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    Limit Test of Heavy Metals - Web Formulas

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    Limit Test of Heavy Metals - Web Formulas

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    86 views2 pages

    Limit Test of Heavy Metals - Web Formulas

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    knbiolabs
    ghg

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    Limit Test of Heavy Metals - Web Formulas https://www.web-formulas.com/Formulas_of_Chemistry/Limit_Test_of_...

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    Current Location > Formulas in Chemistry > Limit test > Limit Test of Heavy Metals

    Limit Test of Heavy Metals


    Recently Added Formulas in Chemistry
    · Limit Test of Arsenic
    Don't forget to try our free app - Agile Log , which helps you track your time spent on various
    · Limit Test of Lead
    · Limit Test of Heavy Metals projects and tasks, :)
    · Limit Test of Iron
    · Limit Test of Sulphate Try It Now
    Principle:
    Limit test of heavy metals is based on the reaction of metallic impurities with hydrogen sulfide
    in acidic medium to form brownish colour solution. Metals that response to this test are lead,
    mercury, bismuth, arsenic, antimony, tin, cadmium, silver, copper, and molybdenum. The
    metallic impurities in substances are expressed as parts of lead per million parts of the
    substance. The usual limit as per Indian Pharmacopoeia is 20 ppm

    Procedure:

    The Indian Pharmacopoeia has adopted three methods for the limit test of heavy metals.

    Method I: Use for the substance which gives clear colorless solution under the specific
    condition.
    Additional Formulas
    · Definition of Limit Tests Test sample Standard compound
    · Limit Test of Chloride Solution is prepared as per the monograph and Take 2 ml of standard lead solution and dilute to
    · Limit Test of Sulphate 25 ml is transferred in Nessler’s cylinder 25 ml with water
    · Limit Test of Iron
    · Limit Test of Heavy Metals
    Adjust the pH between 3 to 4 by adding dilute Adjust the pH between 3 to 4 by adding dilute
    · Limit Test of Lead acetic acid ‘Sp’ or dilute ammonia solution acetic acid ‘Sp’ or dilute ammonia solution ‘Sp’
    · Limit Test of Arsenic ‘Sp’
    Dilute with water to 35 ml Dilute with water to 35 ml
    Add freshly prepared 10 ml of hydrogen Add freshly prepared 10 ml of hydrogen
    sulphide solution sulphide solution
    Dilute with water to 50 ml Dilute with water to 50 ml
    Allow to stand for five minutes Allow to stand for five minutes
    View downwards over a white surface View downwards over a white surface

    Observation:

    The color produce in sample solution should not be greater than standard solution. If color
    produces in sample solution is less than the standard solution, the sample will pass the limit test
    of heavy metals and vice versa.

    Method II: Use for the substance which do not give clear colorless solution under the specific
    condition.

    Test sample Standard compound


    Weigh specific quantity of test substance, moisten Take 2 ml of standard lead solution and
    with sulphuric acid and ignite on a low flame till dilute to 25 ml with water
    completely charred
    Add few drops of nitric acid and heat to 500 °C
    Allow to cool and add 4 ml of hydrochloric acid and
    evaporate to dryness
    Moisten the residue with 10 ml of hydrochloric acid
    and digest for two minutes

    Dilute with water to 35 ml Dilute with water to 35 ml


    Add freshly prepared 10 ml of hydrogen sulphide Add freshly prepared 10 ml of hydrogen
    solution sulphide solution
    Dilute with water to 50 ml Dilute with water to 50 ml
    Allow to stand for five minutes Allow to stand for five minutes
    View downwards over a white surface View downwards over a white surface

    1 of 2 8/17/2020 4:15 PM
    Limit Test of Heavy Metals - Web Formulas https://www.web-formulas.com/Formulas_of_Chemistry/Limit_Test_of_...

    Observation:
    Agile Log - Project The color produce in sample solution should not be greater than standard solution. If color
    produces in sample solution is less than the standard solution, the sample will pass the limit test
    Time Management of heavy metals and vice versa.
    We track the time for you, so you
    Method III: Use for the substance which gives clear colorless solution in sodium hydroxide
    can focus on your tasks.
    solution.
    Show me more... Test sample Standard compound
    Or try our FREE app now Solution is prepared as per the monograph and Take 2 ml of standard lead solution
    25 ml is transferred in Nessler’s cylinder or
    weigh specific amount of substance and
    dissolve in 20 ml of water and add 5 ml of
    dilute sodium hydroxide solution
    Make up the volume to 50 ml with water Add 5 ml of dilute sodium hydroxide solution
    and make up the volume to 50 ml with water
    Add 5 drops of sodium sulphide solution Add 5 drops of sodium sulphide solution
    Mix and set aside for 5 min Mix and set aside for 5 min
    View downwards over a white surface View downwards over a white surface

    Observation:
    The color produce in sample solution should not be greater than standard solution. If color
    produces in sample solution is less than the standard solution, the sample will pass the limit test
    of heavy metals and vice versa.

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    2 of 2 8/17/2020 4:15 PM

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