CLOSED

Version 0.4

Language English

Run 1

RunSerial 152

Instrument DMA Q800 V7.5 Build 127

Module DMA Multi-Frequency - Strain

Operator Hasni

File \\Upmdma-hp\ta\Data\DMA\amali\08.04.2015\G7\COKE BOTTLE

ProcName Temp

InstSerial 0800-0511

Clamp Tension: Film

Sample COKE BOTTLE

Geometry "Rectangular (Length, Width, Thickness)"

GeomFactor 28.563940 1/mm 0.045872 1/mm 1.310273 1/mm�

Size 21.8 6.36 0.12 mm

SampParams 0.42

Method Temp

Comment

Xcomment Air Bearing Gas: Air

Text

FreqTab 1

Multiplex None

InstCalDate Electronics: 2013-10-10 10:31:36 0.00005

InstCalDate Force: 2013-10-10 10:46:19 0.0103 Enabled

InstCalDate Dynamic: 2013-10-10 12:01:35 0.0158 Enabled

InstCalDate Clamp Date: 2015-04-08 11:29:35

InstCalDate Clamp Mass: 18.1 gm

InstCalDate Clamp Offset: -4.50 mm

InstCalDate Clamp Compliance: 0.409 um/N

TempCal 0 pts

Settings OscAmp 20.0 StaticF 0.0100 MinOscF 0.00001 StabCyc 4 AvgCyc 3

StoreStable AutoZero LengthFixed

Controls Gas 1 Event Off Sampling 2.0

AutoAnalysis Off

MacroFile

Nsig 17

Sig1 Time (min)

Sig2 Temperature (�C)

Sig3 Storage Modulus (MPa)

Sig4 Loss Modulus (MPa)

Sig5 Stress (MPa)

Sig6 Tan Delta

Sig7 Frequency (Hz)

Sig8 Drive Force (N)

Sig9 Amplitude (�m)

Sig10 Strain (%)

Sig11 Displacement (�m)

Sig12 Static Force (N)

Sig13 Position (mm)

Sig14 Length (mm)

Sig15 Force (N)

Sig16 Stiffness (N/m)

Sig17 GCA Pressure (kPa gauge)

