The Sample Analysis at Mars (SAM) instrument on the Curiosity rover has detected evidence of oxyc... more The Sample Analysis at Mars (SAM) instrument on the Curiosity rover has detected evidence of oxychlorine compounds (i.e., perchlorates and chlorates) in Gale crater, which has implications for past habitability, diagenesis, aqueous processes, interpretation of in situ organic analyses, understanding the martian chlorine cycle, and hazards and resources for future human exploration. Pure oxychlorines and mixtures of oxychlorines with Mars-analog phases have been analyzed for their oxygen (O2) and hydrogen chloride (HCl) releases on SAM laboratory analog instruments in order to constrain which phases are present in Gale crater. These studies demonstrated that oxychlorines evolve O2 releases with peaks between ~200 and 600 °C, although the thermal decomposition temperatures and the amount of evolved O2 decrease when iron phases are present in the sample. Mg and Fe oxychlorines decompose into oxides and release HCl between ~200 and 542 °C. Ca, Na, and K oxychlorines thermally decompose ...
Metabolt is a portable soil incubator to characterize the metabolic activity of microbial ecosyst... more Metabolt is a portable soil incubator to characterize the metabolic activity of microbial ecosystems in soils. It measures the electrical conductivity, the redox potential, and the concentration of certain metabolism-related gases in the headspace just above a given sample of regolith. In its current design, the overall weight of Metabolt, including the soils (250 g), is 1.9 kg with a maximum power consumption of 1.5 W. Metabolt has been designed to monitor the activity of the soil microbiome for Earth and space applications. In particular, it can be used to monitor the health of soils, the atmospheric-regolith fixation, and release of gaseous species such as N2, H2O, CO2, O2, N2O, NH3, etc., that affect the Earth climate and atmospheric chemistry. It may be used to detect and monitor life signatures in soils, treated or untreated, as well as in controlled environments like greenhouse facilities in space, laboratory research environments like anaerobic chambers, or simulating facili...
We describe a versatile simulation chamber that operates under representative space conditions (p... more We describe a versatile simulation chamber that operates under representative space conditions (pressures from < 10−5 mbar to ambient and temperatures from 163 to 423 K), the SpaceQ chamber. This chamber allows to test instrumentation, procedures, and materials and evaluate their performance when exposed to outgassing, thermal vacuum, low temperatures, baking, dry heat microbial reduction (DHMR) sterilization protocols, and water. The SpaceQ is a cubical stainless-steel chamber of 27,000 cm3 with a door of aluminum. The chamber has a table which can be cooled using liquid nitrogen. The chamber walls can be heated (for outgassing, thermal vacuum, or dry heat applications) using an outer jacket. The chamber walls include two viewports and 12 utility ports (KF, CF, and Swagelok connectors). It has sensors for temperature, relative humidity, and pressure, a UV–VIS–NIR spectrometer, a UV irradiation lamp that operates within the chamber as well as a stainless-steel syringe for water v...
Tribocorrosion is a degradation phenomenon of material surfaces subjected to the combined action ... more Tribocorrosion is a degradation phenomenon of material surfaces subjected to the combined action of mechanical loading and corrosion attack caused by the environment. Although corrosive chemical species such as materials like chloride atoms, chlorides and perchlorates have been detected on the Martian surface, there is a lack of studies of its impact on materials for landed spacecraft and structures that will support surface operations on Mars. Here we present a series of experiments on the stainless-steel material of the ExoMars 2020 Rosalind Franklin rover wheels. We show how tribocorrosion induced by brines accelerate wear on the materials of the wheels. Our results do not compromise the nominal ExoMars mission but have implications for future long-term surface operations in support of future human exploration or extended robotic missions on Mars.
With no large-scale granitic continental crust, all environments on Mars are fundamentally derive... more With no large-scale granitic continental crust, all environments on Mars are fundamentally derived from basaltic sources or, in the case of environments such as ices, evaporitic, and sedimentary deposits, influenced by the composition of the volcanic crust. Therefore, the selection of samples on Mars by robots and humans for investigating habitability or testing for the presence of life should be guided by our understanding of the microbial ecology of volcanic terrains on the Earth. In this paper, we discuss the microbial ecology of volcanic rocks and hydrothermal systems on the Earth. We draw on microbiological investigations of volcanic environments accomplished both by microbiology-focused studies and Mars analog studies such as the NASA BASALT project. A synthesis of these data emphasises a number of common patterns that include: (1) the heterogeneous distribution of biomass and diversity in all studied materials, (2) physical, chemical, and biological factors that can cause het...
