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Lab Manual
Lab Manual
CONCRETE
TECHNOLOGY LAB
FINENESS BY SIEVING:
PROCEDURE:
1. Weigh accurately 100 g of cement and place it on a standard 90 micron IS sieve.
2. Break down any air-set lumps in the cement sample with fingers.
3. Continuously sieve the sample giving circular and vertical motion for a period of
15 minutes.
4. Weigh the residue left on the sieve. As per IS code the percentage residue
should not exceed 10%.
PRECAUTIONS: Air set lumps in the cement sample are to be crushed using fingers
and not to be pressed with the sieve. Sieving shall be done holding the sieve in both
hands and with gentle wrist motion. More or less continuous rotation of the sieve shall
be carried out throughout sieving.
OBSERVATIONS:
COMMENTS:
NORMAL CONSISTENCY OF CEMENT
(IS: 269 - 1989 and IS: 4031 - 1988 (Part 4))
AIM: To determine the quantity of water required to produce a cement paste of standard
consistency.
APPARATUS: Vicat apparatus (conforming to IS: 5513 - 1976) with plunger (10 mm in
diameter) balance, weights, gauging trowel.
PROCEDURE:
1. Prepare a paste of weighed quantity of cement (300 grams) with a weighed
quantity of potable or distilled water, starting with 26% water of 300g of cement.
2. Take care that the time of gauging is not less than 3 minutes, not more than 5
minutes and the gauging shall be completed before setting occurs.
3. The gauging time shall be counted from the time of adding the water to the dry
cement until commencing to fill the mould.
4. Fill the vicat mould with this paste, the mould resting upon a non porous plate.
5. After completely filling the mould, trim off the surface of the paste, making it in level
with the top of the mould. The mould may slightly be shaken to expel the air.
6. Place the test block with the mould, together with the non-porous resting plate, under
the rod bearing the plunger (10mm diameter), lower the plunger gently to touch the surface
of the test block and quickly release, allowing it to penetrate into the paste.
7. This operation shall be carried out immediately after filling the mould.
8. Prepare trial pastes with varying percentages of water and test as described
above until the amount of water necessary for making the standard consistency as
defined above is obtained.
9. Express the amount of water as a percentage by weight of the dry cement.
PRECAUTIONS: Clean appliances shall be used for gauging. In filling the mould the operator
hands and the blade of the gauging trowel shall alone be used. The temperature of cement,
water and that of test room, at the time when the above operations are being performed, shall
be 27 + 2 C. For each repetition of the experiment fresh cement is to be taken.
OBSERVATIONS:
Weight of cement Weight of water Plunger Consistency of
Time
S. No taken in gms taken in gms penetration cement in % by
(a) (b) (mm) Taken weight b/a * 100
RESULT: Normal consistency for the given sample of cement is
COMMENTS:
INITIAL AND FINAL SETTING TIMES OF CEMENT
(IS: 269- 1989 and IS: 4031- 1988 part 5)
AIM: To determine the initial and final setting times for the given sample of cement.
INTRODUCTION: In actual construction dealing with cement, mortar or concrete, certain time is
required for mixing, transporting and placing. During this time cement paste, mortar, or concrete
should be in plastic condition. The time interval for which the cement products remain in plastic
condition is known as the setting time. Initial setting time is regarded as the time elapsed
between the moment that the water is added to the cement to the time that the paste starts
losing its plasticity. The final setting time is the time elapsed between the moment the water is
added to the cement, and the time when the paste has completely lost its plasticity and has
attained sufficient firmness to resist certain pressure. The constituents and fineness of cement is
maintained in such a way that the concrete remains in plastic condition for certain minimum
time. Once the concrete is placed in the final position, compacted and finished it should lose its
plasticity in the earliest possible time so that it is least vulnerable to damages from external
destructive agencies. This time should not be more than 10 hours which is referred to as final
setting time. Initial setting time should not be less than 30 minutes.
PROCEDURE:
Preparation of Test Block:
1. Prepare a neat cement paste by gauging 300 grams of cement with 0.85 times
the water required to give a paste of standard consistency.