Date 8/4/2015

Time 11:34:58

OrgMethod 1: Data storage On

OrgMethod 2: Equilibrate at 28.00 �C

OrgMethod 3: Ramp 5.00 �C/min to 160.00 �C

OrgFile C:\TA\Data\DMA\amali\08.04.2015\G7\COKE BOTTLE

StartOfData

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15.21508 8.877626 443664 0
10.4085 64.17241 12646.65 291.9674 11.61717 0.02310225 1
7.507756 20.00922 0.09178543 -4.75083 0.01000202 10.71907
15.21501 8.866225 443106.9 0
10.4585 64.42276 12629.53 292.6881 11.60158 0.02319142 1
7.49914 20.00972 0.09178769 -4.813982 0.01000246 10.719
15.21495 8.854325 442501.3 0
10.5085 64.67319 12612.21 293.4286 11.58664 0.0232828 1
7.491062 20.00964 0.09178734 -4.879086 0.01000291 10.71894
15.21489 8.842921 441933 0
10.5585 64.92413 12594.68 294.226 11.57067 0.02337938 1
7.482226 20.00981 0.09178812 -4.945492 0.01000127 10.71887
15.21482 8.830734 441320.2 0
10.6085 65.17496 12576.94 295.0501 11.55549 0.02347882 1
7.474005 20.00986 0.09178834 -5.01385 0.01000052 10.7188
15.21475 8.819147 440740 0
10.6585 65.42578 12559.01 295.9284 11.53926 0.02358328 1
7.465028 20.00978 0.09178799 -5.084164 0.01000104 10.71874
15.21468 8.806759 440122.8 0
10.7085 65.67689 12540.81 296.8458 11.52385 0.02369174 1
 7.456662 20.01014 0.09178962 -5.15643 0.01000156 10.71866
15.21461 8.795 439527.3 0
10.7585 65.9275 12522.42 297.81 11.50734 0.02380468 1
7.447544 20.00989 0.09178849 -5.230974 0.01000208 10.71859
15.21453 8.782405 438903.2 0
10.8085 66.17806 12503.76 298.8235 11.4917 0.02392249 1
7.439038 20.01082 0.09179274 -5.307472 0.01000282 10.71851
15.21446 8.770468 438286.3 0
10.8585 66.42912 12484.81 299.8845 11.47455 0.02404515 1
7.42955 20.00996 0.09178879 -5.386248 0.01000222 10.71843
15.21438 8.757376 437651 0
10.9085 66.67996 12465.56 301.0086 11.45854 0.0241739 1
7.420826 20.01121 0.09179452 -5.468604 0.01000051 10.71835
15.2143 8.745157 437013 0
10.9585 66.93116 12445.99 302.1783 11.44098 0.0243075 1
7.411122 20.01002 0.09178907 -5.552914 0.01000095 10.71826
15.21421 8.731756 436369.2 0
11.0085 67.18182 12426.12 303.4212 11.4245 0.02444813 1
7.402106 20.01158 0.09179626 -5.640805 0.01000184 10.71818
15.21412 8.719176 435706.4 0
11.0585 67.43225 12405.91 304.7106 11.40675 0.02459375 1
7.39234 20.01058 0.09179168 -5.730974 0.0100025 10.71809
15.21403 8.705631 435051.4 0
11.1085 67.68328 12385.27 306.0888 11.38955 0.0247481 1
7.38288 20.01192 0.0917978 -5.825701 0.01000317 10.71799
15.21394 8.692501 434366.2 0
11.1585 67.93454 12364.22 307.523 11.37139 0.0249085 1 7.3729
20.01065 0.09179199 -5.92303 0.01000042 10.7179 15.21384
8.678647 433701.4 0
11.2085 68.18487 12342.79 309.0474 11.35383 0.02507774 1
7.363228 20.01244 0.09180022 -6.02492 0.01000123 10.71779
15.21374 8.665245 432992.8 0
11.2585 68.43641 12320.79 310.642 11.33516 0.0252547 1
7.352957 20.01109 0.09179399 -6.130062 0.01000204 10.71769
15.21364 8.650989 432309.8 0
11.3085 68.68726 12298.34 312.3389 11.31685 0.02544185 1
7.342844 20.01262 0.09180099 -6.240414 0.01000293 10.71758
15.21352 8.63702 431578.8 0
11.3585 68.9372 12275.44 314.106 11.29789 0.0256366 1
7.332437 20.01151 0.09179593 -6.354996 0.01000025 10.71746
15.21341 8.622547 430879.4 0
11.4085 69.18816 12251.87 315.9974 11.27886 0.02584407 1