Autonomous exploration requires the use of movable platforms that carry a payload of instruments ... more Autonomous exploration requires the use of movable platforms that carry a payload of instruments with a certain level of autonomy and communication with the operators. This is particularly challenging in subsurface environments, which may be more dangerous for human access and where communication with the surface is limited. Subsurface robotic exploration, which has been to date very limited, is interesting not only for science but also for cost-effective industrial exploitation of resources and safety assessments in mines. Furthermore, it has a direct application to exploration of extra-terrestrial subsurface environments of astrobiological and geological significance such as caves, lava tubes, impact or volcanic craters and subglacial conduits, for deriving in-situ mineralogical resources and establishing preliminary settlements. However, the technological solutions are generally tailor-made and are therefore considered as costly, fragile and environment-specific, further hinderin...
Aeolian processes are believed to play a major role in the landscape evolution of Mars. Investiga... more Aeolian processes are believed to play a major role in the landscape evolution of Mars. Investigations on Martian aeolian landforms such as ripples, transverse aeolian ridges (TARs), and dunes, and aeolian sediment flux measurements are important to enhance our understanding of past and present wind regimes, the ongoing dust cycle, landscape evolution, and geochemistry. These aeolian bedforms are often comprised of loose sand and sharply undulating topography and thus pose a threat to mobility and maneuvers of Mars rovers. Here we present a first-hand account of the distribution, morphologies, and morphometrics of TARs in Oxia Planum, the recently selected ExoMars 2020 Rover landing site. The gridded mapping was performed for contiguous stretches of TARs within all the landing ellipses using 57 sub-meter high resolution imaging science experiment (HiRISE) scenes. We also provide the morphological descriptions for all types of TARs present within the landing ellipses. We use HiRISE d...
The Sample Analysis at Mars (SAM) instrument on the Curiosity rover has detected evidence of oxyc... more The Sample Analysis at Mars (SAM) instrument on the Curiosity rover has detected evidence of oxychlorine compounds (i.e., perchlorates and chlorates) in Gale crater, which has implications for past habitability, diagenesis, aqueous processes, interpretation of in situ organic analyses, understanding the martian chlorine cycle, and hazards and resources for future human exploration. Pure oxychlorines and mixtures of oxychlorines with Mars-analog phases have been analyzed for their oxygen (O2) and hydrogen chloride (HCl) releases on SAM laboratory analog instruments in order to constrain which phases are present in Gale crater. These studies demonstrated that oxychlorines evolve O2 releases with peaks between ~200 and 600 °C, although the thermal decomposition temperatures and the amount of evolved O2 decrease when iron phases are present in the sample. Mg and Fe oxychlorines decompose into oxides and release HCl between ~200 and 542 °C. Ca, Na, and K oxychlorines thermally decompose ...
Metabolt is a portable soil incubator to characterize the metabolic activity of microbial ecosyst... more Metabolt is a portable soil incubator to characterize the metabolic activity of microbial ecosystems in soils. It measures the electrical conductivity, the redox potential, and the concentration of certain metabolism-related gases in the headspace just above a given sample of regolith. In its current design, the overall weight of Metabolt, including the soils (250 g), is 1.9 kg with a maximum power consumption of 1.5 W. Metabolt has been designed to monitor the activity of the soil microbiome for Earth and space applications. In particular, it can be used to monitor the health of soils, the atmospheric-regolith fixation, and release of gaseous species such as N2, H2O, CO2, O2, N2O, NH3, etc., that affect the Earth climate and atmospheric chemistry. It may be used to detect and monitor life signatures in soils, treated or untreated, as well as in controlled environments like greenhouse facilities in space, laboratory research environments like anaerobic chambers, or simulating facili...