2. Potable or distilled water shall be used in preparing the paste.
3. The paste shall be gauged in the manner and under the conditions prescribed in
determination of consistency of standard cement paste.
4. Start a stop-watch at the instant when water is added to the cement.
5. Fill the mould with the cement paste gauged as above the mould resting on a
nonporous plate.
6. Fill the mould completely and smooth off the surface of the paste making it level with
the top of the mould. The cement block thus prepared in the mould is the test block.
PRECAUTIONS: Clean appliances shall be used for gauging. All the apparatus shall be
free from vibration during the test. The temperature of water and that of the test room, at the
time of gauging shall be 27 0C + 20 C. Care shall be taken to keep the needle straight.
OBSERVATIONS:
Time in minutes :
Height in mm fails to penetrate
COMMENTS:
SPECIFIC GRAVITY OF CEMENT
(IS: 269 -1989 AND IS: 4031-1988)
AIM
To determine the specific gravity is normally defined as the ratio between the weight of a
given volume of material and weight of an equal volume of water.To determine the
specific gravity of cement, kerosene which does not recent with cement is used.
APPARATUES
Le Chaterlier”s flask, is made of thin glass having a bulb at the bottom. The capacity of
the bulb is nearly 250 ml. The bulb is 7.8 cm in mean diameter. The stem is graduated
in millimeters. The zero graduation is at a distance of 8.8 cm from the top of the bulb. At
2 cm from the zero, there is another bulb is of length 3.5cm and capacity 17 ml. At 1 cm
from bulb, the stem is marked with 18 ml and is grated up to 24 ml. The portion above
24ml mark is in the form of a funnel of diameter 5cm.
PROCEDURE
(I) Dry the flask carefully and fill with kerosene or naphtha to a point on the stem
between zero and 1 ml.
(II) Record the level of the liquid in the flask as initial reading.
(III) Put a weighted quantity of cement (about 60 gm) into the flask so that level of
kerosene rise to about 22 ml mark, care being taken to avoid splashing and to see that
cement does not adhere to the sides of the above the liquid.
(IV) After putting all the cement to the flask, roll the flask gently in an inclined position to
expel air until no further air bubble rise3s to the surface of the liquid.
= W/(V2-V1)
NOTE
(II) To get more accurate result, the flask should be held in a constant temperature
before each reading is taken.
RESULT
AIM: To determine the soundness of the given sample of cement by "Le Chatelier" Method.
INTRODUCTION: It is essential that the cement concrete shall not undergo appreciable
change in volume after setting. This is ensured by limiting the quantities of free lime,
magnesia and sulphates in cement which are the causes of the change in volume
known as unsoundness. Unsoundness in cement does not come to surface for a
considerable period of time. This test is designed to accelerate the slaking process by
the application of heat and discovering the defects in a short time. Unsoundness
produces cracks, distortion and disintegration there by giving passage to water and
atmospheric gases which may have injurious effects on concrete and reinforcement.
The apparatus for conducting the test consists of small split cylinder of spring brass or
other suitable metal of 0.5mm thickness forming a mould 30 mm internal diameter and
30mm high. On either side of the split mould are attached to indicators with pointed
ends, the distance from these ends to the center of the cylinder being 165 mm. The
mould shall be kept in good condition with the jaws not more than 50mm apart.
PROCEDURE:
1. Place the lightly oiled mould on a lightly oiled glass sheet and fill it with cement
paste formed by gauging cement with 0.78 times the water required to give a paste of
standard consistency.
2. The paste shall be gauged in the manner and under the conditions prescribed in
determination of consistency of standard cement paste, taking care to keep the edges
of the mould gently together
3. While this operation is being performed cover the mould with another piece of glass
sheet, place a small weight on this covering glass sheet and immediately submerge the whole
assembly in water at a temperature of 27 0 - 20 C and keep there for 24 hours.
4. Measure the distance separating the indicator points.
5. Submerge the moulds again in water at the temperature prescribed above.
6. Bring the water to boiling, with the mould kept submerged for 25 to 30 minutes,
and keep it boiling for three hours.
