2009 Table of Contents

Alphabetical Index

Method Latest
number issue
Accelerated Light Exposure of Edible Vegetable Oils........................................................................................Cg 6 –01 (09)
Acetone–Insoluble Matter in Lecithin..............................................................................................................Ja 4 –46 (09)
Acetone Tolerance of Heat–Bodied Drying Oils..............................................................................................Tt 1a –64 (09)
Acetyl and Hydroxyl Values (by saponification)...............................................................................................Cd 4 –40 (99) *
Acid–Insoluble Ash in Oilseed Meal Products..................................................................................................Ba 5b –68 (09)
Acid Value
of Commercial Fatty Acids........................................................................................................................Te 1a –64 (09)
of Dibasic Acids........................................................................................................................................Te 4a –70 (09)
of Drying Oils...........................................................................................................................................Te 2a –64 (09)
of Fats and Oils.........................................................................................................................................Cd 3d –63 (09)
of Fatty Acids . .........................................................................................................................................Da 14 –48 (09)
of Fatty Quaternary Ammonium Chlorides..............................................................................................Te 3a –64 (09)
of Lecithin................................................................................................................................................Ja 6 –55 (09)
Acidity
of Glycerin................................................................................................................................................Ea 2 –38 (73) *
of Sulfonated and Sulfated Oils, Dark Colored, with Exceptions..............................................................F 9b –44 (09)
of Sulfonated and Sulfated Oils, in the Presence of Ammonium or
Triethanolamine Soaps......................................................................................................................F 9c –44 (09)
of Sulfonated and Sulfated Oils, with Exceptions......................................................................................F 9a –44 (09)
Active Ingredients in Sulfonated and Sulfated Oils...........................................................................................F 4 –44 (09)
Active Oxygen Method (AOM) for Fat Stability..............................................................................................Cd 12 –57 (93) *
Activity of Hydrogenation Catalysts.................................................................................................................Tz 1a –78 (09)
Aflatoxins
in Copra and Copra Meal.........................................................................................................................Ah 1 –72 (09)
in Corn.....................................................................................................................................................Aj 1 –86 (09)
in Corn (affinity column)..........................................................................................................................Ab 7 –91 (09)
in Corn by ELISA.....................................................................................................................................Aj 6a –97 (09)
in Corn (whole, cracked, meal, germ).......................................................................................................Aj 3 –87 (09)
in Corn and Peanut by TLC.....................................................................................................................Aa 9a –97 (09)
in Corn, Zearalenone, and a–Zearalenol..................................................................................................Aj 2 –86 (09)
in Cottonseed, Seed Meal, Meats, Flakes...................................................................................................Aa 8 –83 (09)
in Dairy Products, M1 and M2. ................................................................................................................Cb 6 –86 (09)
in Peanut Butter (affinity column)............................................................................................................Ab 7 –91 (09)
in Peanuts (groundnuts), Raw (affinity column).......................................................................................Ab 7 –91 (09)
in Peanuts (groundnuts), Raw, Roasted, Meal, Butter...............................................................................Ab 6 –68 (09)
Aflatoxins B1, B2, and G1 in Corn, Cottonseed, Peanuts, and Peanut Butter....................................................Aj 6 –95 (09)
Aflatoxins, Confirmation by TLC....................................................................................................................Aa 9 –86 (09)
Aflatoxin Standards (preparation).....................................................................................................................Aa 10 –88 (09)
Aflatoxin Detection by PHRED.......................................................................................................................Aa 11 –05 (09)
Alcohol-Insoluble Matter in Fatty Alkyl Sulfates..............................................................................................Dc 3b –59 (09)
Alcohol-Soluble and Alcohol–Insoluble Matter
in Soap and Soap Products........................................................................................................................Da 3 –48 (09)
in Soap Containing Synthetic Detergents..................................................................................................Db 2 –48 (09)
Alcohol-Soluble Matter in Fatty Alkyl Sulfates.................................................................................................Dc 3a –59 (09)
Alkaline Silicates
in Soap and Soap Products........................................................................................................................Da 18 –48 (09)
in Soap Containing Synthetic Detergents..................................................................................................Db 9 –48 (09)
Alkalinity
of Fats and Oils.........................................................................................................................................Cd 3e –02 (09)
of Fatty Alkyl Sulfates...............................................................................................................................Dc 6 –59 (09)
of Glycerin................................................................................................................................................Ea 2 –38 (73) *
of Sulfonated and Sulfated Oils.................................................................................................................F 7 –44 (09)
Alkalinity of Alcohol–Insoluble Matter
in Soda Soap and Products........................................................................................................................Da 7 –48 (09)
in Soda Soap and Products Containing Synthetic Detergents....................................................................Db 5 –48 (09)

