... CD measurements CD spectra were recorded on Jobin-Yvon Dichrographs Mark 111 and V. D. Mark 1... more ... CD measurements CD spectra were recorded on Jobin-Yvon Dichrographs Mark 111 and V. D. Mark 111 is operated by an IBM AT computer. Spectograde solvents (Uvasol, E. Merck, Darmstadt) were used. Measurements were taken in 0.02-1.00 cm cells. Page 8. 948 ...
Journal of Liquid Chromatography & Related Technologies, 1999
Enantiomers of chiral spiro-λ-sulfanes with equatorial diaryl and axial bis(acyloxy), (alkoxy)-(a... more Enantiomers of chiral spiro-λ-sulfanes with equatorial diaryl and axial bis(acyloxy), (alkoxy)-(acyloxy) or (acylamino)-(acyloxy) S-substituents were separated on a Kromasil-based chiral sorbent, namely on O,O′-bis(3,5-dimethylbenzoyl)-N,N′- diallyl-L-tartardiamide silica CSP, by using n-hexane (or n-heptane) – dioxane (or 2-propanol) isocratically mixed mobile phases. Direct chiral separation was monitored by a home-made HPLC-CD system consisting of a circular dichroism (CD) spectrophotometer (Jobin-Yvon Model III
... CD measurements CD spectra were recorded on Jobin-Yvon Dichrographs Mark 111 and V. D. Mark 1... more ... CD measurements CD spectra were recorded on Jobin-Yvon Dichrographs Mark 111 and V. D. Mark 111 is operated by an IBM AT computer. Spectograde solvents (Uvasol, E. Merck, Darmstadt) were used. Measurements were taken in 0.02-1.00 cm cells. Page 8. 948 ...
Journal of Liquid Chromatography & Related Technologies, 1999
Enantiomers of chiral spiro-λ-sulfanes with equatorial diaryl and axial bis(acyloxy), (alkoxy)-(a... more Enantiomers of chiral spiro-λ-sulfanes with equatorial diaryl and axial bis(acyloxy), (alkoxy)-(acyloxy) or (acylamino)-(acyloxy) S-substituents were separated on a Kromasil-based chiral sorbent, namely on O,O′-bis(3,5-dimethylbenzoyl)-N,N′- diallyl-L-tartardiamide silica CSP, by using n-hexane (or n-heptane) – dioxane (or 2-propanol) isocratically mixed mobile phases. Direct chiral separation was monitored by a home-made HPLC-CD system consisting of a circular dichroism (CD) spectrophotometer (Jobin-Yvon Model III
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