Sample : P11909

Operator: HIGOR
Comment : Comment
Group : Higor
Date : 2019-01-24 16:04:55

Measurement Condition
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Instrument: EDX-7000 Atmosphere: Vac. Collimator: 5(mm) Sample Cup:Polypropylene
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Analyte TG kV uA FI Acq.(keV) Anal.(keV) Time(sec) DT(%)
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Al-U Rh 50 95-Auto ---- 0 - 40 0.00-40.00 Live- 100 30
Na-Sc Rh 15 342-Auto ---- 0 - 20 0.00- 4.40 Live- 100 29
Rh-Cd Rh 50 999-Auto #1 0 - 40 19.50-23.50 Live- 100 4
Zn-As,Pb Rh 50 999-Auto #4 0 - 40 8.50-13.00 Live- 100 16
Cr-Fe Rh 50 222-Auto #3 0 - 40 5.20- 6.60 Live- 100 29
S-K Rh 15 829-Auto #2 0 - 20 2.10- 3.40 Live- 100 29

Qualitative Result
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Element: Cl, Mg, Br, Al, Sr, Si, Ca, P , S , K , Ti, Mn, Fe, Ni, Zn, Au, Hg
Rb, Rh, Na, Ba, Tb, I , Cu, Ag

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Peak List
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Channel Line keV Net Int.(cps/uA)
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Al-U ClKaESC 0.88 0.4803
MgKa 1.24 0.7798
BrLa 1.50 0.0585
AlKa 1.50 0.2081
SrLa 1.74 0.1993
SiKa 1.74 2.5461
CaKaESC 1.96 2.9743
P Ka 1.96 0.3227
S Ka 2.30 4.7952
CaKbESC 2.30 0.4441
ClKa 2.62 39.8631
K Ka 3.32 38.3386
K Kb 3.58 5.3674
CaKa 3.70 297.4345
CaKb 4.02 44.4087
TiKa 4.50 0.2316 QF
MnKa 5.90 5.4744
MnKb 6.40 0.8212
Ca SUM 6.40 3.1769
FeKa 6.40 4.4124
Ca SUM 7.04 1.4117
FeKb 7.06 0.0745
CaKaSUM 7.40 1.3812
NiKa 7.40 0.0081 QF
Ca SUM 7.72 0.6052
---- 8.04 0.9161
ZnKa 8.64 0.3551
ZnKb 9.64 0.0280
AuLa 9.64 0.2840 QF
HgLa 10.04 0.3192 QF
HgLb1 11.82 0.2554
BrKa 11.92 2.9242
BrKb 13.30 0.5200
RbKa 13.30 0.2880 QF
SrKa 14.14 8.2665 QF
SrKb 15.82 1.4880
RhKaC 19.14 6.7518
RhKa 20.18 8.1785
RhKbC 21.54 1.1361
RhKb 22.72 1.2385
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Na-Sc ---- 0.56 0.0339
ClKaESC 0.87 0.2379
Sample : P11909
Operator: HIGOR
Comment : Comment
Group : Higor
Date : 2019-01-24 16:04:55

NaKa 1.05 0.0701 QF

MgKa 1.25 0.4264 QF
AlKa 1.48 0.1660 QF
SiKa 1.74 1.3400 QF
CaKaESC 1.99 1.2796
P Ka 1.99 0.3657 QF
S Ka 2.31 2.2739
CaKbESC 2.31 0.1910
ClKa 2.62 19.7379
ClKb 2.82 2.9123
K Ka 3.31 14.1357
K Kb 3.59 0.9924
CaKa 3.69 94.9845 QF
CaKb 4.01 13.3714
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Zn-As,Pb CuKa 8.04 0.0068
ZnKa 8.64 0.0214 QF
BrKa 11.92 0.3438 QF
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Peak List
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Channel Line keV Net Int.(cps/uA)
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Cr-Fe MnKa 5.90 2.0057 QF
FeKa 6.40 2.7371 QF
Ca SUM 6.40 0.6244
MnKb 6.50 0.3009
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S-K S Ka 2.30 0.0884 QF
CaKbESC 2.30 0.0677
ClKa 2.62 2.2790 QF
ClKb 2.82 0.1732
K Ka 3.32 5.4969 QF
K Kb 3.59 0.8240
CaKa 3.69 46.8600
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Quantitative Result
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Analyte Result [3-sigma] Proc.-Calc. Line Int.(cps/uA)
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Ca 47.254 % [ 0.079] Quan-FP CaKa 94.9845
Na 14.882 % [ 1.852] Quan-FP NaKa 0.0701
Mg 12.536 % [ 0.287] Quan-FP MgKa 0.4264
Cl 11.430 % [ 0.080] Quan-FP ClKa 2.2790
K 8.085 % [ 0.035] Quan-FP K Ka 5.4969
Si 2.352 % [ 0.030] Quan-FP SiKa 1.3400
Al 1.347 % [ 0.087] Quan-FP AlKa 0.1660
S 0.900 % [ 0.057] Quan-FP S Ka 0.0884
Mn 0.381 % [ 0.005] Quan-FP MnKa 2.0057
Fe 0.346 % [ 0.004] Quan-FP FeKa 2.7371
P 0.298 % [ 0.021] Quan-FP P Ka 0.3657
Sr 0.073 % [ 0.001] Quan-FP SrKa 8.2665
Ti 0.041 % [ 0.005] Quan-FP TiKa 0.2316
Br 0.038 % [ 0.001] Quan-FP BrKa 0.3438
Hg 0.012 % [ 0.003] Quan-FP HgLa 0.3192
Au 0.012 % [ 0.003] Quan-FP AuLa 0.2840
Zn 0.010 % [ 0.001] Quan-FP ZnKa 0.0214
Rb 0.003 % [ 0.001] Quan-FP RbKa 0.2880
Ni 0.000 % [ 0.002] Quan-FP NiKa 0.0081
Sample : P11909 Group : Higor Date : 2019-01-24 16:04:55
Operator: HIGOR Comment : Comment 01/01
[cps/uA] Al-U

SUM FeKa
CaKa
40
S Ka CaKb ESC
ESC P Ka

SUM NiKa
CaKa SiKa

BrKb RbKa
AlKa

ZnKb AuLa
SUM
ClKa ESC

SUM
20

Ca
ClKa

CaKb
K Ka
K Kb

RhKaC
HgLb1

RhKbC
MnKb

SrKa
MnKa

RhKa
SrLa

BrKa
FeKb
CaKa

SrKb
MgKa
BrLa

----
ZnKa

HgLa

RhKb
TiKa

Ca
Ca
0
0.0 10.0 20.0 30.0
[keV]
[cps/uA] Na-Sc [cps/uA] Rh-Cd [cps/uA] Zn-As,Pb
10.0

BrKa
0.040
0.002
CaKa

7.5
0.030
S Ka CaKb ESC
CaKa ESC P Ka

5.0
0.020
0.001
ClKa
ClKa ESC

K Ka

CaKb
K Kb

2.5

ZnKa
0.010

CuKa
ClKb
SiKa
MgKa
AlKa
----

NaKa

0.0 0.000 0.000

0.0 2.0 4.0 20.0 22.0 10.0 12.0
[keV] [keV] [keV]
[cps/uA] Cr-Fe [cps/uA] S-K

4.00
SUM FeKa

CaKa
0.40
MnKa

3.00
S Ka CaKb ESC
MnKb

2.00
0.20
Ca

K Ka

K Kb
ClKa

1.00
ClKb

0.00 0.00
6.0 3.0
[keV] [keV]