*Surplus method Page 1 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
Amines, Tests
for Fatty Quaternary Ammonium Chlorides.............................................................................................Te 3a –64 (09)
for Primary Amines, by Gas Chromatography...........................................................................................Tf 4a –77 (09)
for Primary, Secondary, and Tertiary Amines, Percent in Fatty Acids.......................................................Tf 3a –64 (09)
Amine Value
Fatty Quaternary Ammonium Chlorides..................................................................................................Te 3a –64 (09)
Primary, Secondary, and Tertiary Indicator Fatty Amines.........................................................................Tf 2b –64 (09)
Primary, Secondary, and Tertiary Potentiometric Fatty Amines................................................................Tf 2a –64 (09)
Total Indicator Fatty Amines....................................................................................................................Tf 1b –64 (09)
Total Potentiometric Fatty Amines...........................................................................................................Tf 1a –64 (09)
Ammonia (total) in Sulfonated and Sulfated Oils.............................................................................................F 8 –44 (09)
Analytical Guidelines for Testing
of Commercial Fatty Acids........................................................................................................................S 1 –64 (09)
of Drying Oils...........................................................................................................................................S 2 –64 (09)
of Epoxidized Oils....................................................................................................................................S 3 –64 (09)
of Fatty Amidoamines...............................................................................................................................S 4b –64 (09)
of Fatty Amines.........................................................................................................................................S 4a –64 (09)
of Fatty Diamines.....................................................................................................................................S 4d –64 (09)
of Fatty Quaternary Ammonium Chlorides..............................................................................................S 4c –64 (09)
for Feed–Grade Fat Products....................................................................................................................Cf 1 –68 (09)
of Polymerized Fatty Acids........................................................................................................................S 5 –64 (09)
Anhydrous Soap (total)....................................................................................................................................Db 6 –48 (09)
Anhydrous Soap and Combined Alkali (total)..................................................................................................Da 8 –48 (09)
Anisidine Value................................................................................................................................................Cd 18 –90 (09)
Antioxidant Analysis........................................................................................................................................Cg 7 –05 (09)
Antioxidants in Oils by HPLC.........................................................................................................................Ce 6 –86 (09)
AOCS & ASTM Methods for Soaps and Detergent Analysis...........................................................................D 1 –99 (09)
Approved Chemists (Criteria)..........................................................................................................................M 5 –09 (09)
Ash
in Drying Oils...........................................................................................................................................Tm 1a –64 (09)
in Fats and Oils.........................................................................................................................................Ca 11 –55 (09)
in Fatty Acids............................................................................................................................................Tm 1a –64 (09)
in Fatty Quaternary Ammonium Chlorides..............................................................................................Tm 2a –64 (09)
in Glycerin................................................................................................................................................Ea 2 –38 (73) *
in Oilseed Cake and Meals........................................................................................................................Ba 5a –49 (09)
in Oilseed Meal, Acid–Insoluble...............................................................................................................Ba 5b –68 (09)
in Soya Flours/Canola Flours....................................................................................................................Bc 5 –49 (09)
Beilstein Test....................................................................................................................................................Ca 7 –35 (90) *
Benzo(a)pyrene in Edible Oils and Fats............................................................................................................Cd 21 –91 (09)
Biodiesel Feedstocks.........................................................................................................................................Ck 1 –07 (09)
Bleaching Test
for Cottonseed Oil (refined)......................................................................................................................Cc 8a –52 (09)
for Evaluation of Clays and Absorbents.....................................................................................................Cc 8f –91 (09)
for Soybean Oil (refined)..........................................................................................................................Cc 8b –52 (09)
for Soybean Oil (modified test).................................................................................................................Cc 8e –63 (09)
for Sunflower Oil (refined)........................................................................................................................Cc 8b –52 (09)
Boemer Number for Detection of Foreign Fats in Pork Fat..............................................................................Cb 5 –40 (93) *
Borax in Soap and Soap Products.....................................................................................................................Da 17 –52 (09)
Break Test (crude soybean oil).........................................................................................................................Ca 10 –40 (89) *
Butyric Acid.....................................................................................................................................................Ca 5c –87 (09)
Butyric Acid (Kirschner value) in Butterfat and Coconut Oils..........................................................................Cd 5 –40 (09)
Cadmium by AAS with Graphite Furnace........................................................................................................Ca 18d–01 (09)
Carbonates
by Gravimetric Absorption Method..........................................................................................................Da 19a–42 (09)
by Volumetric Evolution Method.............................................................................................................Da 19b–42 (09)
b-Carotene in Margarines................................................................................................................................Ce 9 –01 (09)
Cellulose Yield.................................................................................................................................................Bb 3 –47 (09)
Certified Laboratories (Criteria).......................................................................................................................M 6 –09 (09)

*Surplus method Page 2 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
Chlorides
in Glycerin (crude)....................................................................................................................................Ea 2 –38 (73) *
in Soap and Soap Products........................................................................................................................Da 9 –48 (09)
in Soap and Soap Products Containing Synthetic Detergents
Indicator Method......................................................................................................................................Db 7 –48 (09)
Potentiometric Method.............................................................................................................................Db 7b –55 (09)
Chlorinated Solvents (Beilstein Test)...............................................................................................................Ca 7 –35 (90) *
Chlorophyll Pigments (rapeseed)......................................................................................................................Ak 2 –92 (09)
Chlorophyll Pigments (refined and bleached oils)............................................................................................Cc 13d–55 (09)
Chlorophyll Pigments (crude vegetable oils).....................................................................................................Cc 13i –96  (09)
Chromium, Trace Amounts
by AAS......................................................................................................................................................Ca 15 –75 (09)
by AAS with Graphite Furnace.................................................................................................................Ca 18 –79 (09)
cis, cis and trans Isomers, Fatty Acid Composition by GLC..............................................................................Ce 1c –89 (95) *
cis, cis Polyunsaturated Fatty Acids...................................................................................................................Cd 15 –78 (09)
Cloud Point Test.............................................................................................................................................Cc 6 –25 (09)
Cocoa Butter Equivalents.................................................................................................................................Ce 11 –05 (09)
Cocoa Butter Equivalents in Milk Chocolate by GC........................................................................................Ce 11a –07 (09)
Cold Test.........................................................................................................................................................Cc 11 –53 (09)
Collaborative Study Procedures........................................................................................................................M 4 –86 (09)
Color Measurement
by APHA Scale for Glycerin......................................................................................................................Ea 9 –65 (09)
by Color Stability for Fatty Acids (after heating).......................................................................................Td 3a –64 (09)
by Combined Alcohols in Fatty Alkyl Sulfates..........................................................................................Dc 5 –59 (09)
by Combined Alkali in Soap and Soap Products.......................................................................................Da 8 –48 (09)
by Combined Sodium and Potassium Oxides in Soap and Soap Products.................................................Da 27 –48 (09)
by FAC Method........................................................................................................................................Cc 13a –43 (09)
by Fatty Acids (commercial)......................................................................................................................Td 2a –64 (09)
by Gardner for Industrial Oils...................................................................................................................Td 1a –64 (09)
Color (Automated Method)......................................................................................................................Cc 13j –97 (09)
by Gardner for Lecithin............................................................................................................................Ja 9 –87 (09)
by Linear Alkylbenzene Sulfonates (LAS)..................................................................................................Dd 5 –92 (09)
by Lovibond (per ISO Standard)...............................................................................................................Cc 13e –92 (09)
by Lovibond (Wesson)..............................................................................................................................Cc 13b–45 (09)
by Platinum–Cobalt Scale for Light-Colored Liquids................................................................................Td 1b –64 (09)
by Spectrophotometric Color Method for Oils.........................................................................................Cc 13c –50 (09)
by Wesson (Lovibond)..............................................................................................................................Cc 13b–45 (09)
Composition of Dibasic Acids by GLC............................................................................................................Ty 1a –76 (09)
Composition of Fatty Acids by GLC................................................................................................................Ce 1 –62 (09)
Composition of Primary Amines by GLC........................................................................................................Tf 4a –77 (09)
Congeal Point..................................................................................................................................................Cc 14 –59 (09)
Conjugated Dienoic Acid in Castor Oil and Acids...........................................................................................Ti 1a –64 (09)
Consistency, Penetration Method....................................................................................................................Cc 16 –60 (09)
Copper
in Oils by AAS..........................................................................................................................................Ca 15 –75 (09)
in Oils by AAS with Graphite Furnace......................................................................................................Ca 18 –79 (09)
in Soap and Soap Products........................................................................................................................Da 31 –58 (09)
Cottonseed Oil, Detection in Oils by Halphen Test........................................................................................Cb 1 –25 (09)
Crismer Test....................................................................................................................................................Cb 4 –35 (09)
Crude Fatty Acids (total fatty acids plus unsaponifiables).................................................................................Ca 5b –71 (09)
Crude Fiber
in Grains, Meals, Flours, Feeds, and All Fiber–Bearing Materials
Extraction by Filter Bag Technology..................................................................................................Ba 6a –05 (09)
from Which Fat Can Be Extracted.....................................................................................................Ba 6 –84 (09)
in Soya Flours...........................................................................................................................................Bc 6 –49 (09)
Desiccants, Specifications.................................................................................................................................H 9 –87 (09)
Desulfated Fatty Matter, Total.........................................................................................................................F 3 –44 (09)
Dicarboxylic Acid, Composition by GLC........................................................................................................Ty 1a –76 (09)

