J. Compos. Sci., Volume 8, Issue 11 (November 2024) – 35 articles

This paper presents a modified finite element analysis (FEA) model for predicting the axial compression strength of large-diameter concrete-filled steel tubular (CFST) stub columns, addressing the gap in research that has often focused on smaller diameters. The size effect, which significantly impacts the structural performance of large-diameter CFST columns, is a key focus of this study. The goal is to validate the accuracy and reliability of the modified FEA model by comparing its predictions with experimental data from the literature, specifically examining ultimate axial load capacity, failure modes, and deformed shapes. In addition to validating the model, this study includes a comprehensive parametric analysis that explores how critical geometric parameters such as the diameter-to-thickness (D/t) ratio and length-to-diameter (L/D) ratio affect the axial compressive behavior of CFST stub columns. By systematically varying these parameters, the research provides valuable insights into the load-bearing capacity, deformation characteristics, and failure mechanisms of CFST columns. Furthermore, the material properties of the steel tube—particularly its yield strength—and the compressive strength of the concrete core are investigated to optimize the design and safety performance of these columns. The results indicate that the FEA model shows excellent agreement with experimental results, accurately predicting the axial load-strain response. It was observed that as the diameter of the steel tube increases, the peak stress, peak strain, strength index, and ductility index tend to decrease, underscoring the size effect. Conversely, an increase in the yield strength and thickness of the steel tube enhances the ultimate strength of the CFST columns. These findings demonstrate the reliability of the modified FEA model in predicting the behavior of large-diameter CFST columns, offering a useful tool for optimizing designs and improving safety margins in structural applications. Full article

Carbon fiber-reinforced polymer (CFRP), noted for its outstanding properties including high specific strength and superior fatigue resistance, is increasingly employed in aerospace and other demanding applications. This study investigates the interactions between CFRP composites and high-energy lasers (HEL), with continuous wave laser powers reaching up to 120 kW. A novel automated sample exchange system, operated by a robotic arm, minimizes human exposure while enabling a sequence of targeted laser tests. High-speed imaging captures the rapid expansion of a plume consisting of hot gases and dust particles during the experiment. The research significantly advances empirical models by systematically examining the relationship between laser power, perforation times, and ablation rates. It demonstrates scalable predictions for the effects of high-energy laser radiation. A detailed examination of the damaged samples, both visually and via micro-focused computed X-ray tomography, offers insights into heat distribution and ablation dynamics, highlighting the anisotropic thermal properties of CFRP. Compression after impact (CAI) tests further assess the residual strength of the irradiated samples, enhancing the understanding of CFRP’s structural integrity post-irradiation. Collectively, these tests improve the knowledge of the thermal and mechanical behavior of CFRP under extreme irradiation conditions. The findings not only contribute to predictive modeling of CFRP’s response to laser irradiation but enhance the scalability of these models to higher laser powers, providing robust tools for predicting material behavior in high-performance settings. Full article

The objective of the experimental analysis was to assess the impact of the reuse of technological waste (recyclate) on the selected performance properties of the fibrous polymer composite used to produce components for the automotive industry by injection molding technology. Polyphthalamide (PPA), which belongs to a group of high-tech polymers, was chosen as the analyzed material. In accordance with the set goals, the rheological, mechanical, and structural properties of the material were evaluated using ANOVA analysis in the experimental part of the work, depending on the mass ratio of the recycled material added to the virgin material. The influence of the proportion of recycled material on the lifetime of moldings by the method of their exposure at an elevated temperature for a defined time was also assessed. During the research, it was found that at a concentration of up to 40 wt. % of recyclate, its mechanical properties do not change significantly. At a concentration of 50 wt. %, there is a rapid decrease in mechanical properties. In the long term, it can also be said that the addition of recyclate significantly affects the service life of the components. No significant changes in morphology were observed during the analysis of structural properties. Full article

Nanocrystalline mullite was synthetized by annealing a highly porous 3D structure consisting of nanofibrous aluminum oxyhydroxides treated with ethoxysilanes. The chemical, structural, and phase transformations in the aluminosilicate nanosystem were studied in the temperature range between 100 and 1600 °C. The features of the solid-phase synthesis of mullite at the interface of crystalline alumina with a liquid silica layer are discussed. It was established that chemical modification of the alumina surface with ethoxysilanes significantly limits the interphase mass transport and delays the phase transformation of the amorphous oxide into γ-Al₂O₃, which begins at temperatures above 1000 °C, while the basic structural nanofibrils are already crystallized at ~850 °C. The formation of mullite was completed at temperatures ≥ 1200 °C, where the fraction of γ-Al₂O₃ sharply decreased. Full article

