Pneumatics

A full range of pneumatic options provides optimum

performance with all types of columns and detectors.
The Clarus 500 GC may be ordered with or without PPC (programmable pneumatic control). If the
instrument is ordered with PPC, each injector or
detector option may be ordered with conventional
or PPC pneumatics. There are up to 12 PPC zones
configured as 2 carrier (2 zones each), 2 detector
(2 zones each) and 4 auxiliary channels.

Oven
The Clarus 500 GC oven provides easy access to
columns. The oven gives excellent temperature
control and fast cool-down times for maximum
productivity. All temperature and time functions
are microprocessor controlled and are shown on
the touch-screen display. Software selectable
coolant time-out and coolant cut-in temperatures
ensure economical subambient operation.

Carrier gas pneumatics

Carrier gas pneumatics are included with the
Clarus 500 injector
PPC or conventional pneumatics are available
for all injectors
Two carrier zones

Volume:

10,600 cm3

Carrier PPC zones compensate for variations

in ambient temperature and pressure for
maximum stability

Temperature
range:

10 C above ambient to 450 C or

-99 C to 450 C with subambient
accessory

Split vent pneumatics are included with

the Clarus 500 split/splitless and PSS
(programmable split/splitless) injectors

Column overheat User settable up to 450 C

protect:
Temperature
programmer:

3 ramp, 4 plateaus

PPC provides direct setting of split flow

rates and ratios
Split vent PPC zones compensate for variations
in ambient temperature for maximum stability

Minimum
Range

Increment

PPC provides direct setting in mL/min, psig

or kPa or cm/sec

Initial oven
temperature:

-99 C to 450 C

1 C

Automatic leak testing with PPC

Initial time:

0 to 999 min

0.1 min

Rate:

0.1 to 45 C/min

0.1 C

Plateau time:

0 to 999 min

0.1 min

Final oven
temperature:

-99 C to 450 C

1 C

Cool-down
times:

250 C to 50 C: 4.8 min

200 C to 50 C: 3.8 min
50 C to 0 C*: 2.6 min
50 C to -30 C*: 3.4 min
*with liquid CO2

Three-ramps pressure program

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Pneumatic program rates:

0-100.0 psi/min
0-100.0 mL/min
0-200.0 cm/sec
or ballistic
Detector pneumatics
PPC or conventional pneumatics are available
for all detectors (excluding Electrolytic
Conductivity Detector [ELCD])

S P E C I F I C A T I O N S

The PerkinElmer Clarus 500 Gas Chromatograph

(GC) is a fully automated gas chromatograph. The
system offers the capabilities required for laboratories performing large numbers of routine analyses
as well as those involved in research and development. All instrument functions are set up and
monitored through a touch screen. The intuitive
graphical user interface includes a real-time chromatogram display and eight-language support.

G A S C H R O M ATO G R A P H Y

Clarus 500
Gas Chromatograph

 Four detector pneumatic zones

Injectors

PPC provides direct setting in mL/min

The Clarus 500 GC supports a comprehensive array of

injectors that provides accuracy and precision to all of
your sampling applications. Up to two injectors may be
installed and operated simultaneously with independent
temperature control. Every injector is available with PPC
or conventional pneumatics.

Detector PPC zones compensate for variations

in ambient temperature for maximum stability
Auxiliary pneumatics
Four auxiliary zones
PPC provides direct setting in mL/min, psig or kPa
Auxiliary PPC zones compensate for variations in
ambient temperature for maximum stability

Packed-column injector
Removable glass liner for trapping nonvolatile residues
Adapter for on-column injection to wide-bore
capillary columns

Autosampler

50 C to 450 C in 1 C increments
The Clarus 500 GC offers an optional, built-in syringe
autosampler for maximum sampling capabilities. All
control is accomplished through the keyboard or by a
data system such as TotalChrom.
Injection speed:

Normal, fast, slow

Program modes:

Two methods may be programmed

Number of sample
positions:

82, plus one priority

Vial size:

