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    S Y PH Meter

    Uploaded by

    Neelam Kapoor
    This document outlines the procedure for standardizing a pH meter and performing an acid-base titration. Key steps include: 1) Calibrating the pH meter using buffer solutions of pH 4, 7, and 9.2. 2) Titrating an unknown concentration of HCl with 0.1M NaOH solution, recording the pH and volume added at each step. 3) Creating a graph of pH vs volume of NaOH and determining the endpoint volume, then using this value along with the concentrations to calculate the normality of HCl.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd

    S Y PH Meter

    Uploaded by

    Neelam Kapoor
    101 views2 pages
    This document outlines the procedure for standardizing a pH meter and performing an acid-base titration. Key steps include: 1) Calibrating the pH meter using buffer solutions of pH 4, 7, and 9.2. 2) Titrating an unknown concentration of HCl with 0.1M NaOH solution, recording the pH and volume added at each step. 3) Creating a graph of pH vs volume of NaOH and determining the endpoint volume, then using this value along with the concentrations to calculate the normality of HCl.

    Original Description:

    ph meter experiment

    Original Title

    S Y ph meter

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    This document outlines the procedure for standardizing a pH meter and performing an acid-base titration. Key steps include: 1) Calibrating the pH meter using buffer solutions of pH 4, 7, and 9.2. 2) Titrating an unknown concentration of HCl with 0.1M NaOH solution, recording the pH and volume added at each step. 3) Creating a graph of pH vs volume of NaOH and determining the endpoint volume, then using this value along with the concentrations to calculate the normality of HCl.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    101 views2 pages

    S Y PH Meter

    Uploaded by

    Neelam Kapoor
    This document outlines the procedure for standardizing a pH meter and performing an acid-base titration. Key steps include: 1) Calibrating the pH meter using buffer solutions of pH 4, 7, and 9.2. 2) Titrating an unknown concentration of HCl with 0.1M NaOH solution, recording the pH and volume added at each step. 3) Creating a graph of pH vs volume of NaOH and determining the endpoint volume, then using this value along with the concentrations to calculate the normality of HCl.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 2

    Aim : Standardization of pH meter & acid-base titration.

    Apparatus: HCl (unknown conc.), 0.10 M NaOH, beaker,100-mL graduated


    cylinder, buret, pipette ,pH meter and electrode , pH buffer solutions
    (pH 4 ,7and 9.2)
    Theory: Most of the chemical and biochemical processes are profoundly affected by
    the acidity or alkalinity of the medium in which the reaction takes place. All acid
    dissociate in aqueous solution to yield H+ ions. Some acids like HCl, H2SO4, HNO3
    etc. are completely ionized in aqueous medium where as CH3COOH, HCOOH etc.
    ionize to a small extent only. The former is known as strong and the later as weak
    acid. pH of any solution is defined as (–log H+ ) and has values between 0–14. pH <
    7 indicate acidic solution, pH > 7 indicate basic solution and pH = 7 means neutral
    solution. The pH of a solution can be measured accurately with the help of a pH
    meter.
    Procedure:
    1)Switch on the instrument and wait for 10–15 minutes so that machine gets warmed
    up. Measure the temperature of the solution and set the temperature compensate
    control accordingly.
    2)Prepare the buffer solution by adding buffer tablets of pH = 4,7 and pH = 9.2 in 100
    mL of water separately. Wash the electrode with distilled water. Then, dip the
    electrode in the buffer solution (pH = 4) taken in a beaker, so that the electrode
    immersed to the solution properly. Set the pH meter to pH 4 and then rinse the
    electrode with distilled water to remove any excess solution.
    3)Similarly standardize the pH meter using basic buffer solution pH =7and 9.2.
    pH-metric Titration:
    1) Clean the electrode with distilled water. Take 10 mL of HCl solution in a
    100 mL beaker or conical and immerse the electrode in it. If neede add distilled water
    so that electrode is immersed.
    2) Set the burette with 0.1M NaOH solution. Note down the reading shown on the pH
    meter.
    3)Add NaOH solution drop wise from the burette (maximum 0.5 mL at a time), shake
    the solution well and note the corresponding pH values.
    4)Near the end point, volume of NaOH added should be as small as possible
    because the acid is neutralized and there will a sharp increase in pH values.
    5)Plot a graph between pH and volume of NaOH added and find out the volume of
    NaOH required (V2 mL) for complete neutralization of HCl from the graph ie value
    corresponding to pH 7. Then find out the normality of HCl (N1)
    Observation and Calculation:
    pH metric Titration Volume of HCl taken (V1)=…. (mL) . Normality of NaOH N2 =).1N

    pH Volume of NaOH

    N1 V1 = N2 V2
    Result: The normality of the HCl is ________(N)

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