The adoption of prefabricated elements and systems (PBES) in accelerating bridge construction (ABC) and rapidly replacing aging infrastructure has attracted considerable attention from bridge authorities. These prefabricated components facilitate quick assembly, which diminishes the environmental footprint at the construction site, alleviates delays and lane closures, reduces disruption for the traveling public, and ultimately conserves both time and taxpayer resources. The current paper explores the structural behavior of a reinforced concrete (RC) precast full-depth deck panel (FDDP) having 175 mm projected glass-fiber-reinforced polymer (GFRP) bars embedded into a 200 mm wide closure strip filled with ultra-high-performance fiber-reinforced concrete (UHPFRC). Three joint details for moment-resisting connections (MRCs), named the angle joint, C-joint, and zigzag joint, were constructed and loaded to collapse. The controlled slabs and mid-span-connected precast FDDPs were statically loaded to collapse under concentric or eccentric wheel loading. The moment capacity of the controlled slab reinforced with GFRP bars compared with the concrete slab reinforced with steel reinforcing bars was less than 15% for the same reinforcement ratio. The precast FDDPs showed very similar results to those of the controlled slab reinforced with GFRP bars. The RC slab reinforced by steel reinforcing bars failed in the flexural mode, while the slab reinforced by GFRP bars failed in flexural-shear one. Full article

Piezoresistive sensors composed of nickel nanostrands, nickel-coated carbon fibers, and silicone can be used to measure large physical deflections but exhibit viscoelastic properties and creep, leading to a complex and nonlinear electrical response that is difficult to interpret. This study considers the impact of modifying the geometry and architecture of the sensors on their mechanical and electrical performance. Varying the sensor thickness leads to potentially significant differences in conductive fiber alignment, while adding external layers of pure silicone provides elastic support for the sensors, potentially reducing their extreme viscoelastic nature. The impact of such modifications on both mechanical and electrical behavior was assessed by analyzing strain to failure, the magnitude of hysteresis with cycling, the repeatability of the electro-mechanical response, the strain level at which resistance begins to monotonically decrease, and the drift in electrical response with cycling. The results indicate that thicker single-layer sensors have less electrical drift. Sensors with a multilayered architecture exhibit several improvements in behavior, such as increasing the range of the monotonic region by approximately 52%. These improvements become more significant as the thickness of the pure silicone layers increases. Full article

Carbon-reinforced polymer composites form an important category of advanced materials, and there is an increasing demand to enhance their performance using more convenient and scalable processes at low costs. In the present study, graphitic flakes were prepared by the mechanical exfoliation of synthetic graphite electrodes and utilized as an abundant and potentially low-cost filler to fabricate epoxy-based composites with different additive ratios of 1–10 wt.%. The morphological, structural, thermal, and mechanical properties of these composites were investigated. It was found that the thermal conductivity of the composites increases by adding graphite, and this increase mainly depends on the ratio of the graphite additive. The addition of graphite was found to have a diverse effect on the mechanical properties of the composites: the tensile strength of the composites decreases with the addition of graphite, whilst their compressive strength and elastic modulus are enhanced. The results demonstrate that incorporating 5 wt% of commercially available graphite into epoxy not only raises the thermal conductivity of the material from 0.223 to 0.485 W/m·K, but also enhances its compressive strength from 66 MPa to 72 MPa. The diverse influence of graphite provides opportunities to prepare epoxy composites with desirable properties for different applications. Full article

In this study, a “green composite” material made from 60% tree bark and 40% polylactic acid (PLA) was fabricated and evaluated according to its mechanical properties and biodegradability. Biodegradation tests were performed in compost, simulated aquatic environments, and natural soil. In compost, the composite degraded steadily and reached 47% biodegradation after 11 weeks. In soil, the material quickly lost much of its tensile strength, and after 6 weeks, there were signs that the surface and the internal structure had started to deform. Biodegradation in aquatic environments also caused a loss of tensile strength after only a few weeks. Because of the high filler content, excellent biodegradability, and light weight, the composite material has a low environmental footprint. The material could be used in agricultural equipment such as plant pots. Full article