*Surplus method Page 3 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
Diene Value of Drying Oils.............................................................................................................................Th 1a –64 (09)
Dienoic Acids in Dehydrated Castor Oil and Acids..........................................................................................Ti 1a –64 (09)
Dilatometric Method for Solid Fat Index.........................................................................................................Cd 10 –57 (97) *
Dimer Acids, Composition by HPLC..............................................................................................................Tf 5 –91 (09)
Dimethylpolysiloxanes in Fats and Oils............................................................................................................Cd 24 –95 (09)
DowthermTM (heat transfer fluid in fats and oils) by GLC...............................................................................Cd 25 –96 (09)
DowthermTM (heat transfer fluid in fats and oils) by HPLC.............................................................................Cd 25a–00 (09)
Dropping Point................................................................................................................................................Cc 18 –80 (09)
DSC Melting Properties of Fats and Oils.........................................................................................................Cj 1 –94 (09)
Epoxidized Fatty Materials...............................................................................................................................Cd 9 –57 (09)
Erucic Acid in High Erucic Acid Oils and Fats by Packed Column Gas–Liquid Chromatography...................Ce 4 –95 (97) *
Erucic Acid in Oils and Fats.............................................................................................................................Ce 4 –86 (95) *
Essential Fatty Acids.........................................................................................................................................Cd 15 –78 (09)
Ester SO3 in Fatty Alkyl Sulfates .....................................................................................................................Dc 4 –59 (09)
Fat Stability, Active Oxygen Method (AOM)...................................................................................................Cd 12 –57 (93) *
Fat Stability, Oil Stability Index (OSI).............................................................................................................Cd 12b–92 (09)
Fatty Acids
by Capillary GLC.....................................................................................................................................Ce 1e –91 (01) *
cis, cis and trans Isomers by GLC...............................................................................................................Ce 1c –89 (95) *
Combined as Mineral Soaps in Fats..........................................................................................................Ca 4 –25 (09)
Composition by GLC of Methyl Esters.....................................................................................................Ce 1 –62 (09)
Composition by Capillary GC for Nutritional Labeling............................................................................Ce 1h –05 (09)
in Marine and Other Oils Containing Long Chain PUFAs by GC...........................................................Ce 1i –07 (09)
Composition of Marine Oils.....................................................................................................................Ce 1b –89 (09)
Extracted Fats by GC................................................................................................................................Ce 1j –07 (09)
Crude (total fatty acids plus unsaponifiables)............................................................................................Ca 5b –71 (09)
Direct Methylation of Lipids in Complex Matrices...................................................................................Ce 1k –07 (09)
n-3 and n-6 by Capillary GLC..................................................................................................................Ce 1d –91 (93) *
Oxidized in Soap Stocks............................................................................................................................G 3 –53 (09)
Separation of Liquid and Solid..................................................................................................................Cd 6 –38 (89) *
Total in Coconut and Similar Soap Stock.................................................................................................G 4 –40 (09)
Total in Fats or Hydrolyzed Fats...............................................................................................................Ca 5b –71 (09)
Total in Soap Stocks Other Than Coconut...............................................................................................G 3 –53 (09)
trans Composition of Partially Hydrogenated Oils by GLC–IR................................................................Cd 14b–93 (95) *
trans Fatty Acids in Oils and Fats by Capillary GLC.................................................................................Ce 1f –96 (09) *
trans Fatty Acids (isolated) by FTIR..........................................................................................................Cd 14 –95 (09)
trans Fatty Acids by Silver–Ion Exchange HPLC.......................................................................................Ce 1g –96 (09)
Fatty Matter in Soaps.......................................................................................................................................Db 10 –48 (09)
Fiber (crude)
in Grains, Meals, Flours, Feeds.................................................................................................................Ba 6 –84 (09)
Extraction by Filter Bag Technology.........................................................................................................Ba 6a –05 (09)
in Soya Flours...........................................................................................................................................Bc 6 –49 (09)
Fitelson Test for Teaseed Oil...........................................................................................................................Cb 3 –39 (09)
Flash Point
Cleveland Open Cup Method
for Fats and Oils................................................................................................................................Cc 9a –48 (09)
for Fatty Acids and Drying Oils.........................................................................................................Tn 1a –64 (09)
Pensky–Martens Closed Cup Method
for Fats and Oils................................................................................................................................Cc 9b –55 (09)
for Fatty Quaternary Ammonium Chlorides......................................................................................Tn 2a –86 (09)
Flashpoint by Pensky–Martens Closed Cup Flash Tester.................................................................................Cc 9c –95 (09)
Flavor
Correlation of Volatiles with Flavor..........................................................................................................Cg 1 –83 (09)
Panel Evaluation of Vegetable Oils............................................................................................................Cg 2 –83 (09)
Flow Test.........................................................................................................................................................Cc 5 –25 (89) *
Foots (Visible) in Fats and Oils........................................................................................................................Ca 3e –02 (09)
Foreign Fats in Pork Fat and Lard....................................................................................................................Cb 5 –40 (93) *
Foreign Matter in Cottonseed..........................................................................................................................Aa 2 –38 (09)
Free Acid or Free Alkali

