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    111 Titration

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    Elisa
    This document provides instructions for conducting acid-base titration experiments. Students are asked to determine the molarity of strong and weak acid solutions by titrating them with a sodium hydroxide solution of a known concentration and recording the pH changes. Precise procedures are outlined for preparing the solutions, collecting pH data during the titration using a LabQuest interface, identifying the equivalence point on the resulting graph, and safely disposing of the solutions after neutralization. A trial with acetic acid is also to be completed.

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    111 Titration

    Uploaded by

    Elisa
    17 views12 pages
    This document provides instructions for conducting acid-base titration experiments. Students are asked to determine the molarity of strong and weak acid solutions by titrating them with a sodium hydroxide solution of a known concentration and recording the pH changes. Precise procedures are outlined for preparing the solutions, collecting pH data during the titration using a LabQuest interface, identifying the equivalence point on the resulting graph, and safely disposing of the solutions after neutralization. A trial with acetic acid is also to be completed.

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    This document provides instructions for conducting acid-base titration experiments. Students are asked to determine the molarity of strong and weak acid solutions by titrating them with a sodium hydroxide solution of a known concentration and recording the pH changes. Precise procedures are outlined for preparing the solutions, collecting pH data during the titration using a LabQuest interface, identifying the equivalence point on the resulting graph, and safely disposing of the solutions after neutralization. A trial with acetic acid is also to be completed.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    17 views12 pages

    111 Titration

    Uploaded by

    Elisa
    This document provides instructions for conducting acid-base titration experiments. Students are asked to determine the molarity of strong and weak acid solutions by titrating them with a sodium hydroxide solution of a known concentration and recording the pH changes. Precise procedures are outlined for preparing the solutions, collecting pH data during the titration using a LabQuest interface, identifying the equivalence point on the resulting graph, and safely disposing of the solutions after neutralization. A trial with acetic acid is also to be completed.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    of 12

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    Hand in the Flow Chart for EXP 8 (Acid-Base Titration)
    Hand in the Data Processing and Post Lab questions for 7
    (Standardization of NaOH)
    Acid-Base Titration
    Experiment 8 Week of 4/6/15
    Experimental Summary
    Purpose
    Conduct acid-base titrations
    Compare equivalence points of strong and weak acids
    Determine the Molarity of the two acid solutions
    Molarity and Titrating Solutions
    Molarity = moles of solute / liters of solution
    Titration = the process used to determine the volume of a
    solution needed to react with a given amount of another
    substance
    Can be used to determine the molarity of an unknown solution
    Titrant = solution delivered from a buret
    Equivalence point = the region where the smallest change in
    volume causes the greatest change in pH
    Preparing Solutions for Titration
    Add 25 mL HCl to a 50 mL beaker
    This will be your stock solution of HCL
    Add 50 mL DI H2O to a 250 mL beaker
    Use a 10 mL pipet to transfer 10 mL of the HCl to the 250 mL
    beaker
    Add a magnetic stir bar to the beaker and place it on a
    magnetic stirrer
    Set up the assembly as shown in figure 1
    Fill the buret with 0.1 M NaOH
    Setting Up Your LabQuest
    From the File Sensors Screen, select Mode
    This will bring up the mode menu
    Melting Point
    From the drop down menu under the mode function, select
    Events With Entry
    Enter volume for the name and mL for the unit
    This will change the x axis to display as volume, instead of time
    elapsed
    Collecting data
    Immerse the pH probe in the HCl
    solution and begin your data
    collection by pressing the play
    button in the bottom left corner.
    To create a new entry, select the
    Keep button. This will save
    your pH data and direct you to a
    new screen where you must
    enter the volume associated with
    the entry.
    The entry name should be the
    exact volume of NaOH added (to
    the nearest 0.05 mL).
    When the trial is finished
    Use the stock solution of HCL to neutralize the solution
    pH between 6.5 and 7.5
    Pour the solution down the drain
    Rinse the pH sensor, the buret, your 250 mL beaker, and the
    stir bar
    Examine your data
    Final Graph
    After neutralizing and disposing of your solution, examine the
    graph to find the volume at which the greatest change in pH
    is achieved.
    This is the equivalence point
    Acetic Acid Trial
    Repeat a trial using acetic acetic solution
    Use data from a neighbor for trial 2 of the two acids
    Special Considerations
    Goggles and gloves are to be worn at all times
    Make sure that the pH probes are immersed in the buffer
    solution when they are put back.
    NaOH is caustic. Handle with care.
    HCL is a corrosive acid. Handle with care
    Be sure to clean lab benches before leaving
    WASH YOUR HANDS BEFORE LEAVING

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