This work studied biocomposites based on a blend of low-density polyethylene (LDPE) and the ethylene–vinyl acetate copolymer (EVA), filled with 30 wt.% of cellulosic components (microcrystalline cellulose or wood flour). The LDPE/EVA ratio varied from 0 to 100%. It was shown that the addition of EVA to LDPE increased the elasticity of biocomposites. The elongation at break for filled biocomposites increased from 9% to 317% for microcrystalline cellulose and from 9% to 120% for wood flour (with an increase in the EVA content in the matrix from 0 to 50%). The biodegradability of biocomposites was assessed both in laboratory conditions and in open landfill conditions. The EVA content in the matrix also affects the rate of the biodegradation of biocomposites, with an increase in the proportion of the copolymer in the polymer matrix corresponding to increased rates of biodegradation. Biodegradation was confirmed gravimetrically by weight loss, an X-ray diffraction analysis, and the change in color of the samples after exposition in soil media. The prepared biocomposites have a high potential for implementation due to the optimal combination of consumer properties. Full article

We propose a new type of flexible transistor based on carbon-nanotube (CNT) composite thread (CNTCT), i.e., a thread transistor, with ionic gel. In our previous study, we demonstrated that transistor operation was possible by combining metallic and semiconducting CNTCTs as gate and channel with an insulating material. However, its performance was not sufficient. Therefore, we here aim to improve it. For this, we tried to apply ionic gel as a dielectric layer to it. With this, the transistor was expected to be an electric-double-layer transistor. The transistor performance was improved, and the on/off ratio of the transistor increased by more than 4. This is a large value compared to our previous work. In addition, we not only evaluated the performance of the transistors, but also investigated whether they could be used as logic circuits. It was confirmed that the logic circuit composed of the thread transistor also operated correctly and stably for a long period of time. It was also confirmed that the output changed in response to weak external forces. These results indicate that it is a flexible transistor that can be used in a wide range of applications such as logic circuits and sensors. Full article

The development of high-performance composites for mechanical energy dissipation during impact or explosive events is of vital importance for the safety of personnel and infrastructures. Solid–liquid composites are an emerging class of energy absorbers where a liquid-phase filler is seamlessly integrated into a solid matrix to enhance the impact resistance of the protection target. This innovative approach leverages the distinct properties of both phases and the unique interactions between them to achieve superior performance under high-impact conditions. This paper aims to review the liquid-phase materials used in solid–liquid composites, ranging from neat liquids to complex fluids, including liquid nanofoam and shear-thickening fluids, to provide an in-depth analysis of the fundamental physics underpinning the resulting solid–liquid composites, and to explore how their unique properties contribute to enhanced impact resistance and energy absorption. Furthermore, this paper evaluates the advantages and limitations of these solid–liquid composites and offers insights into future directions for the development of solid–liquid composites in various fields, including personal protective equipment, automotive safety systems, and structural protection. Full article

In this study, the wear behavior of AA7075/silicon carbide/fly ash hybrid surface composites processed with a clean and green friction stir processing technique was investigated. The microstructure of the composites was investigated to determine the particle dispersion. Wear tests using a pin-on-disc tribometer were conducted, and wear tracks and debris analyses were conducted using scanning electron microscopic imaging, EDX, and mapping. The wear rate of the composites was higher in the case of the composites with agglomerated zones, which led to the loose SiC/fly ash particles pulling out during the action of dry sliding. However, on the other hand, the wear resistance was improved in the composites with uniformly distributed SiC/fly ash particles. The hard SiC/fly ash particles acted as optimized load-bearing asperities and induced more wear resistance during the action of dry sliding against the mating plate, which was made of mild steel. In the case of the well-dispersed composites, the wear mechanisms shifted from fretting fatigue and adhesion to abrasion. The presence of a high Fe content in the wear debris was confirmed in the most wear-resistant composite sample, S-20, which was produced with the following parameters: tool rotation (w) of 1000 rpm, tool traverse (v) of 40 mm/min, hybrid ratio (HR) of 75:25, and a volume percentage of reinforcements (vol.%) of 8. Full article

