CPS 410 Process Synthesis 410: School of Engineering Department of Chemical Engineering
CPS 410 Process Synthesis 410: School of Engineering Department of Chemical Engineering
CPS 410 Process Synthesis 410: School of Engineering Department of Chemical Engineering
STUDY GUIDE
CPS420 PROCESS SYNTHESIS
TABLE OF CONTENTS
ORGANISATIONAL COMPONENT Page 1. GENERAL PREMISE AND EDUCATIONAL APPROACH ...................................... 3 2. LECTURERS AND VENUES .................................................................................. 3 3. STUDY MATERIAL ................................................................................................. 3 Text books (prescribed)........................................................................................ 3 Text books (additional reading material) .............................................................. 3 4. LEARNING ACTIVITIES.......................................................................................... 4 4.1 Contact time ................................................................................................. 4 4.2 Lectures.......................................................................................................... 4 4.3 Tutorials and assignments.............................................................................. 4 5. ASSESSMENT ........................................................................................................ 4 6. GENERAL............................................................................................................... 4
STUDY COMPONENT
1. MODULE OBJECTIVES, ARTICULATION AND LEARNING OUTCOMES ........... 5 1.1 General objectives.......................................................................................... 5 1.2 Prerequisite background ................................................................................ 5 2. MODULE STRUCTURE .......................................................................................... 5 3. SYLLABUS THEMES .............................................................................................. 6
ORGANISATIONAL COMPONENT
1. GENERAL PREMISE AND EDUCATIONAL APPROACH
The purpose of the study guide is to give an overview of what is expected of the student in the module CPS 410 PROCESS SYNTHESIS 410 The purpose of this module is to create the environment in which the topics covered in previous modules can be integrated in order to successfully plan and execute a process engineering design.
2.
The contact details of the lecturer responsible for CPS420 are given below: Prof. M.D. Heydenrych Room 8-18 Engineering 1 building e-mail: mike.heydenrych@up.ac.za Tel : (012) 420-2199 (083) 603-1530
3.
STUDY MATERIAL
Text books (prescribed) 1. Seader, W.D., Seider, J.D., Lewin, D.R.; Product and Process Design Principles: Synthesis, Analysis and Evaluation; John Wiley & Sons, 2nd ed., 2004.
Text books (supplementary reading material) 2. 3. Sinnot, R.K.; Coulson & Richardson's Chemical Engineering, Vol. 6: Design, Pergamon, 1993 (2nd ed.) Luyben, W.L.; Process Modeling, Simulation and Control for Chemical Engineers, McGraw-Hill, 1991 (2nd ed.)
4.
LEARNING ACTIVITIES
13 of these lectures will be Aspen tutorials and tests, held in the Engineering computer labs. 4.2 Lectures
Lectures are presented on selected topics as set out below: The design process and the synthesis tree Heuristics Separation trains and residue curves PFDs and equipment lists Week 1-3 Week 3-9 Week 9-12 Week 13-14
5.
ASSESSMENT
PASS REQUIREMENTS:
To pass the module, a student has to obtain a final mark of at least 50%, and obtain a mark of at least 50% for the Aspen practical. Calculation of the final mark: The final mark will be calculated as the average of the semester mark and the exam mark. Semester mark: Class tests: Aspen practical: Semester tests (2):
6.
GENERAL
Guideline: The standard policies, rules and arrangements regarding the following will be applicable: Conduct in class Academic dishonesty Absence from certain scheduled activities Pocket calculator specifications
STUDY COMPONENT
1. MODULE OBJECTIVES, ARTICULATION AND LEARNING OUTCOMES
2.
MODULE STRUCTURE
The design process Process creation Heuristics for process synthesis Synthesis of separation chains
3. SYLLABUS THEMES
3.1. SYLLABUS THEME 1: Process simulation (ECSA exit level outcome 5: Engineering methods, skills, tools, including information technology) 1. After completing this syllabus theme, the student will have a working knowledge of Aspen+, and understand the capabilities and limitations of process simulation packages such as Aspen+. 2. Understand the role of a process simulator in obtaining data and carrying out mass and energy balances. 3.2. SYLLABUS THEME: Introduction to Process Synthesis (ECSA exit level 3: Engineering Design) 3.2.1 Learning outcomes 1. Understand the key steps in carrying out a process design. 2. Be aware of ethical, environmental and safety issues and how they affect the design of a new chemical process. 3. Be able to create a new process flow diagram by following the steps involving reactions, separations and T-P change operations. 4. Be able to identify alternative process flow diagrams, and assemble a synthesis tree of such alternatives. 5. Understand the importance of selecting reaction paths that do not involve toxic or hazardous chemicals, or otherwise choosing designs that reduce their possible impact. 6. To be able to distribute the chemicals to account for inert species, to purge species, to achieve high reaction selectivities, to remove exothermic heats of reaction and to combine operations effectively in the same piece of equipment. 7. To be able to apply heuristics in selecting separation processes to separate liquids, vapours and vapour-liquid mixtures. 8. Be knowledgeable about conditions in which process streams should be pumped as liquids or as vapours. 9. Be familiar with industrial separation methods and their basis for separation. 10. Understand the concept of a separation factor and be able to select appropriate separation methods for liquid mixtures. 11. Be able to sequence distillation columns by using heuristics and algorithmic methods. 12. Be familiar with techniques for separating azeotropic mixtures, including the use of residue/distillation curve maps.
3.2.2 Study units Product and Process Design Principles, WD Seider, JD Seader and DR Lewin: Chap 1, 3, 4, 5, 7, 10, 12.