1 s2.0 S0264127517307542 Main
1 s2.0 S0264127517307542 Main
1 s2.0 S0264127517307542 Main
H I G H L I G H T S G R A P H I C A L A B S T R A C T
A R T I C L E I N F O A B S T R A C T
Article history: Structured cellular structures are nowadays printed using additive manufacturing methods like powder
Received 21 April 2017 bed fusion. The relative density of the cellular structures has a big role in the suitability of a lattice for
Received in revised form 23 July 2017 printing due to the minimum printable radius constraint and powder being trapped inside an inclusion. In
Accepted 4 August 2017 this work, the theoretical limits of the printable range of relative density of different lattice types are found
Available online 7 August 2017
based on the cell size using computer methods by leaving other process parameters for further research as
the current parameters are the most basic ones. The results are approximated using simple polynomials to
Keywords: enable practical usage.
Additive manufacturing
© 2017 Elsevier Ltd. All rights reserved.
3D printing
Powder bed fusion
Structured cellular structures
Lattice
Printable relative density
* Corresponding author at: Mechanics of Materials and Structures, Department of Materials Science and Engineering, Ghent University, Technologiepark-Zwijnaarde 903,
Zwijnaarde 9052, Belgium.
E-mail address: niyazi.tanlak@ugent.be (N.Tanlak).
http://dx.doi.org/10.1016/j.matdes.2017.08.007
0264-1275/© 2017 Elsevier Ltd. All rights reserved.
550 N. Tanlak et al. / Materials and Design 133 (2017) 549–558
1. Introduction and loose powder adhesion to struts. Wang et al. [47] marked the
powder adhesion to struts as unavoidable in selective laser melt-
Cellular structures (a.k.a. foams) are known to have a good strength ing (SLM). The overhanging struts increase the problem. Optimizing
to weight ratio. They are used in many engineering applications rang- design and process control can minimize powder adhesion. Powder
ing from passive safety measures to space applications. By introducing adhesion is linked to balling phenomenon giving rise to beads on
structured foams, engineers have better control in tailoring the over- laser melted surfaces on building direction front by Yan et al. [42].
all material properties according to their needs. However, structured Abele et al. [48] claimed that building orientation has not any mean-
cellular materials are hard to produce with conventional manufactur- ingful effect on the printability of scaffolds in SLM processes. They
ing methods. Nonetheless, there are studies about the fabrication of also claimed that powder adhesions have not any meaningful effect.
periodic cellular materials with conventional methods, such as sheet On the other hand, Sallica-Leva et al. [49] concluded that powder
forming,perforated/slottedsheetfolding/drawing[1–4],extrusion[5], adhesion can act as stress concentrators, which in turn affects fatigue
wire assembly [6,7], and investment casting methods [8–12], how- strength of the porous structures. Hazlehurst et al. [50] concluded
ever, these techniques have limited flexibility with respect to structure that surface waviness variation and heterogeneities have a big effect
type and dimensions. On the other hand, additive manufacturing (AM) on the stiffness of lattice structures fabricated by SLM by using
allows an improved flexibility in geometry and size of lattice types. CoCrMo powder. Kim et al. [51] claimed that post-SLM sintering or
That opens up new possibilities for engineering applications. jet blasting can result in localized removal of these powder off the
Based on engineers’ needs, the unit cell of a structured foam is struts without changing the macro-properties of the scaffolds.
tailored such that the global properties of the edifice are adjusted to Leary et al. [52] found that downward facing surfaces of inclined
fulfill the specifications. Type, size and volume fraction of the unit struts had higher surface roughness than upward facing surfaces.
cell (lattice) are subjected to adjustments to reach the desired prop- They worked on overhanging struts having inclinations of 0, 35.26,
erties. Although there are studies about the mechanical properties of 45 and 90◦ being made up of AlSi12Mg by using SLM. They reported
foams [8,9,12-38], the printable ranges of the volume fraction of dif- that horizontal struts (0◦ inclined) were not printable for any of the
ferent lattice types with various cell sizes are not known thoroughly. diameters they tested. But they reported that reducing the spanned
Intuitively, it is tempting to think that such a cellular structure is distance can improve manufacturability for low inclination struts.
always printable. However, the printable density limits may change Similar surface roughness results of Leary et al. were found by Fox
dramatically with respect to the cell size and the type of lattice. et al. [53], Triantaphyllou et al. [54], Drescher et al. [55], and Suard
Either the lower limit or the higher limit of printable density may be et al. [56]. For Ti6Al4V, cantilever strut elements were studied by
paramount according to the needs at hand. The lower printable den- Mazur et al. [57]. They varied inclination angle in the range of
sity limit is based on the minimal feature size that can be printed 0–60◦ with 10◦ increments, and strut diameter of 0.3–1.0 mm with
by a specific process. The maximum printable density limit is prin- 0.1 mm increments. They found out that the minimum manufac-
cipally based on the density up to which all raw material can be turable strut angle is 20◦ and the minimum manufacturable strut
evacuated after manufacture. Although the entrapment of raw mate- diameter is 0.3 mm. On the other hand, they also found out that
rial formally allows the manufacture, the entrapped material will add struts as big as 3 mm are manufacturable while supported at both
mass in comparison with the designed density, which is considered ends. But horizontal struts ended up with oversized diameters due to
unacceptable. For better customization, the limits of the feasibility of high powder adhesion. Weißmann et al. [58] studied vertical and 45◦
printing should be known beforehand. In this work, we will focus on inclined struts fabricated by SLM and Electron Beam Melting (EBM).
selective powder bed fusion or sintering, but can equally be applied The struts from the SLM process were closer to the target specifica-
to several other AM processes. tion than the EBM-manufactured struts. The 45◦ inclined struts had
The printability of lattice structures using powder bed fusion bigger deviations from the desired.
depends on unit cell shape, relative density (i.e. strut radius) of unit Rehme and Emmelmann [59] defined an aspect ratio as cell
cell, strut inclination, powder particle size, powder material, machine edge length to strut diameter to assess the manufacturability by
precision, laser power, laser spot size, laser scanning speed, layer changing strut radius, cell size, and cell type. For 316-L stainless
thickness, and hatch spacing. The effect of spacing between parallel steel, the printable range was in between 3.36 and 22.9 from rela-
laser scans (a.k.a. hatch spacing) on manufacturability was studied by tively low to high, respectively. They also reported that printability
Zhang et al. [39]. They concluded that hatch spacing must be greater increases when strut length gets shorter. About minimum print-
than the laser spot size. They also advised that three times bigger pore able radius, researchers reported several values. The successful pro-
diameter than the maximum powder size must be present because duction of strut diameter of 0.05 mm were achieved by Van Bael
partially melted powder particles stick on strut surfaces. et al. [43] and Hao et al. [60] stated that struts with 0.025 mm radius
Sing et al. [40] reported that laser scan speed and laser power were possible. The studies investigating manufacturability of lattice
did not affect Young’s modulus. But strut diameter or lattice type structures, to authors’ knowledge, concentrated on specific param-
affected the elastic constant significantly while they did not affect the eters for small variations and only for a limited number of lattice
dimensional accuracy. They also reported that with the increase of types. Only one study [59] mentions explicit limits for one machine
laser scan speed or laser power, the powder adhesion on the struts precision and powder type. However, after its publication, other
decreased for Ti6Al4V. Loh et al. [41] found similar results. Other researchers [43,60] reported results beating those values. Through
researchers like Yan et al. [42], Van Bael et al. [43], Pattanayak et al. [44] the advancements in technology, the printable density limits are
also reported strut diameter increase due to powder adhesion. Qiu et changing. On the other hand, the printable density is dependent on
al. [45] studied the effect of laser scanning speed and laser power on the specifications of each process, and in fact, each machine and the
strut size, strut morphology, and surface structures. They compared raw material used. Therefore, there is a need for a tool estimating
two different laser power (150 and 400 W). 400 W resulted in thicker printable density limits of lattice structures based on given condi-
powder adhesion to struts with bigger deviation with respect to the tions. In this work, the authors try to estimate those limits only
laser power of 150 W for AlSi10Mg. Besides, they also found out that by using the most fundamental parameters affecting those limits:
the scanning speeds below 3000 mm/s affected the strut diameter. the machine precision and powder size for different lattice types by
Tsopanos et al. [46] reached similar results. They showed that high leaving the study of other parameters to later studies. Since these are
laser power led to thicker struts of lattices. the most basic factors in terms of printability and some other param-
Van Bael et al. [43] claimed three reasons for the deviations from eters can be modeled with these, the study can be used as the basis
the CAD model: inadequately chosen beam offset, staircase effect, point for further research.