Cancer remains one of the most critical global health issues. Conventional treatments, such as radiotherapy, surgery, or chemotherapy, have limitations, especially concerning side effects, resistance, and recurrence. Consequently, new innovative treatments to overcome these problems are needed. Photothermal therapy (PTT) is a promising alternative that uses photothermal agents that convert near-infrared light (NIR) into heat to kill cancer cells. Nanoparticles can be used as photothermal agents and also as drug delivery platforms, improving the drugs’ stability, allowing for targeted delivery, and reducing toxicity. Due to its broad absorption band, high surface area, and versatility for surface functionalization, tungsten disulfide (WS₂) has high potential in this context. This paper presents the state-of-the-art on the use of WS₂-based materials to achieve effective and biocompatible new anticancer treatment strategies. Full article

Carbon fiber-reinforced epoxy (CF/EP) composites are attractive materials for hydrogen storage tanks due to their high strength-to-weight ratio and outstanding chemical resistance. However, cryogenic temperatures (CTs) have a substantial impact on the tensile strength and interfacial bonding of CF/EP materials, producing problems for their long-term performance and safety in hydrogen storage tank applications. This review paper investigates how low temperatures affect the tensile strength, modulus, and fracture toughness of CF/EP materials, as well as the essential interfacial interactions between carbon fibers (CFs) and the epoxy matrix (EP) in cryogenic environments. Material toughening techniques have evolved significantly, including the incorporation of nano-fillers, hybrid fibers, and enhanced resin formulations, to improve the durability and performance of CF/EP materials in cryogenic conditions. This review also assesses the hydrogen barrier properties of various composites, emphasizing the importance of reducing hydrogen permeability in order to retain material integrity. This review concludes by highlighting the importance of optimizing CF/EP composite design and fabrication for long-term performance and safety in hydrogen storage systems. It examines the prospects for using CF/EP composites in hydrogen storage tanks, as well as future research directions. Full article

Amid the shift away from fossil fuels, third-generation perovskite solar cells (PSCs) have become pivotal due to their high efficiency and low production costs. This review concentrates on semi-transparent perovskite solar cells (ST-PSCs), highlighting their power conversion efficiency (PCE) and average visible transmittance (AVT). We address strategies to optimize ST-PSC performance, tackling inherent challenges, such as optical losses from reflection, parasitic absorption, and thermalization loss, which impact the operational efficiency under variable environmental conditions. ST-PSCs are distinguished by their lightweight, flexible, and translucent properties, allowing for diverse applications in urban building integration, agricultural greenhouses, and wearable technology. These cells integrate seamlessly into various settings, enhancing energy harnessing without compromising on aesthetic or structural elements. However, the scalability of ST-PSCs involves challenges related to stability and efficiency in large-scale deployments. The tropical urban landscape of Singapore provides a unique case study for ST-PSC application, blending architectural aesthetics with high solar irradiance to optimize energy efficiency. While the potential for ST-PSCs to contribute to sustainable urban development is immense, significant technological hurdles must be overcome to realize their full potential. Continued advancements in material science and engineering are essential to address these challenges, ensuring the scalability and long-term deployment of ST-PSCs in global energy solutions. Full article

Hydrogels play a crucial role due to their high-water content and 3D structure, which make them ideal for various applications in biomedicine, sensing, and beyond. They can be prepared from a variety of biomaterials, polymers, and their combinations, allowing for versatility in properties and applications. Hydrogels include natural types derived from collagen, gelatin, alginate, and hyaluronic acid, as well as synthetic types based on polyethylene glycol (PEG), polyvinyl alcohol (PVA), and polyacrylamide (PAAm). Each type possesses distinct properties, such as mechanical strength, biodegradability, and biocompatibility, which can be tailored for applications such as wound healing, contact lenses, 3D bioprinting, and tissue engineering. The high-water content of hydrogels mimics natural tissue environments, promoting cell growth and allowing nutrient and waste exchange, which supports the development of functional tissues. They serve as scaffolds in tissue engineering applications, including wound healing, cartilage and bone regeneration, vascular tissue engineering, and organ-on-a-chip systems. Additionally, hydrogels can encapsulate and deliver therapeutic agents, such as growth factors or drugs, to specific target sites in the body. Hydrogels can be prepared through three primary methods: physical crosslinking, which relies on non-covalent interactions such as physical entanglements or hydrogen bonding; chemical crosslinking, which forms covalent bonds between polymer chains to create a stable structure; and irradiation-based crosslinking, where UV irradiation induces rapid hydrogel formation. The choice of crosslinking method depends on the desired properties and applications of the hydrogel. By providing a biomimetic environment, hydrogels facilitate cell growth and differentiation, support tissue formation, and aid in the regeneration of damaged or diseased tissues while delivering therapeutic agents. This review focuses on the critical advancements in processing routes for hydrogel development, summarizing the characterization and application of hydrogels. It also details key applications, including wound healing and cartilage and bone regeneration, as well as the challenges and future perspectives in the field. Full article