7. Remove the mould from the water allow it to cool and measure the distance
between the indicator points.
8. The difference between these two measurements represents the expansion of the cement.
9. For good quality cement this expansion should not be more than 10mm.
OBSERVATIONS:
Initial distance between the indicator points in
mm = Final distance between the indicator
points in mm = Expansion in mm = final length -
initial length = RESULT: Expansion in mm
FINENESS MODULUS OF FINE AND COARSE AGGREGATE
AIM: To determine the fineness modulus of given fine and coarse aggregates.
APPARATUS: IS test sieves, square hole perforated plate 75mm, 40mm, 20mm,
10mm, and fine wire cloth of 4800, 2400, 1200, 600, 300, and 150 Microns. Weighing
balance (Sensitivity 0.1 percent) sieve shaker, tray plates.
INTRODUCTION: Fine aggregate is sand used in mortars. Coarse aggregate is broken stone
used in concrete. The size of the fine aggregate is limited to maximum 4.75 mm (4800 microns)
beyond which it is known as coarse aggregate. Fineness modulus is only a numerical index of
fineness, giving some idea about, the mean size of the particles in the entire body of concrete.
Determination of fineness modulus is considered as a method of standardization of grading of
aggregates i.e. the main object of finding fineness modulus is to grade the given aggregate for
the most economical mix and workability with minimum quantity of cement. It is obtained by
sieving known weight of given aggregate in a set of standard sieves and by adding the percent
weight of material retained on all the sieves and dividing the total percentage by 100.
PROCEDURE:
Coarse aggregate:
1. Take 5Kgs of coarse aggregate (nominal size 20mm) from the sample by quartering.
2. Carry out sieving by hand, shake each sieve in order 75mm ,40mm, 20mm,
10mm, and No's 480, 240, 120, 60, 30, & 15 over a clean dry tray for a period of
not less than 2 minutes.
3. The shaking is done with a varied motion backward and forward, left to right,
circular, clockwise and anticlockwise and with frequent jarring.
4. So that material is kept moving over the sieve surface in frequently changing directions.
5. Find the weight retained on each sieve taken in order
Fine aggregate:
1. Take 1 Kg of sand from sample by quartering in clean dry plate.
2. Arrange the sieves in order of No. 480, 240, 120, 60, 30 and 15 keeping sieve 480 at top
and 15 at bottom.
3. Fix them in the sieve shaking machine with the pan at the bottom and cover at the top.
4. Keep the sand in the top sieve no 480, carry out the sieving in the set of sieves
and arranged before for not less than 10 minutes.
5. Find the weight retained in each sieve.
OBSERVATIONS:
Coarse aggregate: Wt. of coarse aggregate taken: Kgs.
Cumulative
Weight % Weight % weight
S.No Sieve size % Weights
retained retained passing retained
1. 75 mm
2. 40 mm
3. 20 mm
4. 10 mm
5. 4800 microns
6. 2400 microns
7. 1200 microns
8. 600 microns
9. 300 microns
10. 150 microns
Cumulative
Weight % Weight % weight
S.No Sieve size % Weights
retained retained passing retained
1 4800 microns
2 2400 microns
3 1200 microns
4 600 microns
5 300 microns
6 150 microns
PRECAUTIONS:
1. The sample should be taken by quartering.
2. The sieving must be done carefully to prevent the spilling of aggregate.
AIM: To determine the specific gravity, void ratio, porosity and bulk density of given
coarse and fine aggregates.
1. Specific gravity is the weight of aggregate relative to the weight of equal volume of
water. 2. Void ratio is the ratio of volume of voids to the volume of solids in an aggregate.
3. Percentage of voids or porosity is the ratio of volume of voids to the total volume of a
sample of an aggregate.
4. Bulk density or unit weight is the weight of material per unit volume.
OBSERVATIONS:
Void ratio = v1 + v2 - v3 / v3 - v2
Porosity = v1 + v2 - v3 / v1
RESULT:
1) Specific gravity of course aggregate.
2) Void ratio of course aggregate.
3) Porosity of coarse aggregate.
4) Bulk density of course aggregate.