7.321888 20.01334 0.09180431 -6.474789 0.01000114 10.71734
15.21329 8.608024 430114.3 0
11.4585 69.4389 12227.67 317.9816 11.2591 0.02606166 1
7.311042 20.0121 0.09179864 -6.59979 0.0100021 10.71722
15.21316 8.592944 429387.3 0
11.5085 69.69012 12202.74 320.0966 11.23907 0.02629297 1
7.299907 20.01369 0.09180592 -6.73065 0.01000313 10.71709
15.21304 8.577656 428589.4 0
11.5585 69.94032 12177.14 322.3166 11.21864 0.02653582 1
7.288703 20.01283 0.09180199 -6.86704 0.0100006 10.71695
15.2129 8.562069 427829 0
11.6085 70.19104 12150.66 324.6776 11.19759 0.026794 1
7.276982 20.01463 0.09181022 -7.010271 0.01000171 10.71681
15.21276 8.546001 426987.8 0
11.6585 70.44172 12123.28 327.175 11.176 0.02706722 1
7.265121 20.01369 0.0918059 -7.16001 0.01000282 10.71666
15.2126 8.529525 426184.6 0
11.7085 70.6927 12094.88 329.8283 11.15367 0.02735789 1
7.25267 20.01534 0.09181347 -7.317562 0.01000058 10.7165
15.21245 8.512482 425298 0
11.7585 70.94343 12065.44 332.6376 11.13104 0.02766619 1
7.240228 20.01463 0.09181024 -7.483252 0.01000177 10.71634
15.21228 8.495206 424449.8 0
11.8085 71.194 12034.83 335.6152 11.10743 0.027994 1
7.22705 20.01621 0.09181747 -7.658057 0.01000325 10.71616
15.21211 8.477188 423516.2 0
11.8585 71.4451 12002.86 338.7878 11.08339 0.02834428 1
7.213806 20.01576 0.09181542 -7.841976 0.01000094 10.71598
15.21192 8.458847 422609.3 0
11.90867 71.69571 11969.5 342.1448 11.05823 0.02871703 1
7.199756 20.01708 0.09182147 -8.035988 0.01000256 10.71578
15.21173 8.439641 421622 0 Sig1 Time (min)
11.95867 71.9471 11934.45 345.7248 11.0329 0.02911652 1
7.185792 20.01699 0.09182106 -8.241718 0.01000174 10.71558
15.21152 8.420312 420658.3 0 Sig2 Temperature (�C)
12.00867 72.19759 11897.78 349.4992 11.00598 0.02954118 1
7.170725 20.01821 0.09182664 -8.459491 0.01000218 10.71536
15.2113 8.399762 419606 0 Sig3 Storage Modulus
(MPa)
12.05866 72.44874 11859.12 353.5172 10.97898 0.0299966 1
7.15582 20.01862 0.09182852 -8.690284 0.01000165 10.71513
15.21108 8.379158 418568.3 0 Sig4 Loss Modulus (MPa)
12.10866 72.6988 11818.47 357.7426 10.95001 0.03048104 1
7.139594 20.01951 0.09183259 -8.93475 0.01000231 10.71488
15.21083 8.357045 417445.1 0 Sig5 Stress (MPa)
12.15867 72.94988 11774.98 362.2433 10.9211 0.03100398 1
7.123608 20.01999 0.09183482 -9.195819 0.01000185 10.71462
15.21057 8.334986 416333.2 0
12.20867 73.2005 11728.89 366.9608 10.88999 0.03156087 1
7.106153 20.0213 0.09184082 -9.474139 0.01000169 10.71434
15.21029 8.31124 415119.9 0
12.25867 73.45178 11679.84 371.947 10.85844 0.03215834 1
7.088648 20.02213 0.09184465 -9.772641 0.01000161 10.71404
15.20999 8.287163 413900 0
12.30866 73.70226 11627.74 377.1452 10.82451 0.03279387 1
7.06961 20.02284 0.09184789 -10.09133 0.01000167 10.71373
15.20967 8.261269 412592.3 0
12.35866 73.95331 11572.09 382.5956 10.79067 0.03347394 1
7.050818 20.02388 0.09185265 -10.4341 0.01000195 10.71338
15.20933 8.235438 411280.9 0
12.40867 74.20405 11512.66 388.2481 10.75401 0.03419757 1
7.030204 20.02549 0.09186004 -10.80096 0.01000238 10.71302
15.20896 8.20746 409850.8 0
12.45867 74.4538 11449.37 394.0939 10.71632 0.03496621 1
7.009179 20.0275 0.09186924 -11.19549 0.01000185 10.71262
15.20857 8.178695 408373.3 0
