MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : GTN Engineering (India) Ltd Unit-II (PMS) TC No. : EC2153 Date : 20.12.2023
Invoice No.:DWIF/23-24/ Date :
P.O. No.: 4710048186-0 Line Item: 3 PO Date : 07.11.2023 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
BODY FORGING, ULT PLUG Forged,
1299-GTN VALVE 1 ULT150 F/UNION 3257105 Rev L Normalized, 8.30 : 1 100 Nos. AISI 4140 BF-EOF-LRF-VD-CCM
ENDS AISI 4140 ALLOY STEEL Quenched &
FMC SPEC M25070 Tempered, - JSW STEEL
Shot Blasted
Heat Code: OUR DU500001271 Rev C
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo V Ni Grain Size
F18157 0.40 0.87 0.20 0.010 0.018 1.04 0.22 0.001 0.02 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 - - 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 0.30 1.00 -
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AG-984 HT Batch No. of Q&T:- AG-991 Qty :- 100 Nos.
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 8.30 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 37°C 50°C 570°C 5 Hrs (Air Cool)
Forging 8.30 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 37°C 50°C 570°C 5 Hrs (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Testing Annexure 4) Lab Reports 5) HT Graphs 6) Dimensional Report
Note :- We hereby guarantee that no weld repairs have been performed.
. We hereby certify that the above figures are accurate and are contained in the records of the company
For heat treatment batch traceability, "AG-991" is stamped near the heat code.
Furnace calibration has been conducted in accordance with AMS 2750G and meets the specified requirements.
The material is free from radioactive and mercury contamination.
Furnace used for normalizing and austenitizing (CF3): Calibration is due on 22.02.2024.
Furnace used for tempering (CF4): Calibration is due on 24.02.2024.
The above material meets the requirements of ASTM A788/A788M-23.
Method of Forging : Closed Die Forging

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- GTN Engineering (India) Ltd Unit-II (PMS) TC No: EC2153

P.O. No.:- 4710048186-0 Line Item: 3 PO Date : 07.11.2023 Date : 20.12.2023

BODY FORGING, ULT PLUG VALVE 1

Item : ULT150 F/UNION ENDS AISI 4140 ALLOY Material : AISI 4140
STEEL FMC SPEC M25070
Part No.: 3257105 Rev L Heat No. : F18157
Drawing No.: DU500001271 Rev C Ambient Temp : 25°C
Die No.: 1299-GTN Hardness Range:- 277 - 331 HBW
Qty.: 100 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AG-984 QT: AG-991 Sr No. 19/05/007
Reference Standard: ASTM E10 Machine Make: FSA
Load Applied: 3000 Kgs Calibration Agency: MME
Type of Penetrator: Dia 10 mm Carbide Ball Cert. No.: MME/CAL/337/23-24

Std Block Details: SH-0346/23 (Hardness value - 303.2 HBW) Calibrated On: 07.08.2023

Entity Performing Test: WIF Sanaswadi Calibration Due On: 06.02.2024

Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 10.12.2023
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Qty. Hardness in HBW

100 Nos. 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Ajay Joshi (HEAD-MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016

 MAGNETIC PARTICLE EXAMINATION REPORT

Customer : GTN Engineering (India) Ltd Unit-II (PMS)

PO No. : 4710048186-0 Line Item : 3 Report No : EC2153 Date : 20.12.2023

PO Date : 07.11.2023 Test Date : 11 & 12.12.2023

BODY FORGING, ULT PLUG VALVE 1 ULT150

Description : F/UNION ENDS AISI 4140 ALLOY STEEL FMC Die No. : 1299-GTN Heat Code : OUR
SPEC M25070

Part No. : 3257105 Rev L Qty. : 100 Nos.

Material : AISI 4140 Sr. No. : -

Heat No. : F18157 Heat Load No : N AG-984 QT AG-991

Stage of Examination
Drg. No. : DU500001271 Rev C Forged, Normalized, Quenched & Tempered, Shot Blasted
:
Standard /
Acceptance
Spec. / Q00207 Rev E , ASTM E 709-2021 Ed. Q00207 Rev E Clause no: 5.0
Standard / Criteria
Procedure :
Magnetic Particle Equipment (AC / FWDC) : Make - Vector NDT Technologies Model : V6000C