5) Specific gravity of fine aggregate.
6) Void ratio of the given fine aggregate.
7) Porosity of the given time aggregate.
COMMENTS:
.
BULKING OF SAND
PROCEDURE:
1) Take 1000ml measuring jar.
2) Fill it with loose dry sand upto 500ml without tamping at any stage of filling.
3) Then pour that sand on a pan and mix it thoroughly with water whose volume is equal to
2% of that of dry loose sand.
4) Fill the wet loose sand in the container and find the volume of the sand which is in
excess of the dry volume of the sand.
5) Repeat the procedure for moisture content of 4%, 6%, 8%, etc. and note down the readings.
6) Continue the procedure till the sand gets completely saturated i.e till it reaches the
original volume of 500ml.
OBSERVATIONS:
S.No Volume of dry % moisture Volume of wet % Bulking V2 –
loose sand V1 content added loose sand V2 V1 / V1
1. 500 ml 2%
2. 4%
3. 6%
4. 8%
5.
6.
GRAPH: Draw a graph between percentage moisture content on X-axis and percentage bulking
on Y-axis. The points on the graph should be added as a smooth curve. Then from the graph,
determine maximum percentage of bulking and the corresponding moisture content.
PRECAUTIONS:
1) While mixing water with sand grains, mixing should be thorough and uniform.
2) The sample should not be compressed while being filled in jar.
3) The sample must be slowly and gradually poured into measuring jar from its top.
4) Increase in volume of sand due to bulking should be measured accurately.
RESULT: The maximum bulking of the given sand is -----------at -----------% of moisture
content.
COMMENTS:
WORKABILITY TESTS ON FRESH CONCRETE
A) SLUMP TEST
APPARATUS: Iron pan to mix concrete, weighing machine, trowel slump, cone, scale
and tamping rod.
The slump cone is a hollow frustum made of thin steel sheet with internal dimensions,
as the top diameter 10 cms. The bottom diameter 20 cms, and height 30cms. It stands
on a plane non-porous surface. To facilitate vertical lifting from moulded concrete it is
provided with a suitable guide attachment and suitable foot pieces and handles. The
tamping rod is 16mm. dia. 60 cm. long and is bullet pointed at the lower end.
THEORY: Unsupported concrete, when it is fresh, will flow to the sides and a sinking in
height will take place. This vertical settlement is called slump. Slump is a measu6, 0.7
and 0.8. For each mix take 10 Kg. C.A., 5 Kg., FA and 2.5 Kg. Cement.
1) Mix the dry constituents thoroughly to get a uniform colour and then add water.
3) Place the mixed concrete in the cleaned slump cone in 4 layers each approximately
1/4 in height of the mould. Tamp each layer 25 times with tamping rod.
4) Remove the cone immediately, rising it slowly and carefully in the vertical direction.
5) As soon as the concrete settlement comes to a stop, measure the subsistence of the
concrete in cms, which gives the slump.
Note: Slump test is adopted in the Laboratory or during the progress of the work in the field
for determining consistency of concrete where nominal max., size of aggregates does not
exceed 40 mm. Any slump specimen which collapses or shears off laterally gives incorrect
results and at this juncture the test is repeated only true slump should be measured.
OBSERVATIONS:
1) The strokes are to be uniformly applied through the entire area of the concrete section.
2) The cone should be removed very slowly by lifting it upwards without disturbing the
concrete.
3) During filling the mould must be firmly pressed against the base.
4) Vibrations from nearly machinery might also increase subsidence; hence test
should be made beyond the range of ground vibrations.
COMMENTS: This test is not a true guide to workability. For example, a harsh coarse
mix cannot be said to have same workability as one with a large portion of sand even
though they have the same slump.
THEORY: This test is adopted to determine workability of concrete where nominal size
of aggregate does not exceed 40 mm. It is based on the definition, that workability is that
property of concrete, which determines the amount of work required to produce full
compaction. The test consists essentially of applying a standard amount of work to
standard quantity of concrete and measuring the resulting compaction.
The compaction factor is defined as the ratio of the weight of partially compacted concrete to the
weight of fully compacted concrete. It shall be stated to the nearest second decimal place.
