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The Maharaja Sayajirao University of Baroda

Polytechnic ACADEMIC
Department of Petrochemical Technology YEAR
2012-2013
Polytechnic, Near Shastri Bridge, Fatehgunj,Vadodara-2
0265-2781983, , www.msubaroda.ac.in
Diploma : Full Time (Regular)
YEAR III IA 20
CHL3503 : Chemical Engineering V (Mass Transfer Operation II) UA 80
Semester I HOURS 56

COURSE CONTENT / SYLLABUS


Distillation
Vapour liquid equilibria press temp. Concentration diagram, Relative volatility,
ideal solutions, Raoult’s law, Flash Vaporisation, differential or simple
distillation (Rayleigh equation), steam distillation, vacuum distillation,
UNIT-I
principles of rectification, Binary system, material balance and energy balance 15 hrs.
for fractionating column, calculation of ideal stages by McCabe Thiele method,
Introduction of feed, location of feed tray, Minimum reflex ratio and infinite
reflux ratio, Optimum Reflux ratio, condenser & reboiler heat duty, continuous
Contact equipment, HTG, NTG, HOG, NOG, Types of Distillation column.
Types of tray, construction & Operation of distillation column.
Crystallization
Definition, crystal forms, crystal geometry, crystallization Equipments, phase
UNIT-II diagram, crystal yields, material and Energy balance calculation, Mier’s 06 hrs.
supersaturation theory and its limitation effect of operating condition on caking
of crystals prevention of caking.
Membrane separation processes
Types of Membrane – Brief introduction of membrane Separation processes,
UNIT-III 04 hrs.
Reverse osmosis, Micro filtration, Ultra filtration, Dialysis, Pervaporation,
permeation.
Extraction (Liquid – Liquid)
Definition –Field of usefulness, properties of solvent, Solvent requirement
equilateral triangular diagram, System of three liquids one pair partial soluble
system, System of three liquids – two pair partially soluble, System of two pairs
UNIT-IV partially soluble liquids with one Solid Effect of temp. and press on solubility 09 hrs.
diagram, Stagewise contact, calculation for single stage, Extraction and multi-
stage extraction equipments –Settlers, Mixer setter cascade sieve tray tower
Continuous contact Extractor, spray tower, Mechanically Agitated countercurrent
extractor pulsed column, Centrifugal extractor.
Drying
Definition of various terms, equilibrium, principles of Drying rate of drying
UNIT-V curve, Time of drying Batch Drying and continuous drying. Drying equipments 10 hrs.
Direct dryers and indirect dryers, Tray dryer, Rotary Dryer, Drum dryer, spray
dryer.
Adsorption and Ion exchange
UNIT-VI Definition- Industrial application, types of adsorption, Adsorption equilibria, 05 hrs.
equilibrium adsorption of single Vapour & gas mixture in brief, adsorption in
liquids, Adsorption of solute from dilute solution Freundlich Equation & its
scope, nature of adsorption, examples, Properties and application of typical
adsorption, Adsorption operation of various equipments, Ion Exchange,
principles, use of Ion exchange in D.M. water
Leaching
Definition of various terms, preparation of solid, Temp. of leaching methods of
UNIT-VII operation, unsteady state Operation. In place leaching, Heap leaching, 07 hrs.
calculation for single stage leaching, stage efficiency, equipments Percolation
tank, Shank system Agitated vessels, Bollman extractor.
REFERENCES
1. Mass transfer operation by Robert E. Treybal
2. Unit operations. Vol.2 By K.A. Gavhane
The Maharaja Sayajirao University of Baroda
Polytechnic ACADEMIC
Department of Petrochemical Technology YEAR
2012-2013
Polytechnic, Near Shastri Bridge, Fatehgunj,Vadodara-2
0265-2781983, , www.msubaroda.ac.in
Diploma : Full Time (Regular)
YEAR III IA 20
CHL3501 : Plant Operation UA 80
Semester I HOURS 56

COURSE CONTENT / SYLLABUS

Concept of maintenance theory of failure Accident Record keeping


UNIT-I 6 hrs.
failure or break down failures
Organisation check list & for maintenance, preventive maintenance,
UNIT-II Types of preventive maintenance, Record of maintenance & their 6 hrs.
relative usefulness, Modern Management & maintenance techniques.
Construction working & operation aspect (include Start up shut down
UNIT-III trouble shooting & maintenance) For the equipment’s like valves, 6 hrs.
pipes, fittings, flow meters pumps & compressor.
Construction, working & operation aspects (including start up, shut
UNIT-IV down trouble shooting & maintenance for equipment’s like size 6 hrs.
reduction machines, filtration centrifuges & classifiers.
Construction working & operation aspect (including start up, shut
UNIT-V down, trouble shooting & maintenance) for equipment’s such as Heat 8 hrs.
Exchangers & Evaporators.
Construction working & operation aspects (including start up, shut
UNIT-VI down & trouble shooting & maintenance) for equipment’s such as 8 hrs.
distillation tower, absorption tower & extractor.
Construction working & operation aspect & (including start up, shut
UNIT-VII down trouble shooting & maintenance), For the equipment such as 6 hrs.
dryers, crystallisers & cooling tower.
Construction working & operation aspect (including start up, shut
UNIT-VIII down trouble shooting & maintenance) for various reactors. 5 hrs.

Trouble shooting in plants (plant emergency) Electricity of cooling


UNIT-IX water DM water & feed failure, instrument air failure, steam failure, 5 hrs.
pump failure & remedial actions to be taken.
UNIT-X Commissioning Activities
REFERENCES
1. Various Industrial manuals
2. Handbook of Maintenance by McGraw Hill Publications.
Safe and Efficient Plant Operation and Maintenance Edited by Richard Green staff of chemical
3.
Engg. Mc. Graw Hill, New York.

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