Pervious concrete, because of its high porosity, is a suitable material for reducing the effects of water precipitations and is primarily utilized in road pavements. In this study, the effects of binder-to-aggregate (B/A) ratios, as well as mineral admixtures with and without polypropylene fibers (PPFs) (0.2% by volume), including fly ash (FA) or silica fume (SF) (10% by substitution of cement), on the mechanical properties and durability of pervious concrete were experimentally observed. The experimental campaign included the following tests: permeability, porosity, compressive strength, splitting tensile strength, and flexural strength tests. The durability performance was evaluated by observing freeze–thaw cycles and abrasion resistance after 28 d curing. X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), thermal analysis (TGA-DTA), and scanning electron microscopy (SEM) combined with energy dispersive spectroscopy (EDS) were employed to investigate the phase composition and microstructure. The results revealed that, for an assigned B/A ratio identified as optimal, the incorporation of mineral admixtures and fibers mutually compensated for their respective negative effects, resulting in the effective enhancement of both mechanical/microstructural characteristics and durability properties. In general, pervious concrete developed with fly ash or silica fume achieved higher compressive strength (>35 MPA) and permeability of 4 mm/s, whereas the binary combination of fly ash or silica fume with 0.2% PPFs yielded a flexural strength greater than 6 MPA and a permeability of 6 mm/s. Silica fume-based pervious concrete exhibited excellent performance in terms of freeze–thaw (F-T) cycling and abrasion resistance, followed by fiber-reinforced pervious concrete, except fly ash-based pervious concrete. Microstructural analysis showed that the inclusion of fly ash or silica fume reduced the harmful capillary pores and refined the pore enlargement caused by PPFs in the cement interface matrix through micro-filling and a pozzolanic reaction, leading to improved mechanical and durability characteristics of pervious concrete. Full article

The process-induced deformation (PID) during the manufacturing of thermosetting composite materials can significantly compromise manufacturing precision. This paper introduces an innovative method that combines a finite element analysis (FEA), feature classification algorithms, and an Artificial Neural Network (ANN) framework to rapidly predict the PID of a typical L-shaped structure. Initially, a comprehensive range of parameters that influence PID are compiled in this research, followed by the generation of a dataset through FEA considering viscoelastic constitutive models, validated by experimental results. Influential parameters are classified using Random Forest and LASSO regression methods, with each parameter rated according to its impact on PID, delineating their varying degrees of importance. Subsequently, through a hyperparameter analysis, an ANN framework is developed to rapidly predict the PID, while also refining the assessment of the parameters’ significance. This innovative approach achieves a computational time reduction of 98% with less than a 5% loss in accuracy, and highlights that under limited computational conditions, considering only a subset or all of the parameters—the peak temperature, corner angle, coefficient of chemical shrinkage, coefficient of thermal expansion, curing pressure, and $E_1$—minimizes accuracy loss. The study demonstrates that machine learning algorithms can effectively address the challenge of predicting composite material PID, providing valuable insights for practical manufacturing applications. Full article

Wood–Textile Composites (WTCs) are a new type of composite material based on willow wood strips and polypropylene that combines the properties of classic natural-fiber-reinforced polymers with an innovative textile wood design. While the basic quasi-static properties have already been investigated and described, there is a lack of knowledge about the behavior of the material under dynamic-cyclic and dynamic-impact loading as well as in relation to basic wood construction parameters. The present study is intended to contribute to the later use of the developed material, e.g., in architecture. For this purpose, fatigue tests, dart drop tests (impact and penetration), impact bending tests, and embedment tests were carried out. It was shown that embedding wood fabrics in a thermoplastic matrix leads to a significant increase in resistance to impact loads compared to the neat basic materials. It was also shown that the ratio of the failure stress in the fatigue test to the tensile strength of the WTC corresponds to that of other fiber-reinforced thermoplastics at around 70%. The embedment tests showed that WTC has good values compared to neat wood. Full article

