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    Appendixes: Appendix Particle Size - 1 - A - Aluminum

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    The document contains appendices with the following information: 1) Particle size data for aluminum, copper, and magnesium powders. 2) XRD data including 2θ values, d-spacing, intensity ratios for the phases present in samples of aluminum, copper, magnesium, and aluminum alloys containing copper and magnesium. 3) AFM data including particle size distribution for nano alumina powder, mixed alloy+nano particle powders, and powders after corrosion. 4) Tafel test plots showing corrosion rates of aluminum alloys at different sintering temperatures and with different nano particle reinforcements.

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    Appendixes: Appendix Particle Size - 1 - A - Aluminum

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    The document contains appendices with the following information: 1) Particle size data for aluminum, copper, and magnesium powders. 2) XRD data including 2θ values, d-spacing, intensity ratios for the phases present in samples of aluminum, copper, magnesium, and aluminum alloys containing copper and magnesium. 3) AFM data including particle size distribution for nano alumina powder, mixed alloy+nano particle powders, and powders after corrosion. 4) Tafel test plots showing corrosion rates of aluminum alloys at different sintering temperatures and with different nano particle reinforcements.

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    The document contains appendices with the following information: 1) Particle size data for aluminum, copper, and magnesium powders. 2) XRD data including 2θ values, d-spacing, intensity ratios for the phases present in samples of aluminum, copper, magnesium, and aluminum alloys containing copper and magnesium. 3) AFM data including particle size distribution for nano alumina powder, mixed alloy+nano particle powders, and powders after corrosion. 4) Tafel test plots showing corrosion rates of aluminum alloys at different sintering temperatures and with different nano particle reinforcements.

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    © All Rights Reserved
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    Download as pdf or txt
    26 views19 pages

    Appendixes: Appendix Particle Size - 1 - A - Aluminum

    Uploaded by

    Ibrahim Header
    The document contains appendices with the following information: 1) Particle size data for aluminum, copper, and magnesium powders. 2) XRD data including 2θ values, d-spacing, intensity ratios for the phases present in samples of aluminum, copper, magnesium, and aluminum alloys containing copper and magnesium. 3) AFM data including particle size distribution for nano alumina powder, mixed alloy+nano particle powders, and powders after corrosion. 4) Tafel test plots showing corrosion rates of aluminum alloys at different sintering temperatures and with different nano particle reinforcements.

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    APPENDIXES

    Appendix particle size -1-

    -A- Aluminum
    APPENDIXES

    Appendix particle size -1-

    -B- Cupper
    APPENDIXES

    Appendix particle size -1-

    -C- Magnesium
    APPENDIXES
    Appendix XRD-2-

    -A- Aluminum

    *** Basic Data Process ***

    AL

    2 theta dm ds I/IO hkL

    38.80 2.319 2.338 100 (111)

    45.040 2.0111 2.024 47 (200)

    65.400 1.4258 1.431 22 (220)

    78.480 1.217 1.221 22 (311)

    Appendix XRD-2-

    -B- Cupper

    *** Basic Data Process ***

    Cu

    2 theta dm ds I/IO hkL

    43.44 2.0814 2.088 100 (111)

    50.580 1.803 1.808 42 (200)

    74.240 1.276 1.278 21 (220)

    90.020 1.0892 1.090 19 (311)

    95.200 1.0431 1.0436 9 (222)

    Appendix XRD-2-

    -C- Magnesium

    *** Basic Data Process ***

    Mg

    2 theta dm ds I/IO hkL

    36.80 2.4403 2.4519 100 (111)

    32.380 2.7626 2.7782 27 (100)

    47.980 1.8946 1.900 18 (102)

    63.200 1.470 1.4730 20 (103 )

    87.780 1.3638 1.366 20 (112)


    APPENDIXES

    Appendix XRD-3-

    Base alloy (compact 450Mpa and sintering temperature at 560C°)


    Group :( Al-4.5%Cu-1.5%Mg)

    AL 2 theta dm ds I/IO

    38.627 2.329 2.338 100

    44.895 2.0173 2.024 52

    65.255 1.4286 1.4310 28

    78.406 1.2186 1.2210 31

    Al2CuMg

    2 theta dm ds I/IO

    38.627 2.329 2.315 100

    65.255 1.4286 1.416 28

    82,6012 1.1671 1.184 8

    Mg2Cu6Al5

    2 theta dm ds I/IO

    44.895 2.0173 2.027 52

    82.6012 1.1671 1.167 8


    APPENDIXES

    Appendix XRD-4-Al2O3

    AL
    Al2CuMg

    2 theta dm ds I/IO

    68 1.391 1.377 100

    57.5 1.602 1.60 10

    52.5 1.701 1.742 5

    43.5 2.019 2.0782 5

    35 2.596 2.566 80
    APPENDIXES

    Appendix XRD-5-(2.5%Al2O3+2.5%SiO2) after corrosion

    AL
    Al2Cu
    Al2CuMg

    Al2Cu 2 theta dm ds I/IO

    47.302 1.920 1.92 100

    38.459 2.338 2.38 84

    47.302 1.920 1.90 80

    56.115 1.6376 1.61 37

    65.074 1.432 1.41 13

    Al2CuMg 2 theta dm ds I/IO

    38.459 2.330 2.311 100

    44.7018 2.0256 2.016 30

    36.5072 2.4540 2.442 3

    47.3024 1.92014 1.942 20

    50.4191 1.898 1.836 9

    56.1150 1.6376 1.633 7


    APPENDIXES

    Appendix AFM -1-

    A-Nano alumina

    Granularity Cumulation Distribution Report


    Sample:Al 2 O 3 nano powder
    Instrument:CSPM
    Avg. Diameter:50 nm

    Diameter(nm)< Volume(%) Cumulation(%) Diameter(nm)< Volume(%) Cumulation(%) Diameter(nm)< Volume(%) Cumulation(%)