*Surplus method Page 4 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
in Soda Soap.............................................................................................................................................Da 4a –48 (09)
in Soda Soap Containing Synthetic Detergent..........................................................................................Db 3 –48 (09)
Free Fatty Acids
in Castor Beans.........................................................................................................................................Ae 4 –52 (09)
in Cottonseed...........................................................................................................................................Aa 6 –38 (09)
in Crude and Refined Fats and Oils..........................................................................................................Ca 5a –40 (09)
in Crude Vegetable Oils by GC................................................................................................................Ca 5d –01 (09)
in Peanuts (groundnuts)............................................................................................................................Ab 5 –49 (09)
in Soybeans...............................................................................................................................................Ac 5 –41 (09)
Fumonisins B1 and B2 in Corn by LC .............................................................................................................Aj 5 –93 (09)
in Corn by LC..........................................................................................................................................Aj 5a –97 (09)
Glucosinolates (rapeseed).................................................................................................................................Ak 1 –92 (09)
Glycerin, Total and Organic Residue...............................................................................................................Ea 3 –58 (73) *
Glycerine, Free, by HPLC/ELSD.....................................................................................................................Ca 14b –96 (09)
Glycerol by Periodate Method
in Fats and Oils.........................................................................................................................................Ca 14 –56 (09)
in Glycerin................................................................................................................................................Ea 6 –94 (09)
in Soap and Soap Products (free)..............................................................................................................Da 23 –56 (09)
Gossypol, Free in Cottonseed Products............................................................................................................Ba 7 –58 (09)
Gossypol, Free, Rapid Method.........................................................................................................................Ba 7b –96 (09)
Gossypol by HPLC..........................................................................................................................................Ba 8a –99 (09)
Gossypol, Total
in Cottonseed Products.............................................................................................................................Ba 8 –78 (09)
in Crude Cottonseed Oil and Soap Stock..................................................................................................Ca 13 –56 (09)
Halphen Test for Detecting Cottonseed Oil.....................................................................................................Cb 1 –25 (09)
Heat Transfer Fluids
by GLC.....................................................................................................................................................Cd 25 –96 (09)
by HPLC..................................................................................................................................................Cd 25a–07  (09)
Thermal Heating Fluids in Vegetable Oils by GC.....................................................................................Cd 25b–07 (09)
Hexane
Commercial, Specifications.......................................................................................................................H 16 –56 (09)
Free in Extracted Meals.............................................................................................................................Ba 13 –87 (09)
Insolubles in Lecithin................................................................................................................................Ja 3 –87 (09)
Residues in Fats and Oils..........................................................................................................................Ca 3b –87 (09)
Total in Extracted Meals...........................................................................................................................Ba 14 –87 (09)
Hydrocarbons
Mineral Oil in Triglycerides......................................................................................................................Ca 6c –65 (09)
Volatile in Soap and Soap Products...........................................................................................................Da 26 –42 (09)
Steroidal Hydrocarbons in Vegetable Oils.................................................................................................Cd 27 –96 (09)
Hydrogenation Catalyst
Activity.....................................................................................................................................................Tz 1a –78 (09)
Selectivity..................................................................................................................................................Tz 1b –79 (09)
Hydroxyl Value
of Epoxidized Oils....................................................................................................................................Tx 1a –66 (09)
of Fats and Oils (acetyl value)...................................................................................................................Cd 4 –40 (99)*
of Fatty Oils and Alcohols.........................................................................................................................Cd 13 –60 (09)
Impurities in Oilseeds......................................................................................................................................Am 4 –02 (09)
Inorganic Salts..................................................................................................................................................F 6 –44 (09)
Insoluble Impurities
in Fats and Oils.........................................................................................................................................Ca 3a –46 (09)
in Lecithin (hexane insolubles)..................................................................................................................Ja 3 –87 (09)
International Trade Methods...........................................................................................................................Front Matter
Iodine Value
by NIR.....................................................................................................................................................Cd 1e –01 (09)
Calculated from GLC...............................................................................................................................Cd 1c –85 (09)
Cyclohexane Method................................................................................................................................Cd 1b –87 (09)
Cyclohexane-Acetic Acid Method.............................................................................................................Cd 1d –92 (09)
of Drying Oils...........................................................................................................................................Tg 1 –64 (09)

*Surplus method Page 5 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
of Fats and Oils.........................................................................................................................................Cd 1 –25 (93) *
of Fatty Acids............................................................................................................................................Tg 1a –64 (09)
of Fatty Amines, Diamines, and Amidoamines.........................................................................................Tg 2a –64 (09)
of Fatty Quaternary Ammonium Chlorides..............................................................................................Tg 3a –64 (09)
of Lecithin................................................................................................................................................Ja 14 –91 (09)
of Soap and Soap Products........................................................................................................................Da 15 –48 (09)
Iron, Trace Amounts in Oils
by AAS......................................................................................................................................................Ca 15 –75 (09)
by AAS with Graphite Furnace.................................................................................................................Ca 18 –79 (09)
Isopropyl Alcohol, Specifications......................................................................................................................H 18 –58 (09)
Jojoba Oil
Acid Value................................................................................................................................................Ci 4 –91 (09)
Detection of Triglyceride Adulteration.....................................................................................................Ci 2 –91 (09)
Methods for Determination of Quality and Purity....................................................................................Ci 1 –91 (09)
Kernel Content of Tung Fruit..........................................................................................................................Ad 4 –52 (09)
Kirschner Value for Butyric Acid in Butterfat and Coconut Oils......................................................................Cd 5 –40 (09)
Lard, Foreign Fat Content...............................................................................................................................Cb 5 –40 (93) *
Lead in Oils by Graphite Furnace....................................................................................................................Ca 18c –91 (09)
Lecithin Co–Products Analyses........................................................................................................................Ja 12 –89 (09)
Lecithin Phospholipids by HPLC–LSD...........................................................................................................Ja 7c –07 (09)
Lint Residue in Cottonseed..............................................................................................................................Aa 7 –55 (09)
Liquid Fatty Acids in Fats and Oils..................................................................................................................Cd 6 –38 (89) *
Manganese in Oils by Graphite Furnace...........................................................................................................Ca 18 –79 (09)
Mass per Unit Volume (“Liter Weight”) in Air of Oils and Fats.......................................................................Cc 10c –95 (09)
Melting Point
Capillary Tube Method............................................................................................................................Cc 1 –25 (09)
Mettler Dropping Point............................................................................................................................Cc 18 –80 (09)
Slip Melting Point, AOCS Standard.........................................................................................................Cc 3 –25 (09)
Slip Melting Point, ISO Standard.............................................................................................................Cc 3b –92 (09)
Wiley Method...........................................................................................................................................Cc 2 –38 (91) *
Melting Properties of Fats and Oils by DSC....................................................................................................Cj 1 –94 (09)
Metals, Trace
by AAS for Cr, Cu, Fe, Ni in Oils.............................................................................................................Ca 15 –75 (09)
by AAS with Graphite Furnace for Cr, Cu, Fe, Ni, Mn in Oils.................................................................Ca 18 –79 (09)
by ICP-OES.............................................................................................................................................Ca 17 –01 (09)
by Spectrophotometry for Copper.............................................................................................................Da 31 –58 (09)
Methyl Alcohol, Specifications.........................................................................................................................H 17 –58 (09)
Methyl Esters Preparation................................................................................................................................Ce 2 –66 (09)
Mineral Oil in Triglycerides.............................................................................................................................Ca 6c –65 (09)
Miscibility of Oils, Crismer Test......................................................................................................................Cb 4 –35 (09)
Moisture and Volatile Matter, by Air Oven
in Castor Beans.........................................................................................................................................Ae 2 –52 (09)
in Castor Pomace......................................................................................................................................Bd 2 –52 (09)
in Cottonseed...........................................................................................................................................Aa 3 –38 (09)
in Fats and Oils (except coconut and drying oils)......................................................................................Ca 2c –25 (09)
in Flaxseed................................................................................................................................................Af 2 –54 (97) *
in Oilseed Meats, Meal, Cake, and Pellets.................................................................................................Ba 2a –38 (09)
in Oilseed Protein Concentrates................................................................................................................Ba 2b –82 (09)
in Peanuts (groundnuts)............................................................................................................................Ab 2 –49 (09)
in Soap and Soap Products........................................................................................................................Da 2a –48 (09)
in Soap and Soap Products Containing Synthetic Detergents....................................................................Db 1 –48 (09)
in Soya Flours...........................................................................................................................................Bc 2 –49 (09)
in Soybeans...............................................................................................................................................Ac 2 –41 (09)
in Sunflower Seed.....................................................................................................................................Ai 2 –75 (09)
in Tung Fruit (hulls and fruit plus hulls)...................................................................................................Ad 2 –52 (09)
Moisture and Volatile Matter, by Forced Draft Oven
in Oilseed Cake, Meal, Meats, Pellets........................................................................................................Ba 2a –38 (09)
Moisture and Volatile Matter, by Hot Plate Method
Butter, Fats, Margarines, Oils...................................................................................................................Ca 2b –38 (09)