12.50867 74.70494 11381.22 400.1369 10.67489 0.03578678 1
6.98583 20.02896 0.09187594 -11.61867 0.01000154 10.7122
15.20815 8.147076 406764.9 0
12.55866 74.95548 11308.42 406.3357 10.6323 0.0366576 1
6.962005 20.03094 0.09188507 -12.0757 0.01000144 10.71174
15.20769 8.114568 405101.6 0
12.60866 75.20599 11230.41 412.6326 10.58597 0.03757879 1
6.935875 20.03297 0.09189438 -12.56821 0.01000172 10.71125
15.2072 8.079214 403295.8 0
12.65867 75.45708 11146.76 419.0466 10.53791 0.0385575 1
 6.908914 20.035 0.09190368 -13.10044 0.01000111 10.71072
15.20666 8.042532 401424.2 0
12.70867 75.70772 11057.36 425.467 10.48568 0.03958746 1
6.879379 20.03787 0.09191681 -13.67792 0.01000183 10.71014
15.20609 8.00267 399377.4 0
12.75867 75.9586 10961.88 431.9026 10.43119 0.04067482 1
6.848738 20.04037 0.0919283 -14.30649 0.01000196 10.70951
15.20546 7.961084 397252.4 0
12.80867 76.20893 10860.62 438.1772 10.37188 0.0418012 1
6.815113 20.04374 0.09194374 -14.98781 0.01000119 10.70883
15.20478 7.91582 394927.3 0
12.85867 76.45999 10751.97 443.8974 10.30896 0.04293154 1
6.77954 20.04807 0.09196361 -15.72804 0.01000205 10.70809
15.20404 7.867795 392446.5 0
12.90867 76.71079 10636.42 449.6922 10.23926 0.04415254 1
6.739869 20.05188 0.09198111 -16.53045 0.01000232 10.70729
15.20324 7.814605 389719.3 0
12.95867 76.96103 10515.02 455.6358 10.16568 0.04547043 1
6.69815 20.0568 0.09200368 -17.40513 0.01000184 10.70641
15.20236 7.758447 386823.8 0
13.00867 77.2117 10387.05 460.8468 10.08489 0.04677347 1
6.652038 20.06106 0.09202324 -18.35988 0.01000203 10.70546
15.2014 7.696788 383667.9 0
13.05867 77.46239 10252.07 465.4788 9.99932 0.04809402 1
6.603293 20.06755 0.09205299 -19.40057 0.01000169 10.70442
15.20036 7.63148 380289.6 0
13.10867 77.71274 10112 470.629 9.904382 0.04957954 1 6.548813
20.07478 0.09208618 -20.53013 0.01000187 10.70329 15.19924
7.559024 376543.3 0
13.15867 77.96329 9967.126 475.0257 9.787735 0.05103615 1
6.490019 20.08173 0.09211801 -21.76255 0.01000063 10.70206 15.198
7.47 371980 0
13.20867 78.21351 9816.634 478.3966 9.674806 0.0524292 1
6.42577 20.08975 0.09215484 -23.10598 0.01000021 10.70071
15.19666 7.383811 367541.2 0
13.25867 78.46451 9661.452 482.552 9.552792 0.05405398 1
6.356016 20.09952 0.09219965 -24.56496 0.01000068 10.69925
15.1952 7.29069 362729.6 0
13.30867 78.71452 9525.425 488.2124 9.418482 0.05548907 1
6.278899 20.10941 0.09224499 -26.15155 0.01000203 10.69766
15.19361 7.188186 357453.9 0
13.35867 78.96544 9360.587 491.0546 9.274972 0.05706055 1
6.196219 20.12104 0.09229834 -27.87713 0.01000107 10.69594
15.19189 7.078658 351803.8 0
13.40867 79.21586 9192.47 493.6583 9.116816 0.05869062 1
6.104664 20.13402 0.09235791 -29.74628 0.01000234 10.69407
15.19002 6.957954 345581.9 0
13.45867 79.46637 9021.609 496.1622 8.947708 0.06039662 1
6.00628 20.14666 0.0924159 -31.77622 0.01000122 10.69204
15.18799 6.828891 338958.9 0
13.50867 79.71632 8848.851 498.0583 8.763571 0.06206626 1
5.898621 20.16282 0.09249001 -33.97088 0.01000136 10.68984
15.18579 6.688357 331717.3 0
13.55867 79.96714 8673.04 499.4242 8.56723 0.06373066 1
5.783161 20.17827 0.09256089 -36.3436 0.01000172 10.68748
15.18342 6.53851 324037.1 0
