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Name and Formula: Natl. Bur. Stand. (U.S.) Monogr. 25, 18, 59, (1981)

The document provides information on hot pressed silicon nitride (HPSN), including its empirical formula of N4Si3, crystal structure parameters, and density. It was prepared by heating silicon nitride to 1785°C for an hour under pressure. The document also includes a peak list with 60 diffraction peaks for HPSN with corresponding Miller indices, d-spacings, angles, and intensities.

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mustijabhaider
Copyright
© Attribution Non-Commercial (BY-NC)
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
61 views

Name and Formula: Natl. Bur. Stand. (U.S.) Monogr. 25, 18, 59, (1981)

The document provides information on hot pressed silicon nitride (HPSN), including its empirical formula of N4Si3, crystal structure parameters, and density. It was prepared by heating silicon nitride to 1785°C for an hour under pressure. The document also includes a peak list with 60 diffraction peaks for HPSN with corresponding Miller indices, d-spacings, angles, and intensities.

Uploaded by

mustijabhaider
Copyright
© Attribution Non-Commercial (BY-NC)
Available Formats
Download as DOC, PDF, TXT or read online on Scribd
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Name and formula

Reference code:

00-033-1160

Common name:
PDF index name:

HPSN (hot pressed silicon nitride)


Silicon Nitride

Empirical formula:
Chemical formula:

N4Si3
Si3N4

Crystallographic parameters
Crystal system:
Space group:
Space group number:

Hexagonal
P63/m
176

a ():
b ():
c ():
Alpha ():
Beta ():
Gamma ():

7.6044
7.6044
2.9075
90.0000
90.0000
120.0000

Calculated density (g/cm^3):


3.20
Volume of cell (10^6 pm^3): 145.61
Z:
2.00
RIR:

Subfiles and Quality


Subfiles:

Quality:

Inorganic
Alloy, metal or intermetalic
Common Phase
NBS pattern
Star (S)

Comments
Color:
Sample preparation:

Additional pattern:

Grayish white
The sample was prepared at NBS, Gaithersburg, Maryland, USA,
by J. Waring by heating Si3N4 obtained from GTE Products,
Towanda, Pennsylvania, USA to 1785 C for 1 hour at 15 psig.
The sample was contained in a Si3N4 crucible within a
molybdenum crucible.
To replace 9-259 and 29-1132.
See ICSD 8263 (PDF 71-623); ICSD 100135 (PDF 83-1287).

References
Primary reference:

Natl. Bur. Stand. (U.S.) Monogr. 25, 18, 59, (1981)

Peak list
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52

h
1
1
2
1
2
1
3
2
2
2
3
3
2
3
3
0
4
4
1
1
3
2
5
4
3
2
4
5
5
3
2
4
3
5
4
5
3
6
4
4
6
5
5
1
3
6
4
5
2
5
6
4

k
0
1
0
0
1
1
0
0
2
1
1
0
2
1
2
0
1
0
0
1
2
0
0
1
3
1
2
0
1
3
2
2
1
1
3
2
2
0
1
3
1
2
0
0
3
1
2
3
0
1
2
4

l
0
0
0
1
0
1
0
1
0
1
0
1
1
1
0
2
0
1
2
2
1
2
0
1
0
2
0
1
0
1
2
1
2
1
0
0
2
1
2
1
0
1
2
3
2
1
2
0
3
2
0
1

d [A]
6.58300
3.80000
3.29300
2.66000
2.48900
2.31000
2.19390
2.17970
1.90130
1.89160
1.82750
1.75250
1.59110
1.54670
1.51080
1.45340
1.43680
1.43250
1.41970
1.35790
1.34080
1.32990
1.31730
1.28830
1.26750
1.25540
1.24470
1.19980
1.18310
1.16180
1.15510
1.14450
1.13770
1.09570
1.08280
1.05450
1.04760
1.02690
1.02190
1.01470
1.00430
0.99140
0.97610
0.95890
0.95540
0.94920
0.94550
0.94080
0.92980
0.91750
0.91320
0.90340

2Theta[deg] I [%]
13.440
34.0
23.391
35.0
27.056
100.0
33.666
99.0
36.056
93.0
38.958
9.0
41.110
10.0
41.390
31.0
47.800
8.0
48.061
5.0
49.859
12.0
52.150
37.0
57.911
12.0
59.739
6.0
61.309
15.0
64.011
15.0
64.840
8.0
65.059
5.0
65.719
1.0
69.121
1.0
70.130
39.0
70.791
6.0
71.572
5.0
73.442
18.0
74.851
7.0
75.699
16.0
76.466
1.0
79.886
2.0
81.247
2.0
83.062
1.0
83.652
2.0
84.605
3.0
85.230
3.0
89.340
4.0
90.697
3.0
93.855
1.0
94.665
6.0
97.202
1.0
97.840
4.0
98.777
1.0
100.171
2.0
101.970
3.0
104.214
4.0
106.896
3.0
107.464
5.0
108.490
8.0
109.116
1.0
109.924
1.0
111.881
2.0
114.188
1.0
115.027
3.0
117.006
4.0

53
54
55
56
57
58
59
60

5
3
7
6
4
2
3
5

3
0
1
2
3
2
1
2

Stick Pattern

1
3
0
1
2
3
3
2

0.89500
0.88660
0.87220
0.87120
0.86820
0.86340
0.85610
0.85370

118.784
120.645
124.054
124.302
125.056
126.295
128.258
128.926

3.0
5.0
6.0
5.0
5.0
1.0
1.0
2.0

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