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QC Tools For Process/Product Establishment: R&D Feb 16, 2012

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QC Tools for Process/Product

Establishment
R&D
Feb 16, 2012

Objectives

Collection of data during trials

Analysis of data through Control chart to set LCL,


CL!

"evie# the $rocess condition % ste$ ta&en for


corrective action

'onitor the revie#ed $rocess and $re$are control


charts for $rocess consistency

(et the final (OPs % ($ecification of $roducts #ith


u$$er and lo#er limit!

O$timi)ation of 'ai)e starch Quality
to *evelo$ (i)elon + ,
Starch
Grade
Brookfield
Viscosity
pH oist!re
- -.// .!, -0!0
0 -1,/ 2!/ -/!/
3 -4// 2!, 2!4

" f f e c t o f B a s e S t a r c h o # V i s c o s i t y
5
,
.
1
2
4
- /
- -
- 0
/ - 0 3 5
F r e $ ! e # c y
B
%
R
&

'
!
p

V
i
s
c
o
s
i
t
y

(
S
e
c
)
1 * 0 0 c p s
1 + , 0 c p s
1 6 0 0 c p s

" f f e c t o f B a s e S t a r c h o # p H
5
5 ! ,
,
, ! ,
.
. ! ,
1
1 ! ,
2
/ - 0 3 5
F r e $ ! e # c y
p
H
- . , p H
6 . , p H
- . 0 p H

" f f e c t o f B a s e S t a r c h o # o i s t ! r e
- /
- -
- 0
- 3
- 5
- ,
- .
- 1
- 2
/ - 0 3 5
F r e $ ! e # c y

o
i
s
t
!
r
e

'
o
#
t
e
#
t

(
/
)
1 2 . , / o i s t ! r e
- . * / o i s t ! r e
1 0 / o i s t ! r e

Analysis of *ata + 6T"A 7isc!
8ith O$timi)ed 'ai)e (tarch Quality 9:rade 3;
B % R & ' ! p V i s c o s i t y
4
4 ! ,
- /
- / ! ,
- -
- - ! ,
- 0
- 0 ! ,
- 3
/ , - / - , 0 / 0 ,
F r e $ ! e # c y
V
i
s
c
o
s
i
t
y

(
S
e
c
)
0 ' 1
1 ' 1
' 1

Analysis of *ata + $<
8ith O$timi)ed 'ai)e (tarch Quality 9:rade 3;
p H
.
. ! ,
1
1 ! ,
2
2 ! ,
4
/ , - / - , 0 / 0 ,
F r e $ ! e # c y
p
H
0 ' 1
1 ' 1
' 1

Analysis of *ata + 'oisture
8ith O$timi)ed 'ai)e (tarch Quality 9:rade 3;
o i s t ! r e ' o # t e # t s
- 0
- 0 ! 0
- 0 ! 5
- 0 ! .
- 0 ! 2
- 3
- 3 ! 0
/ , - / - , 0 / 0 ,
F r e $ ! e # c y

o
i
s
t
!
r
e

(
/
)
0 ' 1
1 ' 1
' 1

Conclusion

'ai)e starch Quality

'oisture = 4!/ 'a>

$< = 2!, min

7isc! = -4// c$s 'in

O$timi)ed CL % LCL
Parameter LCL CL
6T"A 7isc 9sec; 4!2 -0!5
$< .!4 2!,
'oisture 9?; -0!- -3!-

%H&23S

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