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    Silica Presentation (ENG)

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    lalagabriella.1407

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    © All Rights Reserved
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    Silica Presentation (ENG)

    Uploaded by

    lalagabriella.1407
    2 views19 pages

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    2 views19 pages

    Silica Presentation (ENG)

    Uploaded by

    lalagabriella.1407

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 19

    Chemland Spherical Powder

    2024.02 -1-
    Spherical Powder

    • Spherical powder ▷ Powder with spherical particle shape

    • Provides smooth, light texture, spreadability, and flowability to powder cosmetic compositions.

    • The soft focus effect is superior to flake powder in concealing skin defects such as pores and acne marks.

    • Silica, PMSQ(Polymethysilsesquioxane) Nylon(nylon-6/nylon-12), PMMA(polymethylmethacrylate)etc

    SESQ ML5 (PMSQ) CL-Silica 300 CL-Silica 900


    -2-
    Soft Focus Effect
    Principle Factors
    Specular Reflection Diffuse Reflection

    Control the feeling

    The closer to spherical shape

    The higher the porosity

    High Purify

    Hard Focus Soft Focus

    -3-
    Spherical Powder
    Pickering emulsion
    Definition The contact angle

    Solid particles adsorb at the interface between the two


    phases to form a stabilized emulsion.

    Solid
    particles

    Contact angle between the interface and the surface of the


    solid particle Orientation of the interfacial film

    Θ<90° : O/W Emulsion


    Θ>90° : W/O Emulsion
    &
    Θ=90° : The stable emulsion depends on the oil polarity
    (Polar oils → W/O Emulsion)

    -4-
    Spherical Powder

    USED FOR SPREADABILITY


    SILICA

    PMMA
    PRICE

    CREAMY

    HARDNESS

    SILKY

    ELASTIC
    PMSQ

    NYLON

    URETAN

    ELASTOMER

    * IF PARTICLE SIZE IS BIG, SPREADABLILITY IS GOOD BUT IT’S EASILY REMOVED FROM SKIN
    -5-
    CL-SESQ Series
    (PMSQ)

    -6-
    Polymethylsilsesquioxane (PMSQ)

    • Siloxanes: No solid type (Solid type can be obtained by cross link)


    • Silsesquioxanes: ‘Sesqui’ means 1.5
    Soluble polymer(Wax type), crystalline particle, un-soluble solid in net structure
    • Silica: Crystalline

    -7-
    SESQ ML5 (CL)
    SESQ ML5 (CL)

    • PMSQ-ML5 is spherical powders of polymethylsilsesquioxane


    produced from methyltrimethoxysilane.
    • No added ingredients other than water, methyltrimethoxysilane, base
    (pH control), and acid (pH control).
    • Particle size: 3~6 um
    • Hydrophobic but also can be dispersed in water with Hydrophilic
    organic.
    • Pickering effect in some oil/water phase.
    • Creamy and silky.
    • Soft focus effect.
    • Useful as emollients.
    • Lubricating other powdery materials.
    • Stable at high temperature.
    • Oil absorbency : 40~70%.

    -8-
    SESQ MH5 (CL)
    SESQ MH5 (CL)

    • Hydrophilic polymthylsilsesquioxane consist of the silicone which was


    made by patented Technique.
    • Particle size : 3~6 um
    • Self-soluble in water with out shearing stress due to its high
    hydrophilic character.
    • Oil absorbency : 50-80%.
    • Water Absorbency : 70~100%
    • Excellent skin texture.

    -9-
    CL-SESQ Series
    (PMSQ)

    - 10 -
    CL-Silica
    • Generally called Silicon dioxide (SiO2)

    • Silica comes in different types and is used in many industry, but in cosmetics and personal care products,

    However, in cosmetics and personal care products, amorphous silica powder is primarily used..

    • Amorphous microbead silica is not included in microplastics.

    • It is a white, odorless, hydrophilic powder that gives a light and refreshing feeling.

    • Role in improving cosmetic using feeling.

    • Excellent ball bearing effect due to high hardness.

    - 11 -
    CL-Silica

    • Features of Silica

    •The particles adsorb at the interface between oil and water, enhancing
    Pickering Emulsion emulsification stability and forming a Pickering emulsion.

    • Micro-sized spherical particles diffuse reflection, resulting in scatter light.


    Soft Focus Effect •Conceals skin imperfections and wrinkles, providing skin correction effects.

    • With its large surface area due to porosity, it absorbs sebum and sweat,
    providing a refreshing sensation.
    Sebum Control • Its high absorption capacity allows for the production of products contai
    ning functional oils.

    • Spherical, high-hardness particles do not deform upon skin contact.


    Ball Bearing Effect • Enhances spreadability, dispersibility, lubricity, and prevents clumping i
    n mixed products.

    •The particles maintain their shape and functionality even after exposure
    Stability to high heat.

    - 12 -
    CL-Silica
    • SEM Images of CL Silica

    x1,000 x5,000 x10,000

    CL Silica
    600

    CL Silica
    LA 1000

    - 13 -
    CL-Silica

    • SEM Images of CL Silica 600 and two other products

    CL Silica 600 H company S company


    (x5000) (x6000) (x6000)

    • CL-Silica distinguishes itself with higher purity and more uniformly spherical particle compared to
    competing products

    - 14 -
    Application

    • Transparency Test in EtOH (5% sol.)

    H. Co CL-Silica S.Co • Shows higher transparency compared to other companies


    during the ethanol test

    • Due to uniform particle size, it results in reduced refractive


    index / high purity.

    • When applied in formulations, it can make clear condition.

    - 15 -
    CL-Silica
    • Particle size distribution is narrow compared to other companies
    → Due to high uniformity, lot variation is small and a consistent feeling of use can be given to the formulation.
    * σ1 (standard deviation) sk1 (asymmetry)
    Data
    (Vol. distribution)
    CL Silica 600 H company S company

    Spec. D50 (μm) 6.0 5.0 7.0


    D10 (μm) 5.24 4.08 4.63
    D50 (μm) 6.95 5.93 6.55
    D99 (μm) 18.40 18.39 18.41
    σ1 1.804 1.999 2.019
    sk1 0.2577 0.2804 0.2568

    - 16 -
    Success Story

    Makeup Forever UHD


    Pressed Powder

    - 17 -
    Success Story

    Innisfree No Sebum Neo Essential Blurring Finish Po


    Mineral Powder wder | LANEIGE Indonesia

    - 18 -
    CL-Silica
    • CL Silica : Hollow, Hydrophilic, Amorphous, Spherical
    Name Avg. Size [μm] pH Loss on Drying [%] Oil Absorbency [%]
    CL Silica 300 2.0 ~ 4.0
    CL Silica 600 4.0 ~ 7.0 5.0 ~ 9.0 <5 130 ~ 170
    CL Silica 900 7.0 ~ 10.0

    • CL Silica LA : Non-hollow, Amorphous, Spherical


    Name Avg. Size [μm] pH Loss on Drying [%] Oil Absorbency [%]
    CL Silica LA 300 2.0 ~ 4.0 <5 80 ~ 120
    CL Silica LA 600 4.0 ~ 7.0 5.0 ~ 9.0 <5 90 ~ 120
    CL Silica LA 1000 8.0 ~ 12.0 <5 110 ~ 150

    • CL Silica ELA : Non-hollow, Amorphous, Spherical


    Name Avg. Size [μm] pH Loss on Drying [%] Oil Absorbency [%]
    CL Silica ELA 300 2.0 ~ 4.0
    5.0 ~ 9.0
    CL Silica ELA 600 4.0 ~ 7.0 <5 60 ~ 100
    CL Silica ELA 900 7.0 ~ 10.0 6.0 ~ 8.0

    - 19 -

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