2-mL (0.25 mL with insert) crimptop caps

2-mL screw-top caps

1/8-inch fitting
1/4-inch column adapter available
Conventional pneumatics choice of flow controller
with head-pressure gauge, or flow controller with
head-pressure gauge and digital display of flow
PPC pneumatics programmed flow or pressure
includes readout which displays pressure or
column flow
Split/splitless capillary injector

Number of waste
and wash vials:

Four waste and four wash

Split ratio easily adjustable for a wide range of

analysis conditions

Waste and wash

vial size:

4 mL

Charcoal trap in split vent prevents contamination

of split valve and lab air

Syringe size:

0.5 L, 5.0 L or 50.0 L

Sampling volume:

0.1 L to 0.5 L from the 0.5-L

syringe in 0.1-L increments or
0.5 L to 5.0 L from the 5.0-L
syringe in 0.5-L increments or
5.0 L to 50.0 L from the 50.0-L
syringe in 5.0-L increments

Two choices of liner: 2-mm and 4-mm internal diameter

50 C to 450 C in 1 C increments

Viscosity settings:

0-15

Maximum number
of injections/vial:

15

Maximum number of 15
solvent postwashes:
Maximum number
of sample pumps:

Conventional pneumatics pressure regulator

(0-60 psig) for digital display of column head pressure.
Automatic control of split vent solenoid valve
PPC pneumatics four software configurable modes:
programmed flow, programmed pressure, programmed
velocity or constant flow. Vacuum compensation
software selectable
PPC pneumatics include automatic control of split
vent by split flow or split ratio

15
Programmable on-column capillary injector

Maximum number
15
of sample prewashes:
Minimum sample
volume required:

5 L when used with the

0.25-mL vial insert; 350 L when
used with the 2-mL vial

Reproducibility:

< 0.5% RSD for packed columns

1% C9 in C7, 1 L injected

1/16-inch fitting

Temperature-programmable inlet
Three-ramps temperature program
Oven tracking mode for simple operation
50 C to 500 C in 1 C increments
Heating rate of 1 C/min to 200 C/min or ballistic
1/16-inch fitting

 Conventional pneumatics choice of flow controller

with head-pressure gauge, or flow controller with
head-pressure gauge and digital display of flow

PreVent isolation mode allows a septum change without

interrupting carrier flow. Perform maintenance on the
inlet WHILE chromatography is taking place.

PPC pneumatics include readout which displays

pressure and column flow

ProTect mode eliminates contamination by preventing

heavy components in the sample from reaching the
expensive and retentive chromatographic column.
Allows back flushing during chromatographic run.

PSS programmable split/splitless

capillary injector
Temperature-programmable inlet
Large-volume injection of up to 50 L with autosampler,
150 L manually
Three-ramps temperature program
Oven tracking mode for simple operation with
on-column injection
Split ratio easily adjustable for a wide range of
analysis conditions
Three choices of liner available: 1-mm and 2-mm i.d.
and on-column
Charcoal trap in split vent prevents contamination of
split valve and lab air

MSVent mode allows changing of columns without

cooling and venting the Clarus 500 MS, reducing
instrument downtime, offering a significant time
savings. In addition, MSVent facilitates connection of
the vent to a second detector for dual signal capability,
providing greater flexibility and enhancing productivity.
Gas sampling valves
Wide offering of 4-, 6-, 8- and 10-port valves
Large range of valved systems and standard
analyzers available
Keyboard controlled
1/16- or 1/8-inch fittings

50 C to 500 C in 1 C increments
Heating rate of 1 C/min to 200 C/min or ballistic
1/16-inch fitting
Conventional pneumatics pressure regulator (0-60 psig)
for digital display of column head pressure. Automatic
control of split vent solenoid valve
PPC pneumatics four software configurable modes:
programmed flow, programmed pressure, programmed
velocity or constant flow. Vacuum compensation
software selectable
PPC pneumatics include automatic control of split vent
by split flow or split ratio
PreVent
Unique PerkinElmer sample management system