N. Tanlak et al. / Materials and Design 133 (2017) 549–558 551
2. Problem formulation
To create the CAD models of the lattices, a preprocessor of a commercial CAE software [61] is used together with Python scripting language
to enable the algorithms presented in this study to be embodied. The unit cells with cubic outer boundary space are considered. All struts in a
lattice are assumed to have the same circular cross-sectional area. Fig. 1 shows the unit cell types used schematically.
The numerical prediction of the lower and higher printable density limits of lattice structures for AM problem can be stated mathematically
as follows:
For : 1) ∀t ∈ T | T = {Cubic, Bcc, Fcc, Octahedron, CubicBcc, CubicFcc, BccFcc, Octet, CubicBccFcc}
2) ∀L | L ∈ IR +
3) ∀rmin ∈ r̄min | r̄min = {rmin | rmin ∈ IR+ & rmin ≤ L}
4) ∀Vp ∈ V̄p | V̄p = {Vp | Vp ∈ IR3 & 0 < Vp < L3 } (1)
where r is the strut radius; rl is the critical strut radius value related to qlow ; qlow is the lowest printable relative density; rh is the critical strut
radius value related to qhigh ; qhigh is the highest printable relative density; L is the cell size of a lattice; nvoid is the number of independent void
volumes inside the cell; rmin is the minimum printable radius which is a machine specific value; t is the lattice type; Vp is the volume of the
sphere circumscribing the biggest powder particle used; rinsmax is the radius of the biggest sphere that can fit into every chunk of void volume;
Amin is the corresponding powder cross-sectional area; Yv is the void volume of a lattice; ∂ Y is the surface of the cube enclosing a lattice; Ys is
a sub-volume of Yv ; P is a point; c is a space curve; is Euclidean distance operator; rlump is the corresponding radius of Vp ; I is the interval
1
over which c defined; Iv is the interval over which Yv defined; j is the curvature of a curve at every point; min j(c) is the minimum radius
of curvature of the curve c.
More specifically, the main objective of this study is to find the minimum and the maximum printable relative density for a given lattice
type, lattice size, the minimum printable radius, and the powder lump size. The strut radius values should not be smaller than zero and should
not be bigger than the lattice cell size. While finding the minimum and the maximum printable relative density, the void volume should be
monolithic (see the constraint 2 on the right-hand side of Eq. (1)). One may think that a single lattice having disconnected voids can be printable
as long as the voids are connected to one of the faces of the cubic envelope. However, when considering periodic lattices, and considering that
the faces are symmetry planes, these disconnected voids will turn into closed cavities which entrap powder. By constraining the sub-volume
formation, it is ensured that the powder can go out as long as at least one face is open. Hence, the number of void volumes inside a lattice
should be equal to unity.
The powder used in the AM process has a size. Moreover, the unused powder may form lumps during printing, which in turn makes their
effective radius even bigger, e.g. by partial sintering of loose particles, or by spatter from the process [62], landing on the unused powder zones.
Thus, having a monolithic void volume is not enough on its own in order to take the powder out. In Fig. 2, a 2D schematic shows how a powder
particle can go through the void between two struts. In order to ensure that the powder in the void spaces can be evacuated after printing, the
void volume has to have a minimum hole area which is bigger than the corresponding cross-sectional area of the powder lumps on faces of
the lattices (See the constraint 3 on the right-hand side of Eq. (1).).
