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Interfacial Strength of Plasma-sprayed Hydroxyapatite Coatings

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Abstract

Both tensile and shear adhesion strength tests were performed to evaluate interfacial strength between hydroxyapatite coatings on titanium alloy substrates subjected to anodization and heat treatment prior to deposition as well as post-deposition heat treatment. Results of the tensile adhesion strength tests were influenced by the size of the blasting media and the processing of pre- and post-heat treatments but not influenced by anodization. The finite element method (FEM) analysis of stress distribution during the shear adhesion strength test was also performed to evaluate the degree of stress singularity. The results show that the stress singularity parameters were dominant factors of stress distribution in the stress singularity fields, and they were also expected to influence the “essential” interfacial strength. In addition, the size of the blasting media had the same influence on the shear and tensile adhesion strength tests. This suggests the possibility of estimating tensile adhesion strength using the results of shear adhesion strength.

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Acknowledgments

This work was supported by Japan Thermal Spray Society research grant. We would like to express our gratitude of technical support to Niigata Metallikon Industries Corporation for preparing the specimens, Cybernet Systems Co., Ltd., for stress analysis, and we would like to thank Editage (www.editage.com) for English language editing.

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Authors and Affiliations

  1. Faculty of Engineering, Niigata University, Niigata, Japan

    Motofumi Ohki & Toshiki Hoshina

  2. Graduate School of Natural Science and Technology, Niigata University, Niigata, Japan

    Shogo Takahashi & Ran Jinnai

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  1. Motofumi Ohki
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  2. Shogo Takahashi
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  4. Toshiki Hoshina
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Correspondence to Motofumi Ohki.

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Ohki, M., Takahashi, S., Jinnai, R. et al. Interfacial Strength of Plasma-sprayed Hydroxyapatite Coatings. J Therm Spray Tech 29, 1119–1133 (2020). https://doi.org/10.1007/s11666-020-01041-6

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  • DOI: https://doi.org/10.1007/s11666-020-01041-6

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