13.60867 80.21732 8495.926 500.9906 8.355881 0.0655286 1
5.658047 20.19478 0.0926366 -38.9022 0.01000237 10.68491
15.18086 6.377208 315785 0
13.65867 80.4684 8316.994 501.9992 8.132422 0.06729053 1
5.52494 20.21153 0.09271344 -41.65512 0.01000338 10.68216
15.17811 6.206664 307085.3 0
13.70867 80.71849 8137.375 502.3598 7.896235 0.06898748 1
5.383276 20.23136 0.09280439 -44.60662 0.01000096 10.67921
15.17516 6.026407 297874.6 0
13.75867 80.96858 7956.638 503.048 7.650131 0.07086409 1
5.234462 20.245 0.09286697 -47.7658 0.01000151 10.67605 15.172
5.838579 288396.1 0
13.8125 81.23188 7764.528 503.3024 7.395366 0.0728189 1
5.079203 20.26556 0.09296129 -51.3742 0.01000234 10.67244
15.16839 5.644143 278509.1 0
13.868 81.50689 7561.77 503.1209 7.107406 0.074876 1
4.902896 20.35854 0.09338778 -55.42205 0.01000108 10.6684
15.16434 5.424372 266442.2 0
13.9235 81.78658 7354.488 502.5581 6.79267 0.07699954 1
4.707138 20.29689 0.09310499 -59.67824 0.01000211 10.66414
15.16009 5.184165 255416.8 0
13.979 82.06622 7147.026 501.5818 6.525418 0.07913855 1
4.539947 20.30406 0.09313791 -64.11769 0.01000201 10.6597
15.15565 4.980198 245280.8 0
14.0345 82.34161 6943.164 500.2657 6.242956 0.08126861 1
4.362006 20.39378 0.09354945 -68.88755 0.01000161 10.65493
15.15088 4.764624 233631.2 0
14.09 82.61707 6739.707 498.585 5.943824 0.08341762 1 4.17126
20.31888 0.09320588 -73.84262 0.01000134 10.64998 15.14592
4.536328 223256.7 0
14.1455 82.89672 6533.484 496.4758 5.696925 0.08562066 1
4.01284 20.31886 0.09320578 -78.93182 0.01000152 10.64489
15.14083 4.347893 213983.1 0
14.201 83.17572 6329.66 493.9989 5.449163 0.08783207 1
3.852566 20.39364 0.09354882 -84.31951 0.01000027 10.6395
15.13545 4.158802 203926.4 0
14.2565 83.45139 6130.36 491.215 5.188909 0.0900333 1
3.68294 20.31651 0.09319499 -89.85564 0.01000102 10.63396
15.12991 3.960175 194924 0
14.312 83.73064 5942.994 489.8986 4.978863 0.09230211 1
3.545114 20.31056 0.09316772 -95.49399 0.01000222 10.62832
15.12427 3.799869 187088.3 0
14.3675 84.01062 5743.068 486.335 4.773533 0.09458722 1
3.409333 20.37094 0.09344465 -101.3866 0.0100014 10.62243
15.11838 3.64316 178841.1 0
14.423 84.28551 5549.924 482.5174 4.559438 0.09683759 1
3.26722 20.30198 0.09312837 -107.4227 0.01000131 10.6164
15.11234 3.479762 171400.1 0
14.4785 84.56488 5357.07 478.308 4.386127 0.09914285 1
3.151446 20.28866 0.09306726 -113.5318 0.01000145 10.61029
15.10623 3.347492 164993.2 0
14.534 84.84436 5168.334 473.8097 4.2213 0.101457 1
3.040454 20.34241 0.09331379 -119.8778 0.0100021 10.60394
15.09989 3.221696 158373.4 0
14.5895 85.11986 4986.796 469.1454 4.046143 0.103752 1
2.922548 20.2776 0.09301651 -126.3615 0.01000192 10.59746
15.0934 3.088016 152287.1 0
14.645 85.39535 4810.309 464.3025 3.906144 0.106059 1
2.827642 20.26742 0.09296985 -132.9198 0.01000211 10.5909
15.08684 2.981168 147091.6 0
14.7005 85.67437 4637.149 459.2084 3.773024 0.1084054 1
2.736712 20.30946 0.09316269 -139.6974 0.01000133 10.58412
 15.08007 2.879572 141784.7 0
14.75539 85.94916 4472.616 454.135 3.63061 0.1107299 1
2.639775 20.25439 0.09291007 -146.5536 0.01000225 10.57726
15.07321 2.770882 136804 0
14.806 86.20806 4323.156 449.2383 3.519257 0.1129239 1