Besides, there has to be enough space for powder inside the void volume to let the powder go through. To ensure so, a void sub-volume
is required, whose branches’ cross-sectional area has to be equal to the cross-sectional area of the powder lump, at least. A space curve, c, is
employed to define the sub-volume over the same interval of the void volume. Since the powder is a sphere, checking the cross-sectional area
is not enough to prevent powder entrapment. Hence, the curvature of the space curve is also constrained as defined in the constraint 4 on the
right-hand side of Eq. (1). In other words, there should be, at least, a sub-volume, Ys , inside the void volume whose interval is the same as
the interval the void volume defined over so that it touches the faces of the enclosing cube. By adding the distance to the formulation of Ys , a
pipe-like volume whose cross-section is a circle with rlump is created throughout the interval. By checking the curvature of the curve, one will
be sure that the powder sphere will go through the pipe-like sub-volume; therefore the void volume.
On the other hand, machines are subjected to precision constraints, as well. Hence, they have a limit of the smallest printable radius. For
this reason, the smallest printable radius should be taken into account for estimating limits of being printable for a lattice. Therefore, in order
to find qlow for each lattice type, this constraint has to be taken into account (See the constraint-1 of Eq. (1)).
552 N. Tanlak et al. / Materials and Design 133 (2017) 549–558
rmin
qlow = g r̄ = , t, L (4)
Fig. 3. Typical number of void volumes versus the relative strut radius in unit cell. L
N. Tanlak et al. / Materials and Design 133 (2017) 549–558 553
up, in this case, the printable interval of the relative density of lattice
structures will be narrower than the infinitesimal powder problem.
As can be viewed from the results of the infinitesimally thin pow-
der problem (see Table 3 in Section 4.1), there are bottlenecks in the
void volume. To calculate the higher limit, qhigh , one has to find the
locations and the orientations of these bottlenecks, which are the
smallest interconnecting sections that keep the void volume mono-
lithic and determine whether the cross section lets the powder go
through. From the infinitesimally thin powder problem, one already
knows the positions of the bottlenecks. On both sides of these sep-
aration points (bottlenecks), the cross section increases. Therefore,
checking the void volume’s cross-sectional area at these points and
normal to the bottleneck axis will be enough to check the powder
entrapment. The simplified problem can then be stated as follows:
Maximize q(r, t, L, Vp )
Subjected to : nvoid = 1
2
prins max
on ∂ Y ≥ Amin
2
prins max
on C .P . ≥ Amin (5)
where C.P. stands for the cross plane perpendicular through the
bottleneck points.
The removal of the powder is based on the fact that the mono-
lithic void volume in each cell leads to an interconnected monolithic
void in the multi-cell structure. Therefore the removal of the pow-
der in the voids is possible with help of gravity, vibration and air
pressure, as long as the powder particles can pass through the
bottlenecks in the interconnected cell voids (Fig. 5).
In the infinitesimally thin powder case, the void volume is main-
tained together only with point contact. Slightly bigger values than
the critical radius, rh , will result in multiple void volumes and create
twin points on each side of the newly separated void volumes. Using
the CAD model of a lattice for rh (Vp = 43 pe3 ), one may pinpoint the
Fig. 4. Flow chart of modified bisection method for function at hand which is depicted
in Fig. 3. bottlenecks and their orientations. One may partition the void vol-
ume at the desired location and at the desired orientation such that
one can find the smallest cross-section using CAD representation for
any given strut radius, r (see Fig. 3). Finding the biggest radius of a
Fig. 5. A few hypothetical scenarios for powder and hole cross-sectional area, which Fig. 6. Typical void cross-sectional shape change in terms of strut radius around
powder can be taken out. separation point.
554 N. Tanlak et al. / Materials and Design 133 (2017) 549–558
circle that can be inscribed on the smallest section of the void vol- Table 1
rh
Critical relative radius, , values corresponding to upper relative density limits, qhigh .
ume, rinsmax , is yet another optimization problem which can be stated L
rh
as follows: Lattice type L qhigh
Table 2
Coefficients of the polynomials, g, fitted to r̄ for q.