Detectors
A wide choice of detectors optimized for sensitivity and
selectivity is available for use with the Clarus 500 GC.
All built-in detectors include an automated background
compensation feature that corrects for column bleed.
Whether you choose the Flame Ionization Detector, the
Thermal Conductivity Detector, the Electron Capture
Detector, and/or environmental-specific detectors, all
conform to the highest industry standards for reliability
and performance. Every detector except the Electrolytic
Conductivity Detector (ELCD) is available with PPC or
conventional pneumatics. Up to two detector modules
may be installed and operated simultaneously with
independent temperature and pneumatic control.
Flame Ionization Detector (FID)

Available only on the Clarus 500 GC with PSS or

split/splitless capillary injector and PPC pneumatics

Wide linear dynamic range

Includes injector and detector restrictors

No makeup gas required due to efficient sweeping

of column effluent by hydrogen combustion gas

PreVent time-saver mode prevents higher boiling

components or residues from going through the
column and the detector.

Air flow designed to minimize contamination and

residue buildup
1/8-inch fittings

PreVent enhanced large-volume injection (ELVI)

mode isolates the column and detector from the
effects of high levels of solvent. Eliminate solvent
flooding of the column or allow the use of solvents
such as methylene chloride with an ECD.

Conventional pneumatics pressure regulator for

hydrogen, needle valve for air
PPC pneumatics software flow control of hydrogen
and air
Flame out warning and ready interlock

Operating
temperature:

100 C to 450 C in 1 C increments

Operating
temperature:

100 C to 350 C in 1 C increments

Sensitivity:

> 0.015 coulombs/g C

Sensitivity:

9 V/ppm nonane at 160 mA at the

bridge with a detector temperature
of 100 C
Typically < 1 ppm nonane

Minimum
detectable
quantity:

-12

< 3 10 g C/sec nonane at a

S/N = 2 to 1

Linearity:

> 10

Signal filtration:

50, 200, 800 msec

Minimum
detectable
quantity:

Input range:

1, 20

Linearity:

> 105

Makeup gas:

Not required

Power supply:

Constant current with four

selectable settings:
1: 40 mA
2: 80 mA
3: 120 mA
4: 160 mA

High operating temperature for maximum stability

Signal filtration:

50, 200, 800 msec

1/8-inch fittings
Conventional pneumatics needle valve for makeup gas

Filament
protection:

Self-limiting and resetting after

transient overloads in either channel

PPC pneumatics software flow control of makeup gas

Makeup gas:

Not required for 0.32- to 0.53-mm i.d.

columns with flows 5 mL/min
Required for 0.25-mm or smaller
i.d. columns

Electron Capture Detector (ECD)

High sensitivity
Excellent selectivity

Source:

15 mCi 63Ni

Temperature
protect:

470 C by software

Carrier gas:

Either Ar/CH4 or N2

Photoionization Detector (PID)

Operating
temperature:

100 C to 450 C in 1 C increments

Minimum
detectable
quantity:

< 0.05 pg perchloroethylene with

argon/methane or nitrogen

Special detector for water pollution analysis of samples

containing aromatic compounds.
Internal power supply and lamp control
Series operation kit available

Linearity:

> 10

Can be combined with ELCD in a single

detector position

Signal filtration:

200, 800 msec

1/8-inch fittings

Makeup gas:

Standard

Conventional pneumatics needle valve for makeup gas

PPC pneumatics software flow control of makeup gas

Thermal Conductivity Detector (TCD)

Operating
temperature:

100 C to 250 C in 1 C increments

(can be set to 350 C for cleaning)
< 10 pg benzene

Ideal for series operation

Minimum
detectable
quantity:

1/8-inch fittings

Linearity:

> 107

Conventional pneumatics reference gas

flow controller

Signal filtration:

50, 200, 800 msec

PPC pneumatics software flow control of reference gas

Input range:

1, 20

Makeup gas:

Standard

Capillary-column compatible
Proven constant current design
Software protection to prevent filament burnout

UV source lamp: 10.2 eV

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Combination PID/ELCD

Flame Photometric Detector (FPD)

Specific detector for halogenated compounds.