We describe a versatile simulation chamber that operates under representative space conditions (p... more We describe a versatile simulation chamber that operates under representative space conditions (pressures from < 10−5 mbar to ambient and temperatures from 163 to 423 K), the SpaceQ chamber. This chamber allows to test instrumentation, procedures, and materials and evaluate their performance when exposed to outgassing, thermal vacuum, low temperatures, baking, dry heat microbial reduction (DHMR) sterilization protocols, and water. The SpaceQ is a cubical stainless-steel chamber of 27,000 cm3 with a door of aluminum. The chamber has a table which can be cooled using liquid nitrogen. The chamber walls can be heated (for outgassing, thermal vacuum, or dry heat applications) using an outer jacket. The chamber walls include two viewports and 12 utility ports (KF, CF, and Swagelok connectors). It has sensors for temperature, relative humidity, and pressure, a UV–VIS–NIR spectrometer, a UV irradiation lamp that operates within the chamber as well as a stainless-steel syringe for water v...
Tribocorrosion is a degradation phenomenon of material surfaces subjected to the combined action ... more Tribocorrosion is a degradation phenomenon of material surfaces subjected to the combined action of mechanical loading and corrosion attack caused by the environment. Although corrosive chemical species such as materials like chloride atoms, chlorides and perchlorates have been detected on the Martian surface, there is a lack of studies of its impact on materials for landed spacecraft and structures that will support surface operations on Mars. Here we present a series of experiments on the stainless-steel material of the ExoMars 2020 Rosalind Franklin rover wheels. We show how tribocorrosion induced by brines accelerate wear on the materials of the wheels. Our results do not compromise the nominal ExoMars mission but have implications for future long-term surface operations in support of future human exploration or extended robotic missions on Mars.
With no large-scale granitic continental crust, all environments on Mars are fundamentally derive... more With no large-scale granitic continental crust, all environments on Mars are fundamentally derived from basaltic sources or, in the case of environments such as ices, evaporitic, and sedimentary deposits, influenced by the composition of the volcanic crust. Therefore, the selection of samples on Mars by robots and humans for investigating habitability or testing for the presence of life should be guided by our understanding of the microbial ecology of volcanic terrains on the Earth. In this paper, we discuss the microbial ecology of volcanic rocks and hydrothermal systems on the Earth. We draw on microbiological investigations of volcanic environments accomplished both by microbiology-focused studies and Mars analog studies such as the NASA BASALT project. A synthesis of these data emphasises a number of common patterns that include: (1) the heterogeneous distribution of biomass and diversity in all studied materials, (2) physical, chemical, and biological factors that can cause het...
Autonomous exploration requires the use of movable platforms that carry a payload of instruments ... more Autonomous exploration requires the use of movable platforms that carry a payload of instruments with a certain level of autonomy and communication with the operators. This is particularly challenging in subsurface environments, which may be more dangerous for human access and where communication with the surface is limited. Subsurface robotic exploration, which has been to date very limited, is interesting not only for science but also for cost-effective industrial exploitation of resources and safety assessments in mines. Furthermore, it has a direct application to exploration of extra-terrestrial subsurface environments of astrobiological and geological significance such as caves, lava tubes, impact or volcanic craters and subglacial conduits, for deriving in-situ mineralogical resources and establishing preliminary settlements. However, the technological solutions are generally tailor-made and are therefore considered as costly, fragile and environment-specific, further hinderin...
Aeolian processes are believed to play a major role in the landscape evolution of Mars. Investiga... more Aeolian processes are believed to play a major role in the landscape evolution of Mars. Investigations on Martian aeolian landforms such as ripples, transverse aeolian ridges (TARs), and dunes, and aeolian sediment flux measurements are important to enhance our understanding of past and present wind regimes, the ongoing dust cycle, landscape evolution, and geochemistry. These aeolian bedforms are often comprised of loose sand and sharply undulating topography and thus pose a threat to mobility and maneuvers of Mars rovers. Here we present a first-hand account of the distribution, morphologies, and morphometrics of TARs in Oxia Planum, the recently selected ExoMars 2020 Rover landing site. The gridded mapping was performed for contiguous stretches of TARs within all the landing ellipses using 57 sub-meter high resolution imaging science experiment (HiRISE) scenes. We also provide the morphological descriptions for all types of TARs present within the landing ellipses. We use HiRISE d...
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