Radiative cooling, an emerging technology that reflects sunlight and emits radiation into outer space, has gained much attention due to its energy-efficient nature and broad applicability in buildings, photovoltaic cells, and vehicles. This study focused on fabricating SiO₂-polymethyl methacrylate (PMMA) and TiO₂-SiO₂-PMMA thick films via the blade-coating method. The investigation aimed to improve cooling performance by adding TiO₂ particles to increase the coverage area and utilize the TiO₂ reflectance ability. The characterizations of the emissivity/absorptivity, solar reflectance, and microstructure of the thick films were conducted by using ultraviolet–visible/near-infrared (UV-Vis/NIR) diffuse reflection spectroscopy and scanning electron microscopy, respectively. Experimental results revealed that the maximum temperature drops of approximately 9.4 and 9.8 °C were achieved during the daytime period for SiO₂-PMMA and TiO₂-SiO₂-PMMA thick films. The total solar radiation reflectivity increased from 71.7 to 75.6% for SiO₂-PMMA radiative cooling thick films after adding TiO₂. These findings underscored the potential of TiO₂-SiO₂-PMMA thick films in advancing radiative cooling technology and cooling capabilities across various applications. Full article

This work presents the extrusion-based preparation of new biocomposites from two plant fibres (namely Cannabis sativa L. and Opuntia ficus-indica Mill.) that are added to two different polymers (an ethylene–octene elastomer and polylactic acid), which act as matrices. Structural and morphological characterization (using X-ray diffraction and field emission scanning electron microscopy) have been used to correlate the interactions between the biomass and the polymers employed with the efficiency of the proposed approach. It was found that Opuntia-based composites can be easily formed in a range of biomass/polymer ratios. However, the interaction between hemp and the matrix means that only specific ratios can form tightly bound composites. The present communication thus paves the way for more complex and comprehensive studies on the formulation of biocomposites containing these matrices. Full article

The delayed failure of SiC fibers is commonly described by a power law relating the growth rate to the stress intensity factor K_I, itself following the classical fracture mechanics law with a constant geometrical factor. For low stress levels, relevant for ceramic matrix composite (CMC) applications, this model predicts crack lengths exceeding the specimen size and unrealistic times to failure. Indeed, discrepancies between this model prediction and experiments have been reported. This paper proposes a model improvement with a simple and accessible analytical solution to work around this shortcoming. First, a more accurate description of fracture mechanics is introduced which yields physically reasonable estimates of the crack size at failure. Then, the contribution of silica scale formation to oxidation embrittlement (OE) is evaluated. If the corrected slow crack growth (SCG) model and the OE model are irrelevant when taken separately, their simultaneous presence accurately depicts the observations: OE prevails under low stresses, resulting in a finite lifetime below 150 MPa, whereas SCG takes over above 800 MPa. This result brings new insight for the design of CMC and may as well apply to other types of materials, prone to environment-assisted and stress-accelerated degradation. Full article

Enhancing the fracture strength and ductility of concrete through the incorporation of various types of synthetic and natural fibers with varying textures and contents remains challenging. Natural fibers, being versatile and eco-friendly construction materials, can be an excellent alternative to synthetic fibers. However, studies on natural fiber-reinforced (especially through the incorporation of jute fibers) novel composites like geopolymer binders remain deficient. Thus, the effects of various lengths (15, 25 and 35 mm) and volume contents (0.10, 0.20, 0.30, 0.40, 0.50, 0.60, and 0.70%) of natural jute fibers on the mechanical performance of fiber-reinforced geopolymer concrete were studied. The results revealed that jute fiber reinforcement remarkably affected the workability, compressive strength, fracture strengths, water absorption and microstructure properties of the proposed geopolymer concretes. Increasing the fiber length and volume fractions in the geopolymer matrix lowered the slump values and workability and increased the compressive strength. The specimen prepared with a fiber length of 35 mm and volume fractions of 0.70% displayed the lowest slump value (28 mm) and highest compressive strength (31.5 MPa) at 28 days. In addition, the specimens made with fiber volume fractions of 0.10, 0.20, 0.30, and 0.40% showed a significant improvement in the splitting tensile and flexural strengths. However, increasing the volume of the jute fibers up to 0.50% led to a slight drop in the fracture strength of the geopolymers. The specimens prepared with a length of 25 mm and a volume of 0.40% achieved the highest enhancement of splitting tensile strength (18.7%) and flexural strength (29.1%) at 28 days. In short, sustainable geopolymer concrete with high fracture performance can be obtained by incorporating natural jute fibers, leading to practical applications in the construction sector. The proposed green concrete may enable a reduction in solid waste, thus promoting a more sustainable concrete industry. Full article