Clarus 500 GC controls solenoid valve for venting

Clarus 500 GC software controls photo-multiplier

tube voltage

Combined with PID in a single detector position

Clarus 500 GC software linearizer for sulfur mode

1/8-inch fittings

1/8-inch fittings

Conventional pneumatics pressure regulator for

hydrogen reaction gas

Conventional pneumatics needle valve for hydrogen,

pressure regulator for air

Operating
temperature:

100 C to 450 C in 1 C increments

PPC pneumatics software flow control of hydrogen

and air

Sensitivity:

5 1013 g Cl/sec trihalomethanes

Operating
temperature:

250 C to 450 C in 1 C increments

1 1011 g S/sec thiophene
1 1012 g P/sec tributylphosphate

Linearity:

> 10

Selectivity:

> 106 (Cl:Hydrocarbon)

Minimum
detectable
quantity:

Makeup gas:

Required for flows < 5 mL/min

Linearity:

Sulfur 102 (log-log)

Phosphorus 103

Nitrogen Phosphorus Detector (NPD)

Signal filtration:

50, 200, 800

Modular design

Selectivity:

10,000:1 (S/C)
100,000:1 (P/C)

Makeup gas:

Not required

Signal filtration: 50, 200, 800 msec

Change bead in less than one minute

Prealigned bead
Rapid conditioning, up and running in less than
two hours
1/8-inch fittings
Conventional pneumatics pressure regulator for
hydrogen, needle valve for air
PPC pneumatics software flow control of hydrogen
and air

Touch-screen graphical user interface

The touch-screen graphical user interface incorporates
a number of key features:
Multi-language support (i.e. English, French, Italian,
German, Spanish, Japanese, Chinese and Russian)
Real-time graphic display of chromatogram

Operating
temperature:

100 C to 450 C in 1 C increments

Minimum
detectable
quantity:

5 1013 g N/sec
2,4-dimethylaniline
5 1014 g P/sec tributylphosphate

Linearity:

> 104

Password protection

Signal filtration:

50, 200, 800 msec

Graphical display of temperature and pneumatic

programs

Selectivity:

50,000:1 (N/C)
10:1 (P/N)

Status-summary screen

Input range:

1, 20

Makeup gas:

Not required

Injection countdown for manual injections

Column pressure/flow/velocity calculator
More upgradable firmware
Preventative maintenance counter

Log file
Resolution: 240 x 320
256-color display
Meaningful error/alarm messages

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Other Clarus 500 GC features

Physical details

Recorder attenuation range from 1 to 65,536 in

binary steps

Power
requirements:

120 V 10%, 50/60 Hz, 2.0 kVA*

230 V 10%, 50/60 Hz, 2.0 kVA
* On an independent 20-amp line

Ambient
temperature:

10 C to 32 C

Ambient humidity:

80% maximum relative humidity

without condensation

Mean BTU output:

3400

Weight
GC:
Autosampler:

49 kg (108 lb)
4.5 kg (10 lb)

Long-term battery backup of GC methods, autosampler

programs, flow and temperature-calibration data
Software calibration of oven temperature and carrier
gas flow with PPC and conventional pneumatics
Full instrument control via external computer
Five stored methods
Baseline compensation

26.3 in. (69 cm)

18.4 in. (47 cm)

30.3 in. (77 cm)

21.4 in. (55 cm)

Auxiliary heated zone for accessory devices

28.4 in. (72 cm)

PerkinElmer Life and

Analytical Sciences
710 Bridgeport Avenue
Shelton, CT 06484-4794 USA
Phone: (800) 762-4000 or
(+1) 203-925-4602
www.perkinelmer.com
For a complete listing of our global offices, visit www.perkinelmer.com/lasoffices
2006 PerkinElmer, Inc. All rights reserved. The PerkinElmer logo and design are registered trademarks of PerkinElmer, Inc. Clarus, PerkinElmer and TotalChrom are registered trademarks
and MSVent and PreVent are trademarks of PerkinElmer, Inc. or its subsidiaries, in the United States and other countries. All other trademarks not owned by PerkinElmer, Inc. or its
subsidiaries that are depicted herein are the property of their respective owners. PerkinElmer reserves the right to change this document at any time without notice and disclaims liability
for editorial, pictorial or typographical errors.
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