*Surplus method Page 6 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
Fatty Acids................................................................................................................................................Tb 1a –64 (09)
Modified Moisture and Volatiles...............................................................................................................Ca 2f –93 (09)
Moisture and Volatile Matter, by Vacuum Oven
in Fats and Oils (except coconut)..............................................................................................................Ca 2d –25 (09)
in Oilseed Cake, Meal, Meats, Pellets........................................................................................................Ba 2b –82 (09)
Moisture, by Distillation Method
in Alkylbenzene Sulfonate Products..........................................................................................................Dd 2a –59 (09)
in Fats and Oils.........................................................................................................................................Ca 2a –45 (09)
in Fatty Alkyl Sulfate Products..................................................................................................................Dc 2 –59 (09)
in Lecithin................................................................................................................................................Ja 2a –46 (09)
in Soap and Soap Products . .....................................................................................................................Da 2b –42 (09)
in Sulfonated and Sulfated Oils.................................................................................................................F 1a –44 (09)
Moisture, by Karl Fischer Method
in Alkylbenzene Sulfonate Products..........................................................................................................Dd 2b –59 (89) *
in Fats and Oils.........................................................................................................................................Ca 2e –84 (09)
in Fatty Nitrogen Compounds..................................................................................................................Tb 2a –64 (89) *
in Glycerin................................................................................................................................................Ea 8 –58 (09)
in Industrial Oils and Derivatives..............................................................................................................Tb 2 –64 (97) *
in Lecithin................................................................................................................................................Ja 2b –87 (09)
Molecular Weight (average) of Fatty Quaternary Ammonium Chlorides.........................................................Tv 1a –64 (09)
Mono- and Diglycerides by Capillary GLC......................................................................................................Cd 11b–91 (09)
Mono- and Diglycerides by HPLC–ELSD.......................................................................................................Cd 11d –96 (09)
Mono-, Di-, and Triglycerides by Silica Gel Chromatography.........................................................................Cd 11c –93 (09)
a-Monoglycerides............................................................................................................................................Cd 11 –57 (09)
Near Infrared Reflectance.................................................................................................................................Am 1 –92 (09)
Neutral Oil
in Alkylbenzene Sulfonates (unsulfonated material)..................................................................................Dd 4 –60 (09)
in Neutral Oil and Loss for Fats and Oils..................................................................................................Ca 9f –57 (09)
in Soap Stock (unsaponifiable material)....................................................................................................G 5 –40 (09)
Nitrogen–Ammonia–Protein
Conversion Table......................................................................................................................................Aa 5 –91 (09)
Copper Sulfate Catalyst.............................................................................................................................Ba 4b –87 (90) *
Copper Sulfate Plus Titanium Dioxide Catalyst........................................................................................Ba 4d –90 (09)
in Cottonseed...........................................................................................................................................Aa 5 –38 (89) *
in Cottonseed...........................................................................................................................................Aa 5 –91 (09)
in Oilseeds, Meats, Meal, Cake, and Pellets..............................................................................................Ba 4a –38 (89) *
in Peanuts (groundnuts)............................................................................................................................Ab 4 –50 (89) *
in Peanuts (groundnuts)............................................................................................................................Ab 4 –91 (09)
in Soya Flours...........................................................................................................................................Bc 4 –49 (89) *
in Soya Flours...........................................................................................................................................Bc 4 –91 (09)
in Soybeans...............................................................................................................................................Ac 4 –41 (89) *
in Soybeans...............................................................................................................................................Ac 4 –91 (09)
in Sunflower Seeds....................................................................................................................................Ai 4 –75 (89) *
in Sunflower Seeds....................................................................................................................................Ai 4 –91 (09)
Kjel-Foss Automatic..................................................................................................................................Ba 4c –87 (89) *
Nitrogen Solubility Index (soybean products)...........................................................................................Ba 11 –65 (09)
Nonamines in Fatty Amines and Diamines......................................................................................................Tw 1a –64 (09)
Non-Cocoa-Butter Fats....................................................................................................................................Ce 10 –02 (09)
Nonvolatiles (solids), by Hot Plate Method
for Drying Oils (solutions)........................................................................................................................Tc 1a –64 (09)
for Quaternary Ammonium Chlorides......................................................................................................Tc 2a –64 (09)
Oil Content
by Filter Bag Technology .........................................................................................................................Am 5 –04 (09)
in Castor Beans.........................................................................................................................................Ae 3 –52 (09)
in Castor Pomace...................................................................................................................................... Bd 3 –52 (09)
in Corn Germ...........................................................................................................................................Aj 4 –89 (09)
in Cottonseed...........................................................................................................................................Aa 4 –38 (09)
in Flaxseed................................................................................................................................................Af 3 –54 (95) *
in Linters (cottonseed hulls)......................................................................................................................Bb 2 –38 (09)