This study aims to evaluate the mechanical behavior, by ways of the FEM, of three femoral stems made of a Ti-6Al-4V titanium alloy with transverse holes in the proximal zone and a stem made of a β-type titanium alloy with a stiffness varying from 65 GPa in the proximal zone to 110 GPa in the distal zone and the CFRP composite material. The purpose of the study was to evaluate the effect of stress shielding on an intact femoral bone. A three-dimensional model of the intact femur was created, and the three prostheses were inserted with perfect stem bone fit. Applying constraint conditions such as fixation in all directions of the distal part of the femur and the application of a static load simulating standing still during a gait cycle allowed the stresses of both the implants and the bone to be compared. Evaluating the stress shielding for the three proposed materials was possible by identifying the seven Gruen zones. We can see from the results obtained that the metal alloys produced observable stress shielding in all the Gruen zones. There was a difference for the β-type alloy which, as a result of its stiffness variation from the proximal to the distal zone, did not show any level of stress shielding in Gruen zones 1 and 2. The CFRP composite, in contrast, showed no stress shielding in all of the Gruen zones and is an excellent material for the fabrication of total hip replacements. Further in vitro and in vivo validation studies are needed to make the modeling more accurate and understand the biological effects of the use of the three materials. Full article

This work presents radial basis function collocation methods in pseudospectral form for forecasting the static deformations and free vibration characteristics of thin and thick cross-ply laminated shells. This method utilizes an innovative layerwise shallow shell theory that integrates both translational and rotational degrees of freedom. A collection of numerical examples illustrates the precision and efficacy of the suggested numerical method, highlighting its capability in resolving static and vibrational issues. Full article

Thermoplastic composites have become increasingly popular due to their numerous benefits. To enhance the performance of fiber-reinforced thermoplastic composites, many research efforts have been made using various types of fillers. However, the high melting temperature and viscosity of thermoplastic polymer melt present a primary challenge in achieving uniform filler dispersion. Interply strengthening is one of the simplest and most cost-effective techniques for addressing this challenge. This study utilized micro-size core-shell particles that were dispersed using a sieve. The particles were carefully sprinkled onto the sieve, facilitating their controlled dispersion at the ply interface, after which fabric and thermoplastic films were laid on top. The resulting stacked arrangement was then processed using a hot consolidation cycle via compression molding to produce composite laminate. The impact of incorporating core-shell particles on the mechanical performance of carbon fiber-reinforced polyamide 6 (CF/PA6) laminates was investigated. Results showed that adding 4 wt% core-shell particles led to a maximum improvement of 58.99%, 25.62%, 41.56%, and 47.83% in flexural strength and modulus, interply shear strength, and compression strength, respectively, compared to the pristine composites. Stress-strain curves confirmed that the core-shell particles delayed matrix and interlaminar crack propagation. Furthermore, micrographic images indicated improved interaction of CSPs at the ply interfaces. These findings can improve the interply strength of thermoplastic composites and assist designers in achieving higher performance. Full article

The present study investigates the synthesis and characterization of a zirconium oxide (ZrO₂)-based metal composite doped with cerium (Ce) and yttrium (Y), using chromium (Cr) and nickel (Ni) as base metals. These constituents were selected for their superior mechanical properties and compatibility with the ceramic phase. High-purity powders were homogenized via high-energy ball milling, followed by cold pressing and sintering in a controlled atmosphere of hydrogen. The sintering process was conducted at temperatures ranging from 850 °C to 1350 °C to examine the evolution of microstructure, grain growth, and densification. Scanning electron microscopy (SEM) revealed a homogeneous distribution of phases, with distinct microstructural features attributed to each element at different sintering temperatures. The experimental results revealed that the composite’s density was increased by 30% and porosity was reduced by 61% at a sintering temperature of 1350 °C. The hardness and flexural strength of composite were found to be 23% and 60% higher at 1350 °C, respectively, compared to that at 850 °C, suggesting enhanced mechanical properties due to cerium and yttrium reinforcement within matrix and efficient doping and phase transformation. Overall, incorporation of cerium and yttrium significantly improved mechanical behavior and phase stability of ZrO₂–Cr–Ni composite, highlighting its potential for advanced engineering applications. Full article