Calibration Date: 30.07.2023 : Calibration Due Date: 29.01.2024

Machine Sr. No : 30040419

Bath Temp.
Bath Concentration - 0.1 to 0.4 ml/ 100 ml Bath : 0.35 ml/ 100 ml Bath 48°C Observed 28°C
Required
UV-A Lamp irradiance Intensity - 1000 µWatt / cm² Minimum : 2700µWatt / cm² Make: NDT Consultant (UK) Sr no: 2137 (UV-
A + LUX Meter) Calibrated on: 11.07.2023
Ambient Visible illumination Intensity - 21.5 LUX Max. : 01 LUX Due on:11.01.2024
Type Of Magnetic Particle Material : Wet Fluorescent

Magnetic Particle Used : MG 410 Magnaflux Make Batch no: 23J19 Sep-23
Bath Medium : LTM 105 Carrier oil Batch no: VO9P1572 Sep-23
Surface Temp.
Surface Condition : As Shot Blasted 48°C Observed 25°C
Req.
Area to be examined : 100 % of accessible Surfaces

Magnetizing Process / Method : Wet Fluorescent Continuous Method

Means Of Establishing Magnetization : Current (in Head shot) + En Circling Coil On FWDC Mode

: 48 Gauss - Digital Hall Effect Probe Sr no:6050 Make: NDT Consultant (UK)
Observed Field Strength (Tangential)
Calibrated on: 11.07.2023 Due on:11.01.2024

Magnetization Field : Circular + Longitudinal

Applied Current : Circular : 2640 AMP , Longitudinal : 3600 AMP Technique Sheet No. -
WIF/MT/78 Rev -01
Sensitivity ensured By : QQI - SHIMS CX-430 Date - 09.12.2023
: Within (± 3 Gauss) - Make: GNAT, DRFI Digital Gauss Meter Sr
Residual field ensured after Demagnetization
no:218001 Calibrated on:08.09.2023 Due on:08.03.2024
Result : No relevant linear or rounded indication observed.

Remark : Material is accepted

Examined By Reviewed & Accepted By

Sign Sign
Name : More Vitthal.D. Name : Hemant Takawale
Cert. Type & Level - NDE Level II UT,MT,PT As Per SNT-TC-1A. Cert. Type & Level - NDE Level II UT,MT,PT,VT As Per SNT-TC-1A.
Doc. No:- F-NDT-03 Rev-02 - 09-July 2018
 Mechanical Test Annexure
Die No.: 1299-GTN Material Grade: AISI 4140

Heat No.: F18157 HT Lot No. : AG-991

Heat Code: OUR TC No. : EC2153

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below HT
L 311, 311 Ambient I-23-1016-P 1 149.40 132.29 19.49 59.33
Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
70 68 60 66.00
Single - 32 J Min
LE - 0.51 mm Min -29°C I-23-1017-P 0.88 0.86 0.80 0.85
%Shear - Report 65 65 60 63.33
L
Avg. - 27 J Min
56 58 66 60.00
Single - 20 J Min
LE - Report -40°C I-23-1018-P 0.78 0.80 0.85 0.81

%Shear - Report 60 60 65 61.67

0.5" below
Avg. - 28 J Min 1
HT Surface 32 66 36 44.67
Single - 18.7 J Min
LE - Report
-29°C I-23-1019-P 0.45 0.86 0.51 0.61

%Shear - Report 40 65 40 48.33

T
Avg. - 20 J Min
34 34 66 44.67
Single - 14 J Min
LE - Report -40°C I-23-1020-P 0.47 0.48 0.84 0.60

%Shear - Report 40 40 65 48.33

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
 CERTIFICATE OF COMPLIANCE
Customer : GTN Engineering (India) Ltd Unit-II (PMS) TC No.: EC2153
Date: 20.12.2023
Die No. : 1299-GTN Heat Code : OUR
PO No : 4710048186-0 Line Item No : 3
Offer Qty. : 100 Nos.
Part No/ Rev : 3257105 Rev L Drg No / Rev : DU500001271 Rev C
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
1 ULT150 F/UNION ENDS AISI 4140
ALLOY STEEL FMC SPEC M25070

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : F18157

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 20 Nos.

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : AG-984 Process Spec : Q00025 Rev S

B. Process Name : QT
Heat Lot No. : AG-991 Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI
Q00207 Rev E Clause
Certificate No : EC2153 Process Spec :
no: 5.0

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is to certify that the subjected material is manufactured from the material mentioned above and
has been verified by us according to the specified sample size. The material has been found to conform
to the requirements.
For heat treatment batch traceability, "AG-991" is stamped near the heat code.
The above material meets the requirements of ASTM A788/A788M-23.
Method of Forging : Closed Die Forging
Sign with Stamp
Ajay Joshi (HEAD-MQC, HT & NDT)