Fig. 7. Upper limits for several lattice types based on the two criteria together. R2 is the coefficient of determination.
N. Tanlak et al. / Materials and Design 133 (2017) 549–558 555
Table 3
Solid and void volumes of upper thresholds using infinitesimal powder assumption.
Fig. 9 shows the curves for only rmin = 0.2 mm and rlump = 0.2 Based on the crossing point of the upper and lower limits, there is
mm. However, the possible combinations of rmin and rlump values are a relationship like the following:
endless. Hence, it is necessary to build a dimensionless graph such
that one can find the corresponding printable range for given rmin
r rlump
rmin rh Vp = 43 pe3 rlump
and rlump . In Fig. 10, such a graph is given, whose min
L and L are = − (9)
plotted on the same axis. However, completely independent values L L L
can be selected for them. The relative density values on the graph are
limited up until the corresponding the highest relative density, qhigh , Using this equation, one can calculate the other r value if one
of each lattice. In order to clarify how to use the figure, the print- is given. Fig. 11 shows the boundary of printable zone in terms of
r rlump
able range is found using L = 5 mm, rmin = 0.2 mm, and rlump = dimensionless parameters min L and L . The regions under the lines
0.1 mm for Octet lattice. The resultant range is [0.075, 0.843]. The are the printable zones in Fig. 11. If a combination is on the boundary
corresponding values are marked in Fig. 10. then that means only one value can be printable.
556 N. Tanlak et al. / Materials and Design 133 (2017) 549–558
Fig. 8. Relative density, q, versus relative radius, r̄, of the struts for some lattice types: left: full range; right: the printable range for the infinitesimally thin powder.
The minimum printable feature radius based on strut inclination the realized and planned diameter of struts is a function of strut incli-
can be found either in the literature or by experiment. In literature, nation. Therefore, one can expect a lattice having different diameter
there are several minimum printable radius values in terms of strut struts after printing even if a lattice having equal diameter struts are
inclination. This constraint can be treated via the machine precision intended. To guess the printable limits at such conditions, one needs
(the minimum printable radius) terms in this study. That value can be to estimate radius difference based on inclination angle. After taking
plugged into the equation (Eq. (4)). Moreover, the manufacturability the biggest difference expected, one can hypothetically assume a big-
of horizontal struts was discussed in the literature. Mazur et al. [57] ger powder lump as much as the biggest radius difference foreseen
reported that by using SLM, they achieved to print horizontal struts to find the highest printable limit.
up to 3 mm if they are supported at both ends. In the current state- Despite having useful estimations of the printable density range
of-the-art, the lattices having horizontal struts (e.g. Cubic, CubicBcc, based on the assumptions made here, there is a need for a further
CubicFcc, CubicBccFcc) are not printable unless they are smaller than study which includes other parameters for manufacturability of lat-
3 mm for Ti6Al4V. Hence, the reader must be aware of this limita- tice structures. One can say that the real printable density range may
tion (can be different for every powder material) when they are using be smaller than the one found here as explained in Eq. (10).
Fig. 10.
Powder adhesion problem can also be taken into the account
by the powder lump size. As an example powder lump size can be
qreal corr
low = qlow + qlow = qlow (r̄ + r̄corr )
taken as a couple of times bigger than the biggest powder size used.
The exact amount has to be investigated for every material. Zhang qreal corr
high = qhigh − qhigh = qhigh (r̄ − r̄corr ) (10)
et al. [39] suggested using three times bigger pore sizes. Further-
more, as reported by several authors [52–58], the difference between
Fig. 9. Thresholds of lattice structures using rmin = 0.2 mm and rlump = 0.2 mm. Fig. 10. Printable thresholds of lattice structures in dimensionless form.
N. Tanlak et al. / Materials and Design 133 (2017) 549–558 557
parameters for exact limits. It is easily foreseeable that the real print-
able density range will be narrower than the ones found in this
work. Furthermore, finding the optimized process parameters or the
advancement of technology will approach the printable density lim-
its to the ones found in this paper. Therefore, this study can be taken
as a basis point for further investigations.
Acknowledgment
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