*Surplus method Page 7 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
in Oilseed Meats, Cake, and Meal.............................................................................................................Ba 3 –38 (09)
in Oilseed Residues by NMR....................................................................................................................Ak 5 –01 (09)
in Oilseeds (FOSFA Method)...................................................................................................................Am 2 –93 (09)
in Oilseeds: Supercritical Fluid Extraction Method...................................................................................Am 3 –96 (09)
in Peanuts (groundnuts), Raw or Roasted.................................................................................................Ab 3 –49 (09)
in Rapeseed and other Oilseeds by NMR..................................................................................................Ak 3 –94 (09)
in Safflower Seed.......................................................................................................................................Ag 1 –65 (09)
in Soya Flours...........................................................................................................................................Bc 3 –49 (09)
in Soybeans...............................................................................................................................................Ac 3 –44 (09)
in Sunflower Seed or Dehulled Kernels.....................................................................................................Ai 3 –75 (99) *
in Tung Fruit, Hulled...............................................................................................................................Ad 6 –52 (09)
in Tung Fruit, Kernels..............................................................................................................................Ad 5 –52 (09)
in Tung Fruit, Whole...............................................................................................................................Ad 3 –52 (09)
Olive Oil
Chlorophyll Pigments...............................................................................................................................Ch 4 –91 (09)
Fatty Acids by Capillary GLC...................................................................................................................Ch 2 –91 (09)
trans Unsaturated Fatty Acids by Capillary Column GC...........................................................................Ch 2a –94 (09)
Fatty Acids in 2-Position...........................................................................................................................Ch 3 –91 (09)
Preparation of Methyl Esters.....................................................................................................................Ch 1 –91 (09)
Specific Extinction....................................................................................................................................Ch 5 –91 (09)
Sterol Fraction by TLC and Capillary GLC..............................................................................................Ch 6 –91 (09)
International Trade Standards...................................................................................................................Ch 7 –09 (09)
Wax Content............................................................................................................................................Ch 8 –02 (09)
Organic Residue in Glycerin............................................................................................................................Ea 3 –58 (73) *
Ovens
Air, Specifications.....................................................................................................................................H 3 –45 (09)
Forced Draft, Specifications......................................................................................................................H 1 –39 (09)
Vacuum, Specifications.............................................................................................................................H 4 –45 (09)
Oxidized Fatty Acids in Soap Stocks................................................................................................................G 3 –53 (09)
Oxirane Oxygen in Epoxidized Materials.........................................................................................................Cd 9 –57 (09)
Peroxide Value
of Lecithin................................................................................................................................................Ja 8 –87 (09)
Using Chloroform....................................................................................................................................Cd 8 –53 (03) *
Using Isooctane........................................................................................................................................Cd 8b –90 (09)
Pesticides in Oils and Fats................................................................................................................................Cd 23 –93 (09)
Petroleum Ether, Specifications........................................................................................................................H 2 –41 (09)
pH
of Acidulated Soapstocks...........................................................................................................................G 7 –56 (09)
of Fatty Quaternary Ammonium Chlorides..............................................................................................Tu 1a –64 (09)
Phosphates in Soap and Soap Products (gravimetric method)...........................................................................Da 20a –48 (09)
Phosphates in Soap and Soap Products (titrimetric method)............................................................................Da 20b –57 (09)
Phospholipids
in Lecithin Concentrates by HPLC...........................................................................................................Ja 7b –91 (09)
in Lecithin Phospholipids by HPLC-LSD.................................................................................................Ja 7c –07 (09)
in Lecithin Concentrates by TLC..............................................................................................................Ja 7 –86 (09)
in Vegetable Oil........................................................................................................................................Ca 19 –86 (09)
Phosphorus, Atomic Absorption Spectroscopy.................................................................................................Ca 12b –92 (09)
Phosphorus
in Lecithin (total)......................................................................................................................................Ja 5 –55 (89) *
in Oils.......................................................................................................................................................Ca 12 –55 (09)
in Oils (ISO Method)...............................................................................................................................Ca 12a –02 (09)
in Oil by ICP-OES...................................................................................................................................Ca 20 –99 (09)
Photometric Index (color) of Commercial Fatty Acids.....................................................................................Td 2a –64 (09)
Physical Analysis
Polenske Value..........................................................................................................................................Cd 5 –40 (09)
Tung Fruit (kernel content)......................................................................................................................Ad 4 –52 (09)
Polar Compounds in Frying Fats......................................................................................................................Cd 20 –91 (09)
Polyethylene in Fats and Oils...........................................................................................................................Ca 16 –75 (09)

*Surplus method Page 8 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
Polymerized Triglycerides by Gel-Permeation HPLC.......................................................................................Cd 22 –91 (09)
Polyunsaturated Acids
cis, cis Essential Fatty Acids (enzymatic)....................................................................................................Cd 15 –78 (09)
Commercial Fatty Acids, Spectrophotometric Method.............................................................................Tj 1a –64 (93) *
in Fats and Oils.........................................................................................................................................Cd 7 –58 (09)
Potassium Carbonate in Potash Soaps..............................................................................................................Da 5 –44 (09)
Potassium Oxide in Soap and Soap Products....................................................................................................Da 27 –48 (09)
Precision of Analytical Methods.......................................................................................................................M 1 –92 (09)
Protein Content
by Combustion.........................................................................................................................................Ba 4e –93 (09)
by Combustion (soybean meal analysis)....................................................................................................Ba 4f –00 (09)
Conversion Table......................................................................................................................................Aa 5 –91 (09)
in Cottonseed...........................................................................................................................................Aa 5 –91 (09)
in Oilseed Meats, Meal, Cake, and Pellets.................................................................................................Ba 4a –38 (89) *
in Peanuts (groundnuts)............................................................................................................................Ab 4 –91 (09)
in Soya Flours/Canola Flours....................................................................................................................Bc 4 –91 (09)
in Soybeans...............................................................................................................................................Ac 4 –91 (09)
Protein Dispersibility Index (PDI) (soybean products)..............................................................................Ba 10 –65 (09)
Protein Dispersibility Index (PDI) (revised)..............................................................................................Ba 10a –05 (09)
Protein Dispersibility Index (PDI) (Omni Mixer).....................................................................................Ba 10b –09 (09)
in Sunflower Seeds....................................................................................................................................Ai 4 –91 (09)
Kjel–Foss Automatic Method....................................................................................................................Ba 4c –87 (89) *
with Copper Sulfate Catalyst.....................................................................................................................Ba 4b –87 (90) *
with Copper Sulfate Plus Titanium Dioxide Catalyst................................................................................Ba 4d –90 (09)
Refined and Bleached Color (tallow and greases for soaps)...............................................................................Cc 8d –55 (09)
Refining Loss
Degummed, Expeller Soybean Oil............................................................................................................Ca 9a –52 (09)
Degummed, Hydraulic and Extracted Soybean Oil...................................................................................Ca 9a –52 (09)
Extracted and Reconstituted Prepressed Cottonseed Oils..........................................................................Ca 9a –52 (09)
Extracted Soybean Oil..............................................................................................................................Ca 9a –52 (09)
Vegetable Oils, Crude...............................................................................................................................Ca 9a –52 (09)
Refractive Index
Drying Oils...............................................................................................................................................Tp 1a –64 (09)
Fats and Oils.............................................................................................................................................Cc 7 –25 (09)
Fatty Acids, Commercial...........................................................................................................................Tp 1a –64 (09)
Reichert–Meissl Value......................................................................................................................................Cd 5 –40 (09)
Residual Lint in Cottonseeds............................................................................................................................Aa 7 –55 (09)
Residue, Total and Organic, in Glycerin..........................................................................................................Ea 3 –58 (73) *
Rheological Instrument Calibration.................................................................................................................Cj 3 –99 (09)
Rosin
in Soap and Soap Products........................................................................................................................Da 12 –48 (09)
in Soap Containing Synthetic Detergents..................................................................................................Db 11 –48 (09)
Rosin Acids in Fatty Acids................................................................................................................................Ts 1a –64 (09)
Sampling
of Alkylbenzene Sulfonates........................................................................................................................Dd 1 –59 (09)
of Cottonseed...........................................................................................................................................Aa 1 –38 (09)
of Cottonseed Linters and Hull Fiber........................................................................................................Bb 1 –38 (09)
of Dibasic Acids........................................................................................................................................Ta 1e –70 (09)
of Epoxidized Oils....................................................................................................................................Ta 1 –09 (09)
of Fats and Oils.........................................................................................................................................C 1 –47 (09)
of Fatty Acids, Commercial.......................................................................................................................Ta 1 –09 (09)
of Fatty Alkyl Sulfates...............................................................................................................................Dc 1 –59 (09)
of Fatty Nitrogen Products.......................................................................................................................Ta 1 –09 (09)
of Flaxseed................................................................................................................................................Af 1 –54 (97) *
of Glycerin................................................................................................................................................Ea 1 –38 (09)
of Industrial Oils, General.........................................................................................................................Ta 1 –09 (09)
of Oilseed Slab, Cake, Pellets, Meals.........................................................................................................Ba 1 –38 (09)
of Peanuts (groundnuts), Whole, Shelled..................................................................................................Ab 1 –49 (09)