2.563455 20.2334 0.09281378 -152.9777 0.01000147 10.57084
15.06679 2.685897 132745.7 0
14.856 86.45849 4182.835 444.203 3.417313 0.1150275 1
2.493355 20.23 0.09279816 -159.4523 0.01000107 10.56436 15.06031
2.608093 128922 0
14.906 86.70828 4050.244 440.5891 3.320396 0.1173064 1
2.42657 20.22127 0.09275812 -166.0467 0.01000282 10.55777
15.05372 2.534126 125319.8 0
14.956 86.95899 3924.015 436.2448 3.229918 0.1194922 1
2.364025 20.21518 0.09273019 -172.7749 0.01000189 10.55104
15.04699 2.465074 121941.7 0
15.006 87.20841 3803.642 431.6383 3.144142 0.1216323 1
2.304663 20.2095 0.09270411 -179.6284 0.01000222 10.54419
15.04014 2.39961 118736.7 0
15.056 87.4588 3689.822 428.0794 3.063606 0.1239199 1
2.248767 20.20192 0.09266938 -186.6242 0.01000232 10.53719
15.03314 2.338144 115738.6 0
15.106 87.70795 3583.506 424.5989 2.987306 0.1261771 1
2.195744 20.19611 0.09264272 -193.7518 0.01000234 10.53007
15.02601 2.279912 112888.6 0
15.156 87.95866 3482.537 420.9626 2.91544 0.1284114 1
2.145714 20.18876 0.09260899 -201.0282 0.01000109 10.52279
15.01874 2.225064 110213 0
15.206 88.2082 3387.944 417.946 2.847761 0.1307084 1
2.098518 20.18469 0.09259032 -208.4452 0.01000222 10.51537
15.01132 2.173411 107676.2 0
15.256 88.45929 3299.093 415.57 2.78345 0.1330967 1
2.053641 20.17663 0.09255334 -216.0116 0.01000199 10.50781
15.00375 2.124329 105286.6 0
15.306 88.70891 3233.518 414.5653 2.723181 0.1355838 1
2.011498 20.17234 0.09253366 -223.73 0.01000192 10.50009
14.99604 2.078332 103028.8 0
15.356 88.95936 3154.334 412.2308 2.665662 0.1379216 1
1.971304 20.16572 0.09250334 -231.6044 0.0100022 10.49221
14.98816 2.034433 100885.7 0
15.406 89.20942 3080.698 411.1538 2.611696 0.1404573 1
1.933499 20.16022 0.09247804 -239.6463 0.01000085 10.48417
14.98012 1.993246 98870.29 0
15.456 89.45905 3012.482 410.0808 2.56021 0.1429388 1
1.897478 20.15478 0.09245309 -247.8508 0.01000061 10.47597
14.97191 1.953952 96947.37 0
15.506 89.70953 2948.252 409.1204 2.51186 0.14542 1
1.86358 20.14786 0.09242136 -256.2358 0.01000178 10.46758
14.96353 1.917052 95149.18 0
15.556 89.9588 2888.688 409.0212 2.46604 0.1480284 1
1.831494 20.1436 0.09240182 -264.7886 0.01000175 10.45903
14.95498 1.882081 93433.22 0
15.606 90.20992 2833.115 409.2533 2.422935 0.1506786 1
1.80129 20.13582 0.09236616 -273.5305 0.0100023 10.45029
14.94624 1.849184 91835.53 0
15.656 90.45909 2781.809 409.6622 2.382547 0.1533007 1
1.773004 20.13262 0.09235149 -282.4468 0.01000159 10.44137
14.93732 1.81836 90319.07 0
15.706 90.71016 2733.804 410.6444 2.344049 0.1560284 1
 1.74608 20.12299 0.09230731 -291.5565 0.01000228 10.43226
14.92821 1.788978 88902.18 0
15.756 90.95982 2689.725 412.1803 2.308442 0.15882 1
1.721151 20.11906 0.0922893 -300.8544 0.01000237 10.42296
14.91891 1.761802 87568.81 0
15.806 91.21075 2648.88 413.9084 2.274642 0.1616081 1
1.697595 20.11368 0.0922646 -310.3485 0.01000261 10.41347
14.90942 1.736007 86309.75 0
15.856 91.46062 2611.208 416.0147 2.243371 0.1644272 1
1.675749 20.1041 0.09222064 -320.0464 0.01000216 10.40377
14.89972 1.712141 85163.76 0
15.906 91.71062 2576.507 418.5331 2.214075 0.1672888 1
1.655405 20.10127 0.09220768 -329.938 0.01000201 10.39388
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