This paper brings new information regarding the influence of partial replacement of portland cement with nano silica and mesoscopic ZnO powders in terms of mechanical and antimicrobial properties. The experimental results demonstrate a reduced growth of the opportunistic pathogens Staphylococcus aureus, Pseudomonas aeruginosa, and Candida albicans and an alteration of monospecific biofilm formation when exposed to the cement pastes modified with these additions. The coexistence of silica and ZnO powders modifies the kinetics of portland cement hydration and hardening processes, as well as the nature and composition of resulting compounds. While ZnO powder initially delays the hydration and hardening of portland cement, the addition of nano silica helps alleviate this delay and improves the compressive strengths. The main properties (mechanical strengths and antibacterial properties) of the cement pastes and derived composites (mortars) are assessed and statistically processed to identify the optimum dosage of each component. These materials could be of a particular interest for buildings exposed to conditions favoring microbial colonization, especially health-care facilities where the microbial load of antibiotic resistant and biofilm species is high. Full article

The demand for innovative products from renewable sources has motivated research development to create new sustainable materials. Cassava starch (CS) has been widely used for bonding and composing different types of products. Particleboards produced from cocoa (Theobroma cacao), wood wastes, and CS adhesives can be an environmentally correct and economically profitable alternative to replacing traditional commercial panels. This study aimed to manufacture particleboards made with wood waste extracted from the stem of Theobroma cacao. The panels were bonded with different proportions of CS and urea–formaldehyde (UF) adhesives, and their physical–mechanical properties were determined. To manufacture the panels, cocoa wood wastes were mixed with the adhesive in ratios of 90:10, 70:30, and 50%:50% (CS/UF). Two control treatments were bonded with 100% of both adhesives. The resulting particleboards were employed as a reference to compare properties. The manufacturing process was carried out by cold pressing. Apparent density, water absorption, thickness swelling, and static bending strength were found for all panels. The data obtained were subjected to Levene’s homogeneity test, Shapiro–Wilk’s normality test, analysis of variance (ANOVA), and Tukey’s mean test. The results showed that the highest density value was 497.0 kg m⁻³, corresponding to the treatment composed of cocoa wood wastes bonded with 100% CS adhesive. The water absorption and thickness swelling results after a 24 h immersion showed that the panel formed using cocoa wood wastes and 100% UF had the lowest values, 22.1 and 11.2%. The highest bending strength value was 13.1 MPa for the experimental treatment composed of cocoa wood residue and 100% UF. However, this result did not differ statistically from the treatment (50–50). Therefore, cocoa wood waste combined with adhesive CS may be a sustainable alternative for producing particleboards. Full article

This paper deals with a numerical method of analysis of the performance of shear connectors in transferring load in high-strength concrete-filled steel tube square sections. The novelty of the model is that it considers all the important parameters that affect performance at once: bond strength, the transfer rate of each connector, and the stress distribution and deformation of each element. Four specimens fabricated using different types of connectors were validated using ABAQUS version 2017 software. The deformation of the connectors, concrete damage, and the local instability of the steel tube were extensively investigated. The main parameters considered were the ultimate bond strength and load transfer ratio. The shear connector arrangement consisting of four specimens, namely C1 with 16 studs, a circular rib (C2), a circular rib with 8 studs (C3), and a circular rib with 8 vertical ribs (C4), had a significant influence on the key parameters. Connectors C2, C3, and C4 transferred more than 80% of the total load. The circular rib was more effective in transferring the load and limiting slip than the vertical rib and the studs. The circular rib (C2) transferred the load mainly through the four corners. The deterioration of the concrete and local instability of the steel tube had complex deformations which were influenced by the geometry of the inserted connectors. Full article