*Surplus method Page 9 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
of Polymerized Fatty Acids........................................................................................................................Ta 1 –09 (09)
of Soap and Soap Products........................................................................................................................Da 1 –45 (09)
of Soap Stock............................................................................................................................................G 1 –40 (09)
of Soya Flours...........................................................................................................................................Bc 1 –50 (09)
of Soybeans...............................................................................................................................................Ac 1 –45 (09)
of Sunflower Seed.....................................................................................................................................Ai 1 –80 (93) *
of Tung Fruit............................................................................................................................................Ad 1 –48 (09)
Saponification Color
Refined and Bleached................................................................................................................................Cc 13f –94 (09)
High Quality Tallow, Coconut Oils.........................................................................................................Cc 13g–94 (09)
Tallow, Coconut Oils...............................................................................................................................Cc 13h–94 (09)
Saponification Value
of Deodorizer Distillates and Sludges........................................................................................................Cd 3b –76 (09)
of Drying Oils...........................................................................................................................................Tl 1a –64 (09)
of Fats and Oils.........................................................................................................................................Cd 3 –25 (09)
of Fats and Oils (Calculated).....................................................................................................................Cd 3a –94 (09)
of Fats and Oils, Modified Using Methanol..............................................................................................Cd 3c –91 (09)
of Fatty Acids, Commercial.......................................................................................................................Tl 1a –64 (09)
of Soap and Soap Products........................................................................................................................Da 16 –48 (09)
of Soap Containing Synthetic Detergents..................................................................................................Db 8 –48 (09)
Screen Test
Soap Powders............................................................................................................................................Da 28 –39 (09)
Soya Flours...............................................................................................................................................Bc 7 –51 (09)
Sediment in Fats and Oils................................................................................................................................Ca 3d –02 (09)
Selectivity of Hydrogenation Catalysts.............................................................................................................Tz 1b –79 (09)
Sesame Oil Detection, Modified Villavecchia Test...........................................................................................Cb 2 –40 (09)
Simultaneous Determination of Oil and Moisture
Contents of Oilseeds Using Pulsed Nuclear Magnetic Resonance Spectroscopy........................................Ak 4 –95 (09)
Slip Melting Point, ISO Standard....................................................................................................................Cc 3b –92 (09)
Slip Point
Hard Fats (palm oil)..................................................................................................................................Cc 3 –25 (09)
Soft Fats....................................................................................................................................................Cc 4 –25 (89) *
Smoke, Flash, and Fire Point; Cleveland Open Cup Method...........................................................................Cc 9a –48 (09)
Soap in Oil
by Conductivity Method...........................................................................................................................Cc 15 –60 (89) *
by Titrimetric Method..............................................................................................................................Cc 17 –95 (09)
Sodium Alkylbenzene Sulfonate by Ultraviolet Absorption..............................................................................Dd 3 –60 (09)
Sodium and Calcium by AAS...........................................................................................................................Ca 15b –87 (09)
Sodium Chloride in Glycerin...........................................................................................................................Ea 2 –38 (73) *
Sodium Oxide in Soap and Soap Products.......................................................................................................Da 27 –48 (09)
Sodium Sulfate in Fatty Alkyl Sulfates..............................................................................................................Dc 7 –59 (09)
Softening Point (slip point of hard fats)...........................................................................................................Cc 3 –25 (09)
Solid Fat Content (SFC) by Magnetic Resonance (Direct Method).................................................................Cd 16b –93 (09)
Solid Fat Content (SFC) by Nuclear Magnetic Resonance (Indirect Method)..................................................Cd 16 –81 (09)
Solid Fat Index (SFI) of Fats and Oils..............................................................................................................Cd 10 –57 (95) *
Solid Fatty Acids in Fats and Oils....................................................................................................................Cd 6 –38 (89) *
Soluble Mineral Matter and Fatty Acids Combined as Mineral Soap................................................................Ca 4 –25 (09)
Specifications..................................................................................................................................................... See Section H
Specific Gravity
Drying Oils...............................................................................................................................................To 1b –64 (09)
Fatty Acids, Commercial...........................................................................................................................To 1a –64 (09)
Glycerin....................................................................................................................................................Ea 7 –95 (09)
Liquid Oils and Fats.................................................................................................................................Cc 10a –25 (95) *
Solid Fats and Waxes................................................................................................................................Cc 10b–25 (09)
Spreadability....................................................................................................................................................Cj 4 –00 (09)
Stability and Quality of Fats and Oils (Analytical Guidelines)..........................................................................Cg 3 –91 (09)
Light Exposure Test for Accelerated Aging of Oils....................................................................................Cg 6 –01 (09)
Oven Storage Test for Accelerated Aging of Oils.......................................................................................Cg 5 –97 (09)
Stability of Fats and Oils, Active Oxygen Method (AOM)...............................................................................Cd 12 –57 (93) *

