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    Supplementary Information For: DESIREE Electrospray Ion Source Test Bench and Setup For Collision Induced Dissociation Experiments

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    Mohammad
    The document provides details on the components used in the DESIREE electrospray ion source test bench and setup for Collision Induced Dissociation experiments. It lists the commercial vacuum equipment, mass selection and detection components, as well as specifications for the main beamline elements used in the CID experiments. These include an Extrel quadrupole mass filter for ion selection, turbopumps and backing pumps to maintain vacuum, and microchannel plates for ion detection.

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    Supplementary Information For: DESIREE Electrospray Ion Source Test Bench and Setup For Collision Induced Dissociation Experiments

    Uploaded by

    Mohammad
    34 views2 pages
    The document provides details on the components used in the DESIREE electrospray ion source test bench and setup for Collision Induced Dissociation experiments. It lists the commercial vacuum equipment, mass selection and detection components, as well as specifications for the main beamline elements used in the CID experiments. These include an Extrel quadrupole mass filter for ion selection, turbopumps and backing pumps to maintain vacuum, and microchannel plates for ion detection.

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    EISLAB_instrumentation-supp-info

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    The document provides details on the components used in the DESIREE electrospray ion source test bench and setup for Collision Induced Dissociation experiments. It lists the commercial vacuum equipment, mass selection and detection components, as well as specifications for the main beamline elements used in the CID experiments. These include an Extrel quadrupole mass filter for ion selection, turbopumps and backing pumps to maintain vacuum, and microchannel plates for ion detection.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    34 views2 pages

    Supplementary Information For: DESIREE Electrospray Ion Source Test Bench and Setup For Collision Induced Dissociation Experiments

    Uploaded by

    Mohammad
    The document provides details on the components used in the DESIREE electrospray ion source test bench and setup for Collision Induced Dissociation experiments. It lists the commercial vacuum equipment, mass selection and detection components, as well as specifications for the main beamline elements used in the CID experiments. These include an Extrel quadrupole mass filter for ion selection, turbopumps and backing pumps to maintain vacuum, and microchannel plates for ion detection.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
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    Supplementary Information for: DESIREE electrospray ion source test bench

    and setup for Collision Induced Dissociation experiments


    N. de Ruette,1 M. Wolf,1 L. Giacomozzi,1 J. D. Alexander,1 M. Gatchell,1, 2 M. H. Stockett,1 N. Haag,1
    H. Zettergren,1 H. T. Schmidt,1 and H. Cederquist1
    1)
    Department of Physics, Stockholm University, Stockholm, SE-106 91, Sweden
    2)
    Institut für Ionenphysik und Angewandte Physik, Universität Innsbruck, Technikerstr. 25, A-6020 Innsbruck,
    Austria
    (Dated: 9 May 2018)

    I. LISTS OF COMPONENTS to lower the ions’ effective energies so that they do not
    travel too fast through the quadrupole (this is the case
    Details on commercial components, including the vac- for ions with kinetic energies above 12 eV). The ratio be-
    uum equipment, situated on the high voltage platform tween U and Vpp determines the mass resolution of the
    are given in Table I. Specifications of the main compo- filter. In order to keep a constant peak width across a
    nents of the beamline for CID experiment are listed in scanned mass range, the DC to RF voltage ratio needs
    Table II. to increase with increasing mass. Two commands of the
    CMS quadrupole control the resolution: ∆Res and ∆M .
    The first controls the slope of the linear increase of U/Vpp
    II. EXTREL QUADRUPOLE MASS FILTER and allows primarily to keep the heavier masses at the
    desired resolution. ∆M determines the intercept of this
    The ions are mass selected by an Extrel CMS line with the U-axis, optimizing the resolution at lower
    quadrupole mass filter (see Table I) with a m/z range masses. See Extrel Application Note RA-2010A2 for de-
    of 2-4000 amu/e. The combination of RF and DC volt- tails.
    ages determines the stable ion trajectories through the
    filter for each mass1 . In the Extrel CMS2 , the RF fre-
    III. REFERENCES
    quency is kept constant and variation of the DC Volt-
    age [U] and the peak-to-peak amplitude [Vpp ] of the RF
    voltage in combination is used to record a mass-to-charge 1 R.
    E. March, J. Mass Spectrom. 32, 351 (1997).
    spectrum. A pole bias (offset of the DC voltage), typi- 2 R.E. Pedder, Extrel Application Note RA 2010A: Practical
    cally 12 V below the pole bias on the octupole, is applied Quadrupole Theory: Graphical Theory. (2001).
    2

    TABLE I. Commercial components mounted on the high TABLE II. Commercial components
    voltage platform mounted on the beamline
    Item Notes item notes
    Syringe pump Harvard apparatus Gate valve VAT vacuum valve
    11 plus, single syringe Needle valve Balzers
    RF power supplies Ardara Technologies UDV 135
    Gate valve VAT vacuum valve Capacitance gauge Pfeiffer Vacuum
    Quadrupole Mass Filter Extrel CMS CMR 375
    3/800 Tri filter Microchannel plates Photonis
    Quadrupole Deflector Beam Imaging Solutions PS30434
    QID-900-H Advance Performance
    Active Film Electron Multiplier ETP Electron Multipliers Long-LifeTM
    AF185 MCP 40/32/25/8
    Cryogenerator Sumitomo Heavy Industries D 60:1 NR, TC
    RDK-415D Resistive anode Quantar Technology Inc.
    Pulsed poppet valve Parker Hannifin Corporation Pumping
    (He buffer gas in RET) P/N 009-0279-900 Gas cell and around
    Pumping Turbopumps Pfeiffer TMU 260
    Capillary Capacity N2: 210 L/s
    Roots Pump Leybold-Heraeus WSU 1000 Backing pump Pfeiffer Vacuum - Adixen
    Capacity 1000 m3 h−1 (280 L/s) Pascal 2010 SD
    Backing pump Straight section
    Capacity 65 m3 h−1 (18 L/s) Turbopump Pfeiffer Vacuum
    Octupole trap TMU 1000
    Rotary Vane Pump Pfeiffer Vacuum Duo 35 Capacity N2: 880 L/s
    Capacity 35 m3 h−1 (10 L/s) Backing pump Pfeiffer Vacuum - Adixen
    Octupole guide ACP15
    Turbopump Leybold Turbovac 361
    Capacity N2: 345 L/s
    Backing pump Pfeiffer Vacuum Duo 10M
    Capacity 10 m3 h−1 (2.8 L/s)
    Quadrupole Mass Filter
    Turbopump Leybold Turbovac 361
    Backing pump Pfeiffer Vacuum Duo 10M
    Quadrupole deflector
    Turbopump Pfeiffer Vacuum TMU 260
    Capacity N2: 210 L/s
    Backing pump Pfeiffer Vacuum Duo 10M
    Ring Electrode Trap
    Turbopump Varian Turbo-V 250
    Capacity N2: 250 L/s
    Backing pump Pfeiffer Vacuum Duo 10M

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