    25.00 0.79 0.79 55.00 3.17 11.90 85.00 5.56 57.94


    30.00 1.59 2.38 60.00 3.97 15.87 90.00 7.94 65.87
    35.00 0.79 3.17 65.00 4.76 20.63 95.00 8.73 47.60
    40.00 3.17 6.35 70.00 12.70 33.33 100.00 0.79 50.33
    45.00 1.59 7.94 75.00 10.32 43.65 105.00 9.52 92.86
    50.00 0.79 8.73 80.00 8.73 42.38 110.00 7.14 100.00
    APPENDIXES

    Appendix AFM -3-

    C-(Al-4.5%Cu-1.5%Mg)+(2.5%Al 2 O 3 +2.5%SiO 2 )

    Granularity Cumulation Distribution Report


    Sample: Mixed powders Code: (Al-4.5%Cu
    1.5%Mg)+(2.5%Al 2 O 3 +2.5%SiO 2 )
    Instrument: CSPM
    Avg. Diameter:80.52 nm

    Diameter(nm)< Volume(%) Cumulation(%) Diameter(nm)< Volume(%) Cumulation(%) Diameter(nm)< Volume(%) Cumulation(%)

    80.00 53.33 53.33 100.00 38.33 91.67 100.00 8.33 80.00


    APPENDIXES

    Appendix AFM -4-

    A-(5%Al 2 O 3 ) After Corrosion

    Granularity Cumulation Distribution Report


    Sample:5%Al 2 O 3 nano powder
    Instrument: CSPM
    Avg. Diameter :50 nm
    Diameter Volum Cumulati Diameter Volum Cumulati Diameter Volum Cumulati
    (nm)< e(%) on(%) (nm)< e(%) on(%) (nm)< e(%) on(%)
    20.00 0.74 0.74 50.00 3.12 11.50 80.00 5.51 57.89
    30.00 1.59 2.38 60.00 3.97 15.87 90.00 7.94 65.87
    40.00 3.17 6.35 70.00 12.70 33.33 100.00 0.79 92.86
    50.00 0.79 8.73 80.00 8.73 42.38 110.00 7.14 100.00
    APPENDIXES

    Appendix AFM -4-

    B-(5%SiO2) After Corrosion

    Sample: 5%SiO2nano powder


    Instrument: CSPM
    Avg. Diameter: 25 nm

    Diameter( Volume Cumulatio Diameter Volume Cumulatio Diameter Volume Cumulati


    nm)< (%) n(%) (nm)< % n(%) (nm)< (%) on%
    20.00 5.87 5.87 30.00 15.72 62.32 35.00 12.00 100.00
    25.00 21.87 27.73 32.00 13.32 74.67
    30.00 17.87 45.60 34.00 13.33 87.00
    APPENDIXES

    Appendix AFM -4-

    C-(2.5%Al 2 O 3 +2.5%SiO 2 ) after Corrosion

    Sample: (2.5%Al 2 O 3 +2.5%SiO 2 )


    Instrument: CSPM
    Avg. Diameter:80 nm

    Diameter(nm)< Volume(%) Cumulation(%) Diameter(nm)< Volume(%) Cumulation(%) Diameter(nm)< Volume(%) Cumulation(%)

    80.00 53.33 53.33 100.00 38.28 91.62 100.00 8.00 80.00


    APPENDIXES

    Appendix – 3- Tafel Test

    A-Base alloy(Al-4.5%Cu-1.5%Mg) at different sintering temperatures

    Figure(5-26) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) at 520C

    Figure(5-27) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) at 540C


    APPENDIXES

    Figure(5-28) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) at 560C°

    Figure(5-29) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) at 580C


    APPENDIXES

    Figure(5-30) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) at 600C

    B-Base alloy(Al-4.5%Cu-1.5%Mg) reinforced with nanoparticles

    Figure(5-31) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced 1%NanoAl2O3
    APPENDIXES

    Figure(5-32) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced 3%NanoAl2O3

    Figure(5-33) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced 5%NanoAl2O3
    APPENDIXES

    Figure(5-34) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced 1%NanoSiO2

    Figure(5-34) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced 3%NanoSiO2
    APPENDIXES

    Figure(5-35) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced 5%NanoSiO2

    Figure(5-36) Tafel test for the base alloy (Al-4.5%Cu-1.5%Mg) reinforced


    (2.5%Al2O3+SiO2)
    APPENDIXES

    Appendix – 6-

    Chemical Composition of sintered base alloy

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