*Surplus method Page 10 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
Standard Solutions
Alcoholic Potassium Hydroxide................................................................................................................H 15 –52 (09)
Hydrochloric Acid....................................................................................................................................H 14 –52 (09)
Sodium Hydroxide...................................................................................................................................H 12 –52 (09)
Sulfuric Acid.............................................................................................................................................H 13 –52 (09)
Starch in Soap and Soap Products....................................................................................................................Da 25 –48 (09)
Sterols in Soya Residues by GLC......................................................................................................................Ce 3 –74 (09)
Stigmastadienes in Vegetable Oils....................................................................................................................Cd 26 –96 (09)
Sugars in Soap and Soap Products....................................................................................................................Da 24 –48 (09)
Sulfates in Soap and Soap Products..................................................................................................................Da 22 –48 (09)
Sulfur in Olive Oil
by Coin Test.............................................................................................................................................Ca 8a –35 (90) *
by Silver Benzoate Test.............................................................................................................................Ca 8b –35 (90) *
Sulfuric Anhydride in Sulfonated and Sulfated Oils
by Ash Gravimetric Method......................................................................................................................F 2c –44 (09)
by Extraction Titration Method................................................................................................................F 2b –44 (09)
by Titration Method.................................................................................................................................F 2a –44 (09)
Surplus Status of Methods................................................................................................................................See Index
Teaseed Oil Detection, Fitelson Test...............................................................................................................Cb 3 –39 (09)
Tetrasodium Pyrophosphate.............................................................................................................................Da 21 –48 (09)
Thermometers, Specifications..........................................................................................................................H 5 –40 (09)
2-Thiobarbituric Acid (TBA) Value.................................................................................................................Cd 19 –90 (09)
Thiocyanogen Value........................................................................................................................................Cd 2 –38 (89) *
Titer Test
for Fats and Oils.......................................................................................................................................Cc 12 –59 (09)
for Fatty Acids, Commercial.....................................................................................................................Tr 1a –64 (09)
for Soap and Soap Products......................................................................................................................Da 13 –48 (09)
for Soap Stocks.........................................................................................................................................G 6 –40 (09)
Tocopherols
in Deodorizer Distillates, Total.................................................................................................................Ce 7 –87 (09)
in Lecithin Concentrates by HPLC...........................................................................................................Ja 13 –91 (09)
in Soya Sludge and Residues by GLC........................................................................................................Ce 3 –74 (09)
in Vegetable Oils and Fats by HPLC........................................................................................................Ce 8 –89 (09)
Toluene, Industrial, Specifications...................................................................................................................H 19 –58 (09)
Total Fatty Acids
in Coconut Oil and Palm Oil Soap Stock.................................................................................................G 4 –40 (09)
in Fats or Hydrolyzed Fats........................................................................................................................Ca 5b –71 (09)
in Soap Stocks Other Than Coconut Oil and Palm Oil............................................................................G 3 –53 (09)
Trace Metals in Oils
by AAS (Cr, Cu, Fe, Ni)...........................................................................................................................Ca 15 –75 (09)
by Graphite Furnace AAS (Cr, Cu, Fe, Ni, Mn).......................................................................................Ca 18 –79 (09)
by Graphite Furnace AAS Direct (Cu, Fe, Ni)..........................................................................................Ca 18b –91 (09)
by Graphite Furnace AAS (lead only)........................................................................................................Ca 18c –91 (09)
by ICP–OES.............................................................................................................................................Ca 17 –01 (09)
trans and cis,cis Isomers by GLC.......................................................................................................................Ce 1c –89 (95) *
trans Composition of Partially Hydrogenated Oils by GLC–IR.......................................................................Cd 14b–93 (95) *
trans Isomers (Isolated) by FTIR......................................................................................................................Cd 14 –95 (09)
trans Isomers by Capillary GLC.......................................................................................................................Cd 14c–94 (94) *
trans Isomers by Capillary GLC.......................................................................................................................Ch 2a –94 (09)
trans Isomers in Triglycerides by ATR/FTIR....................................................................................................Cd 14d –99 (09)
Triglycerides by GLC.......................................................................................................................................Ce 5 –86 (09)
Triglycerides by HPLC....................................................................................................................................Ce 5b –89 (09)
Triglycerides (Individual) by HPLC.................................................................................................................Ce 5c –93 (09)
Trypsin Inhibitor Activity in Soybean and Cotton/Soybean Dry Products.......................................................Ba 12 –75 (09)
Tung Fruit, Physical Analysis (kernel content).................................................................................................Ad 4 –52 (09)
Unsaponifiable Matter
in Drying Oils...........................................................................................................................................Tk 1a –64 (09)
in Fats and Oils, Except Marine Oils........................................................................................................Ca 6a –40 (09)
in Fats and Oils, Including Marine Oils....................................................................................................Ca 6b –53 (09)

*Surplus method Page 11 of 12

 ALPHABETICAL INDEX

Method Latest
number issue
in Fats or Hydrolyzed Fats........................................................................................................................Ca 5b –71 (09)
in Fatty Acids, Commercial.......................................................................................................................Tk 1a –64 (09)
in Fatty Acids, Polymerized.......................................................................................................................Tk 1a –64 (09)
in Soap and Soap Products........................................................................................................................Da 11 –42 (09)
Unsaponifiable Nonvolatile Matter in Sulfated Oils.........................................................................................F 5 –44 (09)
Unsaponified Plus Unsaponifiable Matter in Soap and Soap Products.............................................................Da 10 –42 (09)
Unsulfated Material in Fatty Alkyl Sulfates......................................................................................................Dc 8 –59 (09)
Urease Activity (soybean meals, flours, and mill feed).......................................................................................Ba 9 –58 (09)
Villavecchia Test for Sesame Oil, Modified......................................................................................................Cb 2 –40 (09)
Viscosity
Drying Oils, Bubble Time Method...........................................................................................................Tq 1a –64 (09)
Lecithin, Brookfield..................................................................................................................................Ja 10 –87 (09)
Lecithin, Bubble Time Method.................................................................................................................Ja 11 –87 (09)
Transparent Liquids, Bubble Time Method..............................................................................................Ja 11 –87 (09)
Volatile Hydrocarbons in Soap and Soap Products...........................................................................................Da 26 –42 (09)
Volatiles (VOC) in Fats and Oils by GLC........................................................................................................Cg 4 –94 (09)
Volatile Organic Contaminants by GC/MS.....................................................................................................Ca 3c –01 (09)
Water-Immiscible Organic Solvents in Sulfonated and Sulfated Oils...............................................................F 10 –44 (09)
Water-Insoluble Matter
in Soap and Soap Products........................................................................................................................Da 6 –48 (09)
in Soap Containing Synthetic Detergents..................................................................................................Db 4 –48 (09)
Wax Content...................................................................................................................................................Ch 8 –02 (09)
Wiley Melting Point Method...........................................................................................................................Cc 2 –38 (91) *
Writing and Approval of Methods...................................................................................................................M 2 –09 (09)
X-Ray Diffraction Analysis of Fats...................................................................................................................Cj 2 –95 (09)
Zearalenone and a-Zearalenol in Corn............................................................................................................Aj 2 –86 (09)

*Surplus method Page 12 of 12