA, DMA, TMA) Plant
     46,000 MTA
    • Higher Amines Plant
     24,000 MTA
    • Dimethyl Formamide (DMF) Plant
     24,000 MTA
    • Dimethyl Amine Ethanol (DMAE) Plant
     7,000 MTA
    • Choline Chloride (Vitamin B12) Plant
     14,000 MTA
    Introduction
     Several attractive pieces of equipment
    • Compressors
    • Wiped Film Evaporator
    • Mechanical Extractor Column
    • Glass Lined Reactor
    • Larger High Pressure Reactors (600 PSIG) of
    CS and SS
    • Various SS Columns and Exchangers

     Process has been water washed and is


    ready for dismantlement
     57 acres of land, two thirds undeveloped
    Oil/Gas Unit (CO & H2 Production)
    Oil/Gas Unit Summary

    This unit produces carbon monoxide (which is a feedstock for the DMF
    production process) by the partial oxidation of natural gas in oxygen using
    Texaco gasification technology. Natural gas is supplied by pipeline from Transco
    (via Terra), and oxygen is supplied by pipeline from BOC. The Oil Gas Plant is
    located in the north-eastern corner of the site. By-products of this reaction are
    hydrogen and carbon dioxide. Carbon dioxide is removed with potassium
    carbonate solution (Benfield CO2 removal process) and vented, while the
    hydrogen is either flared-off or sent by pipeline to Terra for use as a fuel in its
    ammonia plant. Further separation is performed with membranes to achieve a
    70/30 mix of CO/H2. Arsenic trioxide (a corrosion inhibitor) is used within the Oil
    Gas Plant as a coating to the majority of the finishing process equipment.

    Chemistry:
    Heat + CH4 + ½ O2  CO + 2H2

    Side Reactions include

    3S + CH4 + ½ O2  2H2S + COS


    CH4 + 2O2  CO2 + 2H2O
    Oil/Gas Unit Process Flow
    Methyl Amines Unit
    (Mono, Di and Tri Methyl Amines Production)
    Methyl Amines Unit Summary

    This is a CONTINUOUS operation and is the heart of the plant and is by far the
    largest unit with a capacity of 46,000 MTA mixed amines production. This unit
    produces monomethylamine (MMA), dimethylamine (DMA) and trimethylamine
    (TMA) from the reaction of methanol and ammonia. Methanol and Ammonia is
    delivered via pipeline from a Terra site Methanol storage area and from Terra’s
    ammonia plant. Up to approximately 1,800 tons of methylamines (anhydrous and
    aqueous) are stored at the site in 13 large above ground bulk storage tanks,
    situated adjacent to the plant in the north-western area of the site.

    Chemistry:
    Ammonia & Methanol  Monomethylamine & Water

    Monomethylamine & Methanol  Dimethylamine & Water

    Dimethylamine & Methanol  Trimethylamine & Water

    For Methyl Amines Process Description Click Here


    Methyl Amines Unit Process Flow
    Higher Amines Unit
    Higher Amines Unit Summary

    This unit takes the “lower” amines from the Methyl Amines plant and attaches
    them to a higher molecular weight molecule such as Ethanol, I-Propanol and
    Butanol. This is followed by hydrogenation in a 300 PSIG shell and tube carbon
    steel reaction vessel with catalyst. Separation follows in a series of six columns
    and evaporators. The wiped film evaporator in this unit has never been used.
    Di-methyl Formamide Unit (DMF)
    DMF Unit Summary

    DMF is a CONTINOUS operation produced by the reaction of DMA (from the


    Methylamines Plant) and carbon monoxide (from the Oil Gas Plant) at a capacity
    of 24,000 MTA. The DMF Plant is located between the Methylamines Plant and the
    Oil Gas Plant at the northern area of the site. Approximately 800 tons of DMF is
    stored at the site in two large tanks, located adjacent to the north side of the
    plant. Sodium methoxide (received as a solution in methanol) is used as a
    catalyst in the manufacture of DMF.

    Chemistry:
    Sodium Methoxide in
    Methanol Catalyst


    Dimethylamine & Carbon Dimethylformamide
    Monoxide

    For Di-methyl Formamide Process Description Click Here


    DMF Unit Process Flow
    Di-methyl Amine Ethanol (DMAE) Unit
    DMAE Unit Summary

    This unit has CONTINUOUS front end and a BATCH distillation operation. This
    derivatives unit produces DMAE by the reaction of DMA (piped from methylamines
    plant) and ethylene oxide (EO) at a capacity of 7,000 MTA. Crude DMAE is purified
    in a continuous distillation unit. The resulting product is then stabilized by
    hydrogenation in the hydro-refining column using a Palladium catalyst.
    Approximately 700 tons of DMAE is stored at the site in eight large tanks, located
    to the north and south of the plant.

    Chemistry:


    (CH2)2O (CH3)2NH (CH3)2NC2H4OH
    Ethylene + Dimethylamine Dimethylaminoethanol
    Oxide

    For DMAE Process Description Click Here


    Choline Chloride Unit
    (Vitamin B12 for Chicken Feed)
    Choline Chloride Unit Summary
    This unit has BATCH front end (reaction) and a CONTINUOUS distillation operation.
    This derivatives unit produces Choline Chloride at the rate of 14,000 MTA by the
    reaction of TMA (from Methylamines Plant) with hydrochloric acid and then EO in a
    glass lined, batch reactor. Crude choline chloride is purified in a continuous glass
    distillation column. Piping in this plant is primarily glass lined or Titanium. Heat
    exchangers are primarily carbon block. Approximately 200 tons of aqueous choline
    chloride is stored at the site in four tanks, located adjacent to the west side of the
    plant. Hydrochloric acid is stored in a tank, adjacent to the east side of the plant.

    Chemistry:
    Neutralization


    HCI (aq) + (CH3)3N (liq) [(CH3)2NH]+ Cl (aq)
    Trimethylamine Trimethyl Ammonium Hydrochloride (Salt)

    Ethoxylation
    [(CH3)3NH] + Cl (aq) + CH2-O-CH2 (liq) [(CH3)3NCH2CH2OH]+ Cl (aq)

    Ethylene Oxide  Choline Chloride

    For Choline Chloride Process Description Click Here


    Choline Chloride Process Flow
    Equipment

     For Oil and Gas Equipment List Click Here


     For Methyl Amines (MA) Equipment List Click Here
     For Higher Amines Equipment List Click Here
     For Di-methyl Formamide (DMF) Equipment List Click Here
     For Di-methyl Amine Ethanol (DMAE) Equipment List Click Here
     For Choline Chloride (CC) Equipment List Click Here
     For EOD Equipment List Click Here
     For Export Equipment List Click Here
     For Maintenance Equipment List Click Here
    Contact Information
    MICHAEL JOACHIM SANJEEV REGE
    DIRECTOR, PLANTS DEPT. VP GLOBAL PLANT SALES
    Tele: 609-838-5930 (direct) Tele: 609-838-5938 (direct)
    Mobile: 609-516-9107 Mobile: 609-510-2616
    MichaelJ@ippe.com SanjeevR@ippe.com

    NARENDRA VASWANI
    SALES MGR., FAR EAST
    Tele: +91-265-2341057
    Mobile: +91-98250-64345
    NarendraV@ippe.com

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