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2010 •
2012 •
Molbank
5,5'-(1,4-Phenylenedimethylylidene)bis(1,3-diethyl-2-thioxodihydropyrimidine-4,6(1H,5H)-dione)2010 •
2010 •
2018 •
A derivative of dihydrotetrazolopyrimidine has been successfully synthesized through a cyclocondensation reaction between a chalcone derivative with 5-aminotetrazole. The molecular structure of the title compound was established based on Fourier transform infrared spectra (FTIR), high-resolution mass spectrometry (HRMS), 1D and 2D nuclear magnetic resonance (NMR) spectrum.
Acta Crystallographica Section E Crystallographic Communications
The crystal structure of 1,5-dibenzyl-1 H -pyrazolo[3,4- d ]pyrimidine-4(5 H )-thione2015 •
In the title compound, C19H16N4S, the pyrazolo[3,4-d]pyrimidine ring is close to being planar, with the greatest deviation from the mean plane being 0.023 (2) Å for the C atom bearing the thione S atom. The two phenyl rings are nearly perpendicular to the fused ring system [dihedral angles = 71.4 (2) and 78.1 (2)°], but are oriented in opposite directions; the dihedral angle between the phenyl rings is 32.22 (16)°. In the crystal, linear supramolecular chains along [101] are sustained by C—H...S interactions.
Pyrimidine derivatives are most useful compounds among all the heterocyclic compounds for medicines and other various applications. Some newer pyrimidine derivatives eg. 6-methyl-4-(3-phenyl-pyridin-4-yl-methanone-1-H-pyrazol)-2-thio-N-substituted phenyl pyrimide-5-carboxamide (III a-j) have been synthesized by one pot synthesis from 3-phenyl-1-(pyridin-4-ylcarbonyl)-1-H-pyrazole-4-carbaldehyde, substituted aceto-acetanilide and urea/thiourea in acidic medium. The reactions were carried out based on well known name reaction Biginelli reaction (Aldehyde, diketo compound and urea/ thiourea).The synthesized compounds (III a-j) have been purified by column chromatography and characterized by spectroscopic technique like IR, 1H NMR and mass spectroscopy. Preparation methods for preparation of newer aldehyde 3-phenyl-1-(pyridin-4-ylcarbonyl)-1H-pyrazole-4-carbaldehyde newer dihydropyridine derivatives (III a-j) and Solvent system/ methods for the column chromatography have been discussed in this paper with physical properties of compounds (III a-j).
Acta crystallographica. Section E, Structure reports online
2-[5-(2-Methyl-phen-yl)-3-(2-methyl-styryl)-4,5-di-hydro-1H-pyrazol-1-yl]-6-(thio-phen-2-yl)-4-(tri-fluoro-meth-yl)pyrimidine chloro-form monosolvate2014 •
In the crystal structure of the title compound, C28H23F3N4S·CHCl3, the chloro-form solvate mol-ecules connect the pyrimidine mol-ecules into chains along [101] through weak C-H⋯N and C-H⋯Cl hydrogen-bond inter-actions. There are further connections between adjacent chains through F⋯Cl halogen contacts of 3.185 (3) Å, with the -CF3 group presenting a significant short F⋯F inter-chain distance of 2.712 (4) Å. The five-membered pyrazole ring is approximately planar (r.m.s. deviation = 0.050 Å). The pyrimidine ring makes dihedral angles of 84.15 (8) and 4.56 (8)° with the benzene rings.
2011 •
Rethinking Marxism
Which Materialism and What Matter? Rethinking Marxism from a Materialist-Feminist Perspective2024 •
New Blackfriars
Facing a Liturgy-Starved Church: Do We Need to Think Afresh About the Basics of Ministry2019 •
Remote Sensing
The Discovery of a Buried Temple in Paestum: The Advantages of the Geophysical Multi-Sensor Application2020 •
2023 •
Transplantation Journal
Outcome of High Volume Live Related Renal Transplants in a Developing Country2010 •
2019 •
Parathënie: Lucia Nadin-Aurel Plasari, Barleti i hershëm
Parathënie: Lucia Nadin-Aurel Plasari, Barleti i hershëm2022 •
2018 •
Bioorganic & Medicinal Chemistry Letters
A solid-phase approach to analogues of the antibiotic mureidomycin2000 •
Information Technology Journal
Secure E-commerce Web Development Framework2011 •
Opera in linguistica ukrainiana
Nominative Space of the Concept Parents in Hutsul Linguistic World-Image