PROCEDURE: Conduct test for W/c ratio 0.5, 0.6, 0.7, and 0.8, for each mix take 10 kg
of coarse aggregate 5kg of fine aggregate and 2.5 Kg of cement.
4. Fix the cylinder on the base with fly nuts and bolts
5. Mix coarse and fine aggregates and cement dry until the mixture is uniform in colour
and then with water until concrete appears to be homogeneous.
6. Fill the freshly mixed concrete in upper hopper gently with trowel without compacting.
7. Release the trap door of the upper hopper and allow the concrete of fall into the lower
hopper bringing the concrete into standard compaction.
8. Immediately after the concrete comes to rest, open the trap door of the lower hopper and allow
the concrete to fall into the cylinder, bringing the concrete into standard compaction.
9. Remove the excess concrete above the top of the cylinder by a trowel.
10. Find the weight of cylinder i.e cylinder filled with partially compacted concrete (W2 kgs)
11. Refill the cylinder with same sample of concrete in approx. 4 layers, tamping each
layer with tamping for 25 times in order to obtain full compaction of concrete.
12. Level the mix and weigh the cylinder filled with fully compacted concrete (W3 Kg)
S.No W/c ration Wt. With Wt. With Wt. With partially Wt. With fully Compaction
partially fully compacted compacted factor
compaction compaction concrete(W2- W3) concrete(W3- W1) (W1- W2)/
W2 W3 (Kgs) (Kgs) (W3- W1)
(Kgs) (Kgs)
1 0.5
2 0.6
3 0.7
4 0.8
PRECAUTIONS:
3. If the concrete in the hopper does not fall through when the trap door is released, it should
be freed by passing a metal rod. A single steady penetration will usually affect release.
COMMENTS: It is more sensitive, precise than slump test and is particularly useful to
concrete mixes of low workability.
Suggested ranges of values of compaction factors for different placing conditions.
workability workability
vibration
of reinforce
4 Concreting heavily d High 0.92 to above
section without
vibration
TEST FOR COMPRESSIVE STRENGTH OF CEMENT CONCRETE
(IS: 516 - 1959)
APPARATUS: Testing Machine, two steel bearing platens with hardened faces (As per
IS: 516 - 1959).
THEORY: Tests shall be made at recognized ages of the test specimens, the most
usual being 7 and 28 days, ages of 13 weeks and one year are recommended if tests at
greater ages are required. Where it may be necessary to obtain the early strength, test
may be made at the ages of 24 hours + 1/2 hour and 12 hours + 2 hours. The ages
shall be calculated from the time of the addition of water to the dry ingredients.
Number of Specimens
At least three specimens, preferably from different batches, shall be made for testing at
each selected age.
Placing the specimen in the Testing Machine The bearing surfaces of the testing machine shall
be wiped clean and any loose sand or other material removed from the surfaces of the
specimens which are to be in contact with the compression platens. In the case of the cubes,
the specimen shall be placed in the machine in such a manner that the load shall be applied to
opposite sides of the cubes as cast, that is, not to the top and bottom. The axis of the specimen
shall be carefully aligned with the center of thrust of the spherically seated platten. No packing
shall be used between the faces of the test specimen and the steel platten of the testing
machine. As the spherically seated block is brought to bear on the specimen, that movable
portion shall be rotated gently by hand so that uniform section may be obtained. The load shall
be applied without shock and increased continuously at a rate of approximately 140 Kg/sq
cm/min. Until the resistance of the specimen to the increasing load breaks down and no greater
load can be sustained. The maximum load applied to the specimen shall then be recorded and
the appearance of the concrete and any unusual features in the type of failure shall be noted.
REPORTING OF RESULTS:
The following information shall be included in the report on each test specimen:
a) Identification mark
b) Date of test
c) Age of specimen
d) Curing conditions including date of manufacture of specimen in the field
e) Weight of specimen
f) Dimensions of specimen
g) Compressive strength
h) Maximum load and
i) Appearance of fractured faces of concrete and type of fractures if these are unusual
COMMENTS: