Lubricating Oils Test Methods

Lubricating Oils
Test Methods Page Test Methods Page

Foaming Characteristics of Lubricating Oils ASTM D892, D6082; Oxidation Stability of Inhibited Mineral Insulating Oils IP 335 ........126
IP 146; DIN 51566; FTM 791-3211, 791-3213 ............................108-110 Oxidation Test For Lubricating Oil IP 48 ............................................126
Water Separability of Petroleum Oils and Synthetic Fluids Thermal Oxidation Stability of Automotive, Gear Lubricants
ASTM D1401, D6074, D6158; ISO 6614; DIN 51599; FTM 791-3201..111 ASTM D5704; STP 512A L-60 Performance Test
Demulsibility Characteristics of Lubricating Oils (formerly CRC L-60 Test); FTM 791 B Method 2504 95 ....................127
ASTM D2711..........................................................................................112 Rust Preventing Characteristics of Inhibited Mineral Oil in the
Air Release Properties of Petroleum Oils Presence of Water (Standard and Horizontal Disc Methods)
ASTM D3427; IP 313; DIN 51381 ........................................................113 ASTM D665, D3603, D6158; NACE TM-01-72; IP 135; ISO 7120;
Oxidation Stability of Steam Turbine Oils by Rotating Bomb DIN 51355, DIN 51585; FTM 791-4011, 791-5315 ....................128-129
ASTM D2272..................................................................................114-118 Stability of Lubricating Oils (Work Factor) FTM 791-3451.4 ..........130
Oxidation Stability of Inhibited Mineral Insulating Oil Corrosion of Lead by Lubricating Oils FTM 791-5321 ......................130
by Rotating Bomb ASTM D2112; IP 229 ....................................114-118 Copper Corrosion From Petroleum Products
Oxidation Stability of Gasoline Automotive Engine Oils by ASTM D130, D6074, D6158; IP 154 ....................................................131
Thin-Film Oxidation Uptake (TFOUT) ASTM D4742 ..................114-118 Bearing Compatibility of Turbine Oils FTM 791-3452 ......................131
Oxidation Characteristics of Inhibited Mineral Oils Pour Point of Petroleum Oils
ASTM D943, D2240, D4636, D5968, D6158; DIN 51586, ASTM D97; IP 15; ISO 3016; DIN 51597; FTM 791-201 ............132-133
51587, 51394; FTM 791-5307, 791-5308 ....................................119-122
Cloud Point of Petroleum Oils
Determination of the Sludging Tendencies of Inhibited Mineral Oils ASTM D2500; IP 219; ISO 3015; DIN 51597 ..............................132-133
ASTM D4310..................................................................................119-122
Dielectric Breakdown Voltage of Insulating Oils
Oxidation Stability of Distillate Fuel Oil (Accelerated Method) ASTM D877, D1816; IP 295; FTM 791-5702;
ASTM D2274..................................................................................119-122 NF C 27-221; IEC 156; VDE 0370......................................................134
Oxidation Characteristics of Extreme Pressure Lubricating Oils Coking Tendency of Oil FTM 791-3462 ..............................................135
ASTM D2893..................................................................................119-122
Evaporation Loss of Lubricating Oils (Noack Test)
Oxidation Stability of Mineral Insulating Oils ASTM D2440 ............123 ASTM D5800; DIN 51851; IP 421 ........................................................136
Corrosiveness and Oxidation Stability of Hydraulic Oils, Aircraft
For information on additional test methods for Lubricating Oils:
Turbine Engine Lubricants, and Other Highly Refined Oils Evaporation Loss of Lubricating Greases and Oils
ASTM D4636, D5968; FTM 791-5307, 791-5308; IHC BT-10; please refer to pages 148-149
DIN 51394 ......................................................................................124-125 Estimating Apparent Vapor Pressures and Molecular Weights of Lubricating Oils
Oxidation Stability of Inhibited Mineral Turbine Oils please refer to pages 92-94
IP 280 ....................................................................................................126 Please refer to the Viscosity, Flash Point and General Tests Sections
Additional test methods are available upon request
Oxidation Stability of Straight Mineral Oil IP 306 ............................126 please call or write for information.
Oxidation Stability of Mineral Insulating Oil IP 307 ........................126
www.koehlerinstrument.com
Foaming Characteristics of Lubricating Oils
Test Method
Foaming of lubricating oils in applications involving turbulence, high speed
gearing or high volume pumping can cause inadequate lubrication,
cavitation, overflow and premature oxidation. The sample is blown with a
controlled volume of air at different specified temperatures, including a
newer high temperature test at 150C. The resultant foam is measured at
the end of each aeration period and at different intervals afterward. In the
high temperature test, the amount of time required for the foam to collapse
to 0 after the aeration period is also measured.
Foaming Characteristics Test Baths
Dual-twin models for standard foaming characteristics tests
High temperature liquid bath for Sequence IV tests
Automatic time sequence models for both tests
Custom configurations for specialized applications
Dual Twin Foaming Characteristics Test ApparatusPerforms two
tests at 75F (24C) and two tests at 200F (93.5C). Consists of two 12x18"
(30.5x45.7cm) constant temperature baths with 1000mL test cylinders, certified
diffusers, air delivery tubes, and flowmeters (94mL/min.) for each sample.
Baths are equipped with microprocessor temperature controls, copper
immersion heaters and 120hp circulation stirrers to maintain temperature
uniformity of 1F (0.5C). Microprocessor PID control provides quick
temperature stabilization without overshoot and the bath is protected by an
overtemperature control circuit that interrupts power should bath temperature K43041
exceed a programmed cut-off point. Dual LED displays provide actual and Sequence IV
setpoint temperature values in C/F format. Test cylinders are held securely in Liquid Foaming
place by quick-locking cams in the bath cover assembly. A separate stainless Characteristics
steel support rack is provided to hold the test cylinders after removal from the Apparatus
bath. Cold bath (24C) has built-in coils for circulating exit air from the high
temperature test cylinders prior to passing to a volume meter, and a separate High Temperature Sequence IV Liquid Foam Test BathFor two tests
coil for circulating cooling water or refrigerant when the ambient temperature at 150C with a flow rate of 200mL/min. in accordance with ASTM D6082
exceeds the test temperature. Supplied with rubber stoppers and glass air specifications. Consists of a constant temperature bath with 1000mL test
outlet tubes for each cylinder. Bath controls are enclosed in a finished steel cylinders, certified diffusers, air delivery tubes and flowmeters.
base with chemical resistant polyurethane enamel finish. Communications Microprocessor PID control provides quick temperature stabilization without
software as seen on page 110 (RS232, etc.), ramp-to-set and other overshoot and the bath is protected by an overtemperature control circuit that
enhanced features are available as extra cost options. Contact your Koehler interrupts power should bath temperature exceed a programmed cut-off point.
representative for information. Dual LED displays provide actual and setpoint temperature values in C/F
FTM 791-3213 Aircraft Lubricants TestEmploys more severe format. Quick response copper immersion heaters provide efficient high
conditions, smaller sample, increased air flow, and longer aeration period to temperature operation, and a stirrer unit provides complete circulation for
test the foaming characteristics of aircraft-turbine lubricants. All models are temperature uniformity of better than 1F (0.5C). Locking cams hold the
available on special order for FTM 791-3213 testing. Please call or write for test cylinders in a vertical position, and a separate rack is provided to hold the
specifications and ordering information. cylinders after removal from the bath. For operator safety, an acrylic heat shield
surrounds the Borosilicate Glass bath jar. Communications software (RS232,
Specifications Included Accessories etc.), ramp-to-set and other enhanced features are available as extra cost
Conforms to the specifications of: Test Cylinders, 1000mL (4) options. Contact your Koehler representative for information.
ASTM D892; IP 146; DIN 51566; Diffuser Stones, calibrated and
FTM 791-3211, 791-3213*; NF T certified (4) Specifications
60-129 Air Delivery Tube Assemblies (4) Conforms to the specifications of: ASTM D6082
Temperature Control: Air Outlet Tubes (4) Temperature Control:
Digital Setpoint and Displays C/F Rubber Stoppers (4) Digital Setpoint and Displays C/F switchable
switchable Bath Jars (2) Built-in Overtemperature Cut-off Protection
Built-in Overtemperature Cut-off Support Rack (1) Included Accessories
Protection Acrylic Safety Shield, 18" Test Cylinders, 1000mL (2) Bath Jar (1)
Diffuser Stones, calibrated and certified (2) Support Rack (1)
*Requires modifications to standard equipment.
Air Delivery Tube Assemblies (2) Rubber Stoppers (2)
This equipment is available with a digital-indicating mass flow controller in place of the Air Outlet Tube (2) Acrylic Safety Shield, 18"
standard flowmeter. Please call or write for specifications and/or ordering information.
Digital Flowmeter option

is available for this unit. ! Software compatible, inquire
with Koehler Customer Service.
108
Ordering Information
Catalog Electrical Bath Air Bath Dimensions Shipping
Model No. Requirements Temperature Flow Rate Capacity lxwxh,in.(cm) Information
Dual- K43002 115V 24C
Twin 60Hz (75F) 3214x15x3114 Shipping Wgt.
15.6A (82x38x79.4) 217 lbs
K43092 220-240V and 9 gal Net Weight: (98.4kg)
50/60Hz (38.5L) 108 lbs (49kg) Dimensions
8.1A 93.5C 94mL/min each 29.6 Cu. ft.
Automatic K43003 115V (200F) bath
Time 60Hz 3214x15x3114 Shipping Wgt.
Sequence 16A (82x38x79.4) 227 lbs
K43093 220-240V (Operator Net Weight: (103kg)
50/60Hz variable) 118 lbs (53.5kg) Dimensions:
8A 33 Cu. ft.
Sequence K43041 115V 150C
IV 60Hz (302F) 1634x15x3114 Shipping Wgt.
Liquid 14A 200mL/min 9 gal (42.5x38x79.4) 89 lbs
(Operator (38.5L) Net Weight: (40.4kg)
K43049 220-240V variable) 62 lbs (28.1kg) Dimensions
50/60Hz 16.3 Cu. ft.
7A
D892 and D6082 Dual Twin Foaming Characteristics Test

ApparatusFor four tests in accordance with control ASTM D6082 and ASTM
D892 specifications. Dual liquid baths feature digital temperature control for
Sequences I through IV. Four flowmeters maintain the required flow rate of 94
and 200mL/min to the air diffusers. Requires the use of an external chiller to
perform the Sequence I and III tests at 24C.
Specifications
Conforms to the specifications of:
ASTM D892, D6082; IP 146; DIN 51566; FTM 791-3211; NF T 60-129
Temperature Control:
Digital Setpoint and Displays C/F switchable
Built-in Overtemperature Cut-off Protection
Included Accessories
Test Cylinders, 1000mL (4)
Diffuser Stones, calibrated and certified (4)
Air Delivery Tube Assemblies (4)
Air Outlet Tubes (4)
Rubber Stoppers (4)
Bath Jars (2)
Support Rack (1)
Acrylic Safety Shield, 18"
K43092 Dual-Twin Foaming Characteristics Apparatus

Accessories and Additional Ordering Information
For a complete listing of accessories and information on ordering a complete
package for ASTM D892 and/or D6082 testing, please turn to page 110.
Catalog Electrical Bath Air Bath Dimensions Shipping
Model No. Requirements Temperature Flow Rate Capacity lxwxh,in.(cm) Information
D892/D6082 K43005 115V Left (Cold) Bath: Ambient to 93.5C
Dual Twin 60Hz (200F) External Chiller required to 3214x15x3114 Shipping Wgt.
15.6A perform Sequence I and III at 24C 94mL/min and 9 gal (82x38x79.4) 217 lbs
K43095 220-240V 200mL/min (38.5L) Net Weight: (98.4kg)
50/60Hz Right (Hot) Bath: Ambient to 150C each 108 lbs (49kg) Dimensions:
8.1A (302F) 29.6 Cu. ft.

109
Accessories
Catalog No.
387-115-001 Air Pump, oil-less. Delivers 100% oil-free air. 115V 60Hz
387-230-001 Air Pump, oil-less. 220-240V 50/60Hz
K43026 Wet Test Gas Meter
For volume measurements of air leaving the test cylinders.
Note: One meter is required for each test cylinder.
Not required for the Alternative Procedure - Section 9.1.
332-005-005 Drying Tower. 300mm
K43025 Diffuser Stone Test Apparatus
For maximum pore diameter and permeability tests on
diffuser stones. Consists of 90cm manometer, 500mL flask,
flowmeter, graduate, delivery tube assembly and control valve.
K33031 Refrigerated Recirculator
Use with foam test baths for 24C tests (Sequence I and III).
Microprocessor based digital control and quiet running
compressor provide reliable operation and accurate control
within 0.5C. For complete specifications, please contact
Koehler Customer Service. 115V 60Hz, 8A
Advanced Communications Software Package for Data Management
K33032 Refrigerated Recirculator, 220-240V 50Hz, 4A
250-000-12F ASTM 12F Thermometer. Range: 5 to +215F
Test apparatus for ASTM D892 Sequence I, II and III 250-000-12C ASTM 12C Thermometer. Range: 20 to +102C
Catalog No. Order Qty 250-000-41C ASTM 41C Thermometer. Range: 98 to 152C
K43002 Dual Twin Foam Test Apparatus 1 344-100-01C Certified Diffuser Stone. Calibrated and certified for
(or K43003 Automatic Time Sequence Model) compliance with ASTM specifications for pore diameter
387-115-001 Air Pump 1 and permeability
K43025 Diffuser Stone Test Apparatus 1 344-100-001 Diffuser Stone, non-calibrated
250-000-12F ASTM 12F Thermometer 2 344-005-001 Stainless Steel Mott Diffuser
(or 250-000-12C ASTM 12C Thermometer) 344-005-01C Stainless Steel Mott Diffuser Certified
K43026 Wet Test Gas Meter 1 K43012 Test Cylinder
(not required for Alternative Procedure) Replacement 1000mL cylinder. Includes retaining ring.
332-005-005 Drying Tower 1
For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections
on pages 184 through 191.
Test apparatus for ASTM D6082 Sequence IV

Catalog No. Order Qty
K43041 Sequence IV Foam Test Bath 1
K43025 Diffuser Stone Test Apparatus 1
K43026 Wet Test Gas Meter 1
387-115-001 Air Pump 1
250-000-41C ASTM 41C Thermometer 1
Test apparatus for ASTM D892 and D6082

K43005 D892 and D6082 Dual Twin Foam Test 1
Apparatus
K43025 Diffuser Stone Test Apparatus 1
K43026 Wet Test Gas Meter 1
387-115-001 Air Pump 1
250-000-12F ASTM 12F Thermometer 2
(or 250-000-12C ASTM 12C Thermometer)
250-000-41C ASTM 41C Thermometer 2
110
Water Separability of Petroleum Oils and Synthetic Fluids
Test Method
The ability of a lubricating oil to separate from water and resist
emulsification is an important performance characteristic for applications
involving water contamination and turbulence. Water separability is
determined by stirring equal volumes of water and sample together at a
controlled temperature to form an emulsion and observing the time
required for separation of the emulsion to occur. This method is suitable for
petroleum oils and synthetic fluids.
Water Separability Tester
Tests emulsion characteristics of lubricating oils
Seven sample capacity
Movable digital stirrer with microprocessor control incorporates advanced
features for flexibility and ease of operation
Clear, illuminated heating bath provides excellent visibility
Microprocessor temperature control with digital display and built-in
protection against overtemperature and low liquid level hazards
Conforms to ASTM, ISO and related standards for water separability testing
Optional sensor for direct measurement of sample temperature
With built in drain for convenient draining of bath medium
Seven-sample Water Separability Tester provides full visibility and K39400 Water
Separability Tester
microprocessor control of all functions for simplified, accurate testing of up to
seven samples at a time. Use for specification of new oils and monitoring of
in-service petroleum oils and synthetic fluids.
Specifications
Seven position heating bathA full visibility bath immerses seven 100mL
Conforms to the specifications of: ASTM D1401, D6074, D6158; ISO 6614;
cylinders at the proper depth per ASTM and ISO specifications. Sample
cylinders are held securely in place by stainless steel supports inside the bath. DIN 51599; FTM 791-3201; NF T 60-125
A microprocessor based heater controls bath operating controls bath fluid Stirrer Range: 0-2000rpm
temperature with greater than 1C accuracy and stability throughout the Accuracy: 1.0rpm
operating range of 25C to 84C. Large LED readouts display setpoint and Drive: 110hp (75W), high torque
actual temperatures in Celsius or Fahrenheit scale at the operators option. For Bath Temperature Range: 25C to 84C
most samples, ASTM/ISO sample temperatures of 54C and 82C are attained Control Stability: 0.05C
within 10 minutes after placement of the test cylinders into the stabilized bath. Capacity: seven (7) 100mL graduated cylinders
Clear polycarbonate tank has backlighting for excellent visibility when viewing Construction: Clear polycarbonate tank 10"x11.25"x9.5" (25.5x28x24cm)
emulsion separations in the test cylinders. Cut-off circuits for low water level Medium: Water or white technical oil
and over-temperature conditions provide protection in the event of equipment Medium Capacity: 15.15L (4 gal)
malfunction. Easy removal of top plate for filling or cleaning the bath. Electrical Requirements:
Polycarbonate jar is encased in a Polyester-Epoxy finished steel housing with 115V 60Hz, Single Phase, 12A
a protective distortion-free viewing window and a solid foundation. 220-240V 50/60 Hz, Single Phase, 12A
Microprocessor sample stirrerTo avoid sample movement, the sample stirrer
Dimensions lxwxh, in.(cm) Included Accessories
housing pivots to each test position in the bath and locks securely in place
20.75x15.25x29.5 Seven 100mL Cylinders
at the required position in relation to the 100mL sample cylinder. The digital
stirrer offers complete flexibility for test duration and stirring speed at the push (52.7x38.75x 74.9)
of a button. Operating speed and count down time are prominently displayed Net Weight: 78 lbs (35.5kg)
on a large backlit LCD panel. A wide operating range of 0-2000rpm permits Ordering Information
in-house customized testing with 1rpm accuracy, and the operator may select
a stirring time of up to 99.99 minutes. At the end of the selected interval, the Catalog No. Order Qty
stirrer automatically shuts off and alerts the operator with audible and visual K39400 Water Separability Tester, 115V 60Hz 1
K39496 Water Separability Tester, 230V 50/60Hz
signals that the settling period has commenced. For added convenience, all test
parameters are stored in memory and repeated in subsequent tests until they Accessories
are changed by the operator. Engaging the stirrer mechanism is visible to the 332-002-018 Cylinder 100mL, graduated from 5 to 100mL
operator and housed in a clear tube for added safety. with 1.0mL divisions
250-000-19F ASTM 19F Thermometer. Range: 120 to 134F 1
For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections 250-000-19C ASTM 19C Thermometer. Range: 49 to 57C
on pages 184 through 191. 250-000-21F ASTM 21F Thermometer. Range: 174 to 188F 1
250-000-21C ASTM 21C Thermometer. Range: 79 to 87C
! Software compatible, inquire

K39252
K39251
PTFE Policeman
Test Tube Rack
7
1
111
Demulsibility Characteristics of Lubricating Oils
Test Method
Tests the ability of medium to high viscosity oils to separate from water
when water contamination and turbulence are encountered. The sample is
stirred together with distilled water for 5 min. at constant temperature. After
a specified settling period, the degree of separation is measured by volume
and the percentage of water in oil is determined. For lighter oils and
synthetic fluids, the ASTM D1401 Water Separability Test is used.
Demulsibility Apparatus
Conforms to the specifications of ASTM D2711
Variable stirrer speed
Choice of digital or analog bath models
StirrerComplete stirrer assembly per Fig. 1 and 2 of ASTM D2711,
including variable high speed drive motor, stainless steel propeller shaft,
top, center and bottom bearings, and steel motor housing with positioning
plate. Entire assembly mounts vertically in K39190/K39199 Constant
Temperature Bath. Built-in tachometer disc allows for precise stirrer
speed adjustment.
Constant Temperature BathsStandard model holds two K39103 Stirrers
and two K39120 Separatory Funnels in proper alignment for demulsibility
characteristics testing. Stirrers mount securely on a stainless steel support
plate having brackets for testing and drainage positions. Separate motor speed
controls are provided for each stirrer. All wetted parts are constructed of
stainless steel.
Microprocessor digital temperature control with dual LED displays for
K39190 Demulsibility Bath With Stirrers and Funnels
setpoint and actual temperatures and an illuminated bath interior with window
for viewing sample cylinders. Digital LED speed control is provided for each
Accessories stirrer.
Catalog No. Order Qty Specifications
K39120 Separatory Funnel 2 Conforms to the specifications of: ASTM D2711
With 0-500mL graduations. Meets ASTM specifications.
Capacity: Two (2) sample-water mixtures
K39130 Solvent Tank. Immerses stirrer assembly for 1
Maximum Temperature: 212F (100C)
convenient cleaning after testing.
Temperature Control: Microprocessor digital control with LED display
K39140 Forced Warm Air Dryer, 115V 60Hz
Bath Medium: 9 gal (38.5L) water
High output 1400W dryer and brass cylinder
Electrical Requirements:
mounted on a sturdy base. Rapidly dries
115V 60Hz
stirrer assembly after cleaning.
220-240V 50/60 Hz
K39149 Forced Warm Air Dryer, 220-240V 50/60Hz 1
K39150 Sampling Gauge and Centering Device 1 Dimensions: WxDxH in (cm) Shipping Information
Per Fig. X1.1 of ASTM D2711. Aids in accurately 1514x15x37(39x38x94) Shipping Weight 133 lbs (60.3kg)
obtaining 50mL samples from separatory funnels Net Weight: 72 lbs (32.6kg) Dimensions: 25.4 Cu. ft.
for the percent water in oil determination.
360-000-003 Digital Tachometer 1 Ordering Information
Hand held non-contact LCD tachometer
takes measurements up to 3 ft away with 1rpm Catalog No. Order Qty
accuracy. Supplied with four 1.5V AA batteries. K39190 Demulsibility Bath, 115V, 60Hz
1
250-000-09F ASTM 9F Thermometer K39199 Demulsibility Bath, 220-240V, 50/60Hz
Range: 20 to 230F 1 K39103 Stirrer** 2
250-000-09C ASTM 9C Thermometer **Suitable for use with K39190 & K39199
Range: 5 to +110C
K39170 Conditioning Bath, 115V 60Hz 1
Constant temperature water bath holds 8 separatory
funnels in two removable 4-unit racks for conditioning
prior to testing in Demulsibility Apparatus.
K39179
Includes microprocessor digital temperature control,
automatic water level control and gabled cover.
Conditioning Bath, 220-240V 50/60Hz
112
Air Release Properties of Petroleum Oils
K88500 Air Release Value Apparatus
Test Method Specifications Included Accessories

The ability of a turbine, hydraulic, or lubricating oil to separate entrained air Conforms to the specifications of: ASTM 12C Thermometer
is a key performance characteristic in applications where agitation causes ASTM D3427; IP 313; ISO 9120; Sinkers, 5mL and 10mL
a dispersion of air bubbles in the oil. To determine air release properties, DIN 51381; NF E 48-614 Drying oven
the sample is heated to a specified test temperature and blown with Temperature Range: Pressure gauge
compressed air. After the air flow is stopped, the time required for the ambient to 75C (167F) Circulating Bath
air entrained in the oil to reduce in volume to 0.2% is the air bubble Electrical Requirements: Air Bath for Sinker
separation time. 115V 60Hz, 3.0A Balance
230V 50Hz, 1.5A Platinum Wire
Air Release Value Apparatus 230V 60Hz, 1.5A Jacketed Test Vessel
Conforms to ASTM D3427, IP 313 and related specifications
Dimensions lxwxh,in.(cm)
High accuracy temperature control with digital setpoint and display
24x28x3814 (61x71x97) Shipping Information
Digital control panel leads user from start to finish of test operation
(Air Release Value Apparatus only) Shipping Weight for complete system:
Automatic calculation of final sample density for determination of air
Net Weight for complete system: 300 lbs (136kg)
release value
225 lbs (103kg) Dimensions: 50.7 Cu. ft.
Redundant overtemperature protection circuitry assures safe operation
The Koehler Air Release Value Apparatus consists of a test vessel and air
flow control equipment for delivering heated air at the specified flow rate to a
lubricating oil sample maintained at constant temperature. Microprocessor- Catalog No. Order Qty
based control panel guides user from start to finish of test operation and K88500 Air Release Value Apparatus,
provides density calculation and timing operation for measuring the air release 115V 60Hz 1
value of the test sample. The system includes drying oven for warming test oil K88501 Air Release Value Apparatus,
at temperatures of up to 100C; circulating bath with digital temperature 230V 50Hz
controller and air bath for sinker; compressed air heater with digital K88502 Air Release Value Apparatus,
temperature controller, overtemperature and overpressure protection circuitry; 230V 60Hz
pressure gauge; thermometer. Optional Windows software automatically
measures the time for air release.

113
Oxidation Stability RPVOT & TFOUT
Oxidation Stability of Steam
Turbine Oils by Rotating Pressure Vessel (Bomb)
Oxidation Stability of Inhibited Mineral
Insulating Oil by Rotating Pressure Vessel (Bomb)
Oxidation Stability of Gasoline
Automotive Engine Oils by Thin
Film Oxidation Uptake (TFOUT)
Test Method
The RPVOT (RBOT) procedure employs severe oxidation conditions to
rapidly determine oxidation stability. Suitable for both new and in-service
oils, the RPVOT (RBOT) method is applicable to many types of petroleum
oils. The sample is oxidized in the presence of water and a copper
catalyst in a stainless steel pressure vessel under an initial pressure of
90psi (620kPa). Pressure inside the vessel is recorded electronically or
mechanically while the vessel is rotated at 100rpm at constant
temperature, and the amount of time required for a specified drop in
pressure is the oxidation stability of the sample. A variation of the RPVOT Oxidata Pressure Measurement System
(RBOT) method is the Thin Film Oxidation Uptake Test (TFOUT) for
gasoline automotive engine oils.
Oxidata Pressure Measurement Systems
RPVOT (RBOT) Test Apparatus Electronic pressure measurement systems exclusively designed for RPVOT
2, 3 and 4-unit systems (RBOT), TFOUT and other ASTM oxidation test methods
Oxidata Pressure Measurement System Powerful Oxidata software for Windows and Windows 95
Conforms to ASTM D2112, D2272 and IP 229 specifications for RPVOT environments
(RBOT) testing Monitors up to twelve pressure and four temperature channels
Conforms to ASTM D4742 specifications for TFOUT testing Can be installed to most manufacturers RPVOT(RBOT)/TFOUT
test apparatus
For product specifications and ordering information:
Oxidation Pressure Vessels Page 114 Complete electronic measurement systems for plotting pressure versus
Oxidation Baths Page 116 time and temperature in RPVOT (RBOT) and TFOUT testing. Each system
Beakers and Accessories Page 117 includes transducers, bomb couplings, RTD probe assembly, multiplexer, data
Catalysts Page 117 acquisition card, software, and mounting and connecting hardware. Systems
Pressure Recorder Page 117 are available in two, three and four pressure vessel configurations, and
Oxidata Pressure Measurement System Page 115 additional channels can be added for up to a total of twelve pressure and four
Complete Systems, 2, 3 and 4-Unit Page 118 temperature channels.
Oxidation Pressure Vessel Koehler pressure measurement systems for RPVOT (RBOT) and TFOUT
feature Oxidata, a high accuracy pressure measurement software package
Polished stainless steel construction designed exclusively for ASTM oxidation test methods. Designed to run in
Can be converted for use in the Thin Film Oxidation Uptake Test (TFOUT) a Windows or Windows 95 environment, Oxidata monitors up to twelve
Consists of pressure vessel body, cap and stem with inlet needle valve in samples simultaneously, with graphical or tabular display of results.
accordance with ASTM specifications. Vessel holds one borosilicate glass Each channel can be independently configured for any of the applicable
sample container between two PTFE discs. Closure ring tightens by hand to ASTM standard test methods without compromising the independence or
seal cap to pressure vessel body. Vessel connects to pressure recorder or accuracy of the other channels. Independent start and stop times and user
rotary transducer and rotates on magnetic carriage in RBOT bath. Withstands programmable end points add even greater flexibility.
working pressure of 500psi (3450kPa) per ASTM specifications. Stainless The software plots your data on screen on line, real time, and automatically saves
steel construction ensures proper rate of heat transfer. Closure ring is your data on disk or to the hard drive during the test to prevent loss of valuable
constructed of chrome plated steel. Includes PTFE fluorocarbon wear disc and data. Multiple display options include the ability to view the status of all twelve
sample container cover disc. pressure channels on screen simultaneously and then click on any one channel
for a graph display; or to view four channels in graphical format simultaneously.
Ordering Information Powerful program features allow you to change axes, have colored plot lines and
Catalog No. zoom in on a specific plot sector to view data in greater detail.
K70000 Oxidation Pressure Vessel
K70092 Aluminum Insert
Converts standard K70000 Oxidation Pressure Vessel
for use in the TFOUT method
114
Oxidata Features and Specifications
On-line, real time monitoring of up to twelve samples simultaneously -
results plot directly to the screen for instant monitoring or printout of results
Menu options for RPVOT (RBOT) or TFOUT testing, as well as for other
ASTM fuel and lubricant oxidation tests
Programmable automatic end point detection with graphical and tabular
representation
Each channel can be configured and operated independently with different
start/stop times and different ASTM test methods
Zoom in feature allows for magnification of any plot sector on any channel
for a more detailed study
Monitors and reports temperatures of as many as four baths
simultaneously using accessory RTDs, and calculates and displays average
temperature for each bath. Exports data to spreadsheet programs
such as Microsoft Excel, Lotus 1-2-3, etc.
Temperature and pressure calibration capability
Data is saved directly to the hard drive during testing to prevent loss of
Oxidata Software automatically calculates and displays the endpoint of RPVOT
valuable data
(RBOT)/TFOUT test methods.
Operates in Windows 2000 or higher
Simple upgrade from existing Koehler data acquisition systems
Included Accessories (for the pressure measurement systems)

Rotary transducers (connects directly to bomb)
Data acquisition box with USB interface
Oxidata software
Multiplexer
RTD probe assembly (1)
Mounting Bracket for bath
Connecting cables and hardware
Computer Requirements
Processor: Intel Pentium II or similar (minimum)
Memory (RAM): 256MB or higher
Speed: 500 MHz or higher
Windows 2000 or higher
Disk Space: 15 MB free space (minimum)
Communications Port: One USB port
Other Software: Microsoft Excel (97 or above)
One RS232 port for temperature controller (optional)
Real-time plot screen displays pressure versus time for up to twelve samples
simultaneously.
The ordering information below is for installation to Koehler equipment. Oxidata Retrofit Kits
For other makes of equipment, a few basic hardware items may also be To upgrade your existing Koehler electronic pressure measurement system to
required - please contact your Koehler representative for assistance. the Oxidata software, please refer to page 118.
Catalog No.
RBOT/TFOUT Electronic Pressure Measurement System
K70502-XP Two-Unit System, 115V 60Hz
K70592-XP Two-Unit System, 220-240V 50/60Hz
K70503-XP Three-Unit System, 115V 60Hz
K70593-XP Three-Unit System, 220-240V 50/60Hz
K70504-XP Four-Unit System, 115V 60Hz
K70594-XP Four-Unit System, 220-240V 50/60Hz
115
Oxidation Baths
Two, three and four-pressure vessel models
Conforming to ASTM requirements for RPVOT (RBOT) and TFOUT testing
Constant temperature bath rotates oxidation pressure vessels at 100rpm at an
angle of 30 in accordance with ASTM specifications. Includes drive system
and oil bath with electronic solid state temperature control. Meets ASTM
requirements for heat transfer capability and temperature control precision.
A convenient carriage arrangement allows the oxidation vessels to be inserted

quickly and securely in the drive system. A strong magnet holds the vessel in
place while locating pins in the carriage engage the base of the vessel. PTFE
guides support the pressure vessel stem for added stability. If the vessel
becomes obstructed for any reason, the magnetic carriage releases it to
prevent damage. A chain and sprocket drive system powered by a heavy duty
capacitor start motor rotates the vessel carriages at 100rpm. Drive shafts ride
on PTFE fluorocarbon bearings which provide extended service and are
compatible with silicone heat transfer fluids and other types of bath oils.
Bath temperature is controlled within ASTM specified limits by an electronic

solid state controller with C/F switchable digital setpoint and display.
Overtemperature protection is provided by a built-in limit control that
Specifications
automatically interrupts power to the bath when bath liquid temperature
Conforms to the specifications of: ASTM D2112, D2272, D4742; IP 229
exceeds 16.7C (30F) above the temperature setting or 177C (350F). Power
Capacity: 2, 3 or 4 oxidation pressure vessels
must then be manually restored by the operator after checking the cause of the
Temperature Control:
problem. Pressure vessel carriage vanes circulate the bath oil during testing to
Maximum Temperature: 200C (392F)
ensure temperature uniformity, and an auxiliary stirrer can be operated
Control Stability: 0.02C (0.04F)
between tests to prevent sludging of non-silicone bath oils.
Heater Range:
2 and 3-pressure vessel models: 0-2750W
The bath interior is constructed of welded stainless steel and is fully insulated.
4-pressure vessel models: 0-3750W
A hinged section of the bath cover provides easy access to the vessel
Recommended Bath Medium: high temperature silicone heat transfer fluid
carriages. Vapor barriers in the cover close around the vessel stems to contain
(355-001-002 or 355-001-004page 8)
vapors from the hot bath medium. A chemical resistant polyurethane finish
Drive System: 100rpm positive drive transmission powered by a continuous
protects the bath exterior and control cabinet.
duty 12hp ball bearing motor with built-in gear reducer
Catalog No Capacity Electrical Requirements Bath Capacity, gal (L) Dimensions, lxwxh,in.(cm) Net Weight Shipping Weight
K70200 2 oxidation 220-240V 60Hz, 17.17A 18 (68) 28x26x33 237 lbs 356 lbs (161.5kg)
K70290 vessels 220-240V 50Hz, 17.17A (71x66x84) (107.5kg) 25.3 Cu. ft.
K70390 vessels 220-240V 50Hz, 17.17A (94x66x84) (129kg) 32 Cu. ft.
K70490 vessels 220-240V 50Hz, 21.5A (117x66x84) (170kg) 40.3 Cu. ft.
For verifying bath temperature in accordance with ASTM and

IP test method specifications
Catalog No.
250-001-37C IP 37C Thermometer. Range: 144 to 156C
For RPVOT (RBOT) method.
For ASTM D2112 method.
For TFOUT method.
116
Oxidation Pressure Vessel Accessories Pressure Vessel Support Racks
Sample beakers for RBOT and TFOUT methods For convenient handling of oxidation pressure vessel during assembly
Oxygen charging accessories and disassembly
Ordering Information Securely holds vessel-recorder assembly in an upright position. Convenient for
assembling and disassembling vessel. Equipped with drainage trough for bath
Catalog No.
oil remaining on the vessel exterior after testing.
Sample Beakers
K70040 RPVOT (RBOT) Sample Beaker Ordering Information
Borosilicate glass, 175mL
Catalog No.
Meets ASTM D2112, D2272 specifications
K70017 Pressure Vessel Support Rack, 2-Unit
K70091 TFOUT Sample Container
Borosilicate glass. Meets ASTM D4742 specifications
Oxygen Charging Accessories
K70080 Charging Hose. 6 ft (1.8m), with connections Catalysts
K70082 Female Quick Disconnect Coupling, for charging hose For Rotating Pressure Vessel Oxidation Test (RPVOT)
K70081-1 Male Quick Disconnect Coupling, 14" NPT, For Thin Film Oxidation Uptake Test (TFOUT)
for oxidation pressure vessel
K70013 Oxygen Pressure Regulator Ordering Information
Oxidation Pressure Vessel Accessories Catalog No.

K70050 Silicone O-ring Copper Catalyst for RPVOT (RBOT) Method
Replacement seal for pressure vessel lid-body K70030 Copper Catalyst Coil
connection Prepared in accordance with ASTM specifications
K70049 Sample Beaker Cover (PTFE disk) and packed in a sealed glass container with
K70048 TFOUT Sample Beaker Cover (PTFE disk) nitrogen atmosphere. Ready to use.
K70000-03008 Spring. Inserts in pressure vessel to hold K70090 Copper Catalyst Wire
RPVOT (RBOT) beaker and cover in place 1.63mm electrolytic copper wire in 500 ft (152m) lengths.
K700-0-3A Spring. Inserts in pressure vessel to hold K70002 Winding Mandrel
TFOUT container and cover in place Machined aluminum mandrel for winding copper wire into
coils meeting ASTM specifications.
Pressure Recorder Mounts on K70003/K70004 Drive Unit
K70003 Drive Unit for Winding Mandrel
Conforms to ASTM D2112, D2272, D4742 and IP 229 specifications
Slow speed gear motor mounted on a sturdy base.
Records pressure inside oxidation bomb on 24-hour charts. Range 0 to
Facilitates coil winding procedure. 115V
200psi, accurate to within 2% of scale range, 24-hour spring wound chart
K70004 Drive Unit for Winding Mandrel
movement. Housed in a finished metal case. Includes cartridge pen.
Similar to K70003 but for operation on 220-240V
Catalyst Package for TFOUT Method
Catalog No.
K70093 Catalyst Package A
K70010/24 Pressure Recorder, 24-hour
For simulating IIID engine
test. Includes 3 catalyst packages
Accessories K70095 Catalyst Package B
K70018 Replacement Cartridge Pen
For simulating IIIE engine test.
308-000-004 Recorder Chart, 24-hour
Includes 3 catalyst packages
Box of 60 charts
Oxidata pressure measurement equipment is now available for the RPVOT

(RBOT) and TFOUT Methods. Please refer to page 115.
117
Oxidation RPVOT & TFOUT
2 Unit RBOT System: 4-Unit RBOT System:
K70200 Oxidation Bath (or K70290) K70400 Oxidation Bath (or K70490)
K70000 Oxidation Pressure Vessel (2) K70000 Oxidation Pressure Vessel (4)
K70502-XP Oxidata Pressure Measurement System (or K70592-XP) K70504-XP Oxidata Pressure Measurement System (or K70594-XP)
K70002 Winding Mandrel K70508 Mounting Bracket for Four-Unit XP System
K70003 Drive Unit (or K70004) K70002 Winding Mandrel
K70017 Pressure Vessel Support Rack K70003 Drive Unit (or K70004)
250-001-37C IP 37C Bath Thermometer K70012 Pressure Vessel Support Rack
K70080 Charging Hose 250-001-37C IP 37C Thermometer
K70082 Female Quick Disconnect Coupling for charging hose K70080 Charging Hose
K70082 Female Quick Disconnect Coupling for charging hose
K70081-1 Male Quick Disconnect Coupling for oxidation
K70081-1 Male Quick Disconnect Coupling for oxidation
pressure vessel (2)
pressure vessel (4)
K70013 Oxygen Pressure Regulator
} }
K70013 Oxygen Pressure Regulator
K70030 Copper Catalyst Coils Order sufficient
K70030 Copper Catalyst Coil Order sufficient
K70090 Copper Catalyst Wire, 500 ft. quantity to K70090 Copper Catalyst Wire, 500 ft. quantity to
K70040 Sample Container meet anticipated K70040 Sample Container meet anticipated
K70050 Silicone O-ring testing requirements. K70050 Silicone O-ring testing requirements.
3-Unit RBOT System: For TFOUT testing, make the following substitutions:
K70300 Oxidation Bath (or K70390) K70091 Sample Beaker (replaces K70040)
K70000 Oxidation Pressure Vessel (3) K70092 Aluminum Insert (2, 3 or 4)
K70503-XP
K70002
K70003
Oxidata Pressure Measurement System (or K70593-XP)
Winding Mandrel
Drive Unit (or K70004)
K70095 }TFOUT Catalyst Package (in lieu of K70030, K70090,
K70002, K70003)
K70011 Pressure Vessel Support Rack 250-000-100C ASTM 100C Thermometer (replaces 250-001-37C)
250-001-37C IP 37C Thermometer
K70080 Charging Hose Oxidata Retrofit Kits
K70082 Female Quick Disconnect Coupling for charging hose To upgrade existing DOS-based Koehler electronic pressure measurement
K70081-1 Male Quick Disconnect Coupling for oxidation systems to the Oxidata system. Kits include Oxidata software, data
pressure vessel (3) acquisition card, multiplexer board, RTD probe assembly and connecting
}
K70013 Oxygen Pressure Regulator cables. Does not include rotary transducers or bath mounting bracket.
K70030 Copper Catalyst Coils Order sufficient For information on upgrading other makes of equipment to the Oxidata
K70090 Copper Catalyst Wire, 500 ft. quantity to system, please contact your Koehler representative.
K70040 Sample container meet anticipated
K70050 Silicone O-ring testing requirements. Ordering Information
Catalog No.
K70502RETRO 2-Unit Oxidata Pressure Measurement System
without Transducers, 115V 60Hz
without Transducers, 220-240V 50/60Hz
without Transducers, 220-240V 50/60Hz
without Transducers, 220-240 50/60Hz
Accessories
K70500 Rotary Transducer
Includes electronic transducer and rotating stainless
steel housing
K70519 RTD Kit, for monitoring the temperature
of an additional bath
118
Oxidation Stability and Corrosiveness of Petroleum Oils
Test Method
Various methods are available for testing the resistance to oxidation and/or
the corrosiveness of lubricants, insulating oils, hydraulic oils and distillate
fuel oils. The samples are subjected to a metered flow of air at elevated
temperatures, sometimes in the presence of a metal catalyst. Each of the
tests referenced on this page are also represented on other pages in this
section of the catalog.
High Temperature Convertible Oxidation Bath

Conforms to various ASTM, Federal and International Standards
Removable racks hold different types of glassware for different tests
Equipped with flowmeters or digital mass flow controls to measure and
control the required flow rates
Microprocessor digital temperature control
High temperature liquid bath for oxidation stability and corrosiveness tests
at temperatures of up to 200C. Available in different configurations for
convertibility between several oxidation stability and corrosivity test methods
including Cummins oxidation test. Removable rack/top plate assemblies
remove and install with minimum effort to easily convert the bath between
test methods. For most test methods, twelve sets of glassware can be
accommodated in each rack assembly. Select flowmeters or digital mass flow
control to maintain air flow at the required rates. Microprocessor PID control
provides quick temperature stabilization without overshoot, and the bath is
protected by an overtemperature control circuit that interrupts power should
bath temperature exceed a programmed cut-off point. Dual LED displays provide
actual and setpoint temperature values in C/F format. Communication
K12230 High Temperature Convertible Oxidation Bath
software (RS232, etc.) ramp-to-set and other enhanced features are available
as extra cost options. Contact your Koehler representative for information.
Specifications
Conforms to the specifications of*: Catalog No.
ASTM D943, D2274, D2440, D2893, D4310, D4636, D4871**, D5968, Please contact your Koehler representative for information on glassware
D6594; DIN 51394, 51586, 51587; FTM 791-5307, 791-5308 racks and airflow control options prior to order placement.
*with the appropriate glassware rack and flow control equipment installed
see ordering information. K12230 High Temperature Convertible Oxidation Bath,
**Modified versions of this equipment are available for D4871 (UOT) 115V 60Hz
test method. K12239 High Temperature Convertible Oxidation Bath,
Capacity: Twelve (12) sets of glassware. For ASTM D5968, FTM 791-5307, 220-240V 50/60Hz
and FTM 791-5308, only ten (10) sets of glassware.
Temperature Range: Ambient to 200C Accessories
Temperature Control Accuracy: 0.2F (0.1C) K1223-R943 Sample Rack for D943, D2274, D2983, D4310 testing
Bath Medium: Silicone heat transfer fluid K1223-R2440 Sample Rack for D2440 testing
Flow Rate: As specified for ASTM or applicable specifications K1223-R4636 Sample Rack for D4636, D5968, D6594 testing
Electrical Requirements: K1223-3L Flowmeter Stand with Flowmeters for D943,
115V 60Hz, Single Phase, 27.3A D2274, D2440, D4310 testing (range 3 0.1 L/hr)
220-240V 50/60Hz, Single Phase, 14.6A K1223-10L Flowmeter Stand with Flowmeters for D2893, D4636,
D5968, D6594 testing (range to 10 0.5 L/hr)
Dimensions Ixwxh,in.(cm)
Bath (without glassware): 2512x24x42(65x61x107) To order glassware and other accessories please refer to the pages in
Shipping Information (without glassware) this section of the catalog that correspond to the test methods that you
Shipping Weight: 213 lbs (96.6kg) will be following.
Dimensions: 29 Cu. ft.

119
Oxidation
Oxidation Characteristics of
Inhibited Mineral Oils
Sludging and Corrosion Tendencies of Inhibited
Mineral Oils
Oxidation Stability of Distillate
Fuel Oil (Accelerated Method)
Oxidation Characteristics of
Extreme-Pressure Lubrication Oils
Test Method
Evaluates oxidation stability by subjecting the sample to a temperature of 95C
in the presence of oxygen or dry air. For inhibited mineral oils, the sample is
reacted with oxygen in the presence of water and an iron-copper catalyst.
Oxidation Stability Apparatus

Thirty and sixty-place liquid baths for high volume testing requirements
Eight and twelve-place liquid baths for benchtop placement
Twelve-place solid block bath
Conforming to ASTM and related test method specifications
Special baths for ASTM D2893 and AOCS CD12-57 tests
For product specifications and ordering information:

30 and 60-place Oxidation Baths - page 121
Solid-Block Oxidation Bath - page 121
Oxidation Cell Glassware and Accessories - page 122
Iron-Copper Catalyst and Thermometers - page 122
K12219 Oxidation Stability Bath
Eight and Twelve-Place Oxidation Baths
Conforming to ASTM and related test method specifications Specifications
Constant temperature baths with solid state temperature control, calibrated Conforms to the specifications of:
ASTM D943, D2274, D2893*, D4310, D6158; AOCS CD12-57**
flowmeters and condenser water manifold for oxidation stability tests on fuels
DIN 51586, 51587; ISO 4263, ISO 12205; NF M 07-047; NF T 60-150
and lubricants. Individual flowmeters and control valves for each oxidation cell
Test Capacity: 8 or 12 oxidation cells
deliver air flow at the rate of 3L/h. Condenser water manifold has individual
Temperature Range: ambient to 212F (100C)
control valves for each cell. Microprocessor PID control provides quick Temperature Control Stability: 0.2F (0.1C)
temperature stabilization without overshoot, and the bath is protected by a Bath Medium: white technical oil
redundant overtemperature control circuit that interrupts power should Bath Capacity:
bath temperature exceed a programmed cut-off point. Display provides 8-place model: 10 gal (37.8L)
actual setpoint temperature values in C/F format. Communications 12-place model: 19 gal (71.9L)
software (RS232, etc.), ramp-to-set and other enhanced features are Electrical Requirements:
available as extra cost options. Double-wall insulated baths are equipped 8-place model: 115V 60Hz, Single Phase, 13.0A
with copper immersion heaters and a 120 hp circulation stirrer. Stainless 220-240V 50/60Hz, Single Phase, 6.8A
steel bath interior has a built-in support rack and overflow/drain to immerse 12-place model: 115V 60Hz, Single Phase, 32.6A
the test cells at the required depth. Order oxidation cell glassware and 220-240V 50/60Hz, Single Phase, 17.0A
accessories separately.
Catalog No.
8-place model: 1712x25x42 (44x64x107)
12-place model: 22x14x42 (57.15x35.56x107) K12200 Oxidation Bath, 8-Unit, 115V 60Hz
K12290 Oxidation Bath, 8-Unit, 220-240V 50/60Hz
Shipping Information: K12212 Oxidation Bath, 12-Unit, 115V 60Hz
Shipping Weight:
8-place model: 137 lbs (62.1kg) K12219 Oxidation Bath, 12-Unit, 220-240V 50/60Hz
12-place model: 213 lbs (96.6kg) *Modified versions of this equipment are available for ASTM D2893
Dimensions: **Oxidation Characteristics of Extreme Pressure Lubricating Oils and
8-place model: 29 Cu. ft. AOCS CD12-57 Fat Stability-Active Oxygen Method. Information will be
12-place model: 29 Cu. ft. furnished upon request.

120
Oxidation
30- and 60-Place Oxidation Baths
Convenient operation and servicing of thirty or sixty test cells
Complete bath temperature, water level, air flow and condenser water systems
Constant temperature water baths for high volume oxidation stability
applications. Provides temperature control, metered air flow and condenser
water supply controls for as many as thirty or sixty cells in a single system,
eliminating the need for multiple water and electrical feeds and oxygen supply
tanks. Microprocessor PID control provides quick temperature stabilization
without overshoot, and the bath is protected by a redundant overtemperature
control circuit that interrupts power should bath temperature exceed a
programmed cut-off point. Display provides actual setpoint temperature
values in C/F format. Communications software (RS232, etc.),
ramp-to-set and other enhanced features are available as extra cost options.
A 6 or 12kW heat exchanger with heavy duty magnetic drive circulation pump
provides rapid and uniform heat transfer throughout the bath. Bath liquid
depth is automatically maintained within ASTM specified tolerances by an
electronic water level control system. Two banks of individually controlled
flowmeters maintain the required oxygen flow rate to each test cell, and Advanced Communications Software Package for Data Management
condenser water control valves for each cell are mounted on manifolds along
the sides of the bath. A centrally mounted trough collects condenser waste 12-Place Solid-Block Oxidation Bath
water for convenient disposal or recirculation through an external cooling Accommodates twelve oxidation cells
device. Bath interior is constructed of heavy gauge welded stainless steel. All Microprocessor digital temperature control
components are easily accessible for servicing if required. Supplied with a Constant temperature aluminum block oxidation bath with flowmeters and
sturdy finished angle-iron frame for floor standing installation. Order oxidation condenser water manifold for twelve cells. Insulated solid block design
cell glassware and accessories separately. provides efficient operation at temperatures of up to 450F (232C).
Specifications Microprocessor temperature control unit features digital setpoint and display
Conforms to the specifications of: and built-in overtemperature protection. Includes individual flowmeters and
ASTM D943, D2274, D2893*, D4310, D6158; ISO 4263, 12205 control valves for each cell, delivering air flow at the rate of 3L/h. Condenser
AOCS CD12-57*; DIN 51586, DIN 51587; NF M 07-047; NF T 60-150 water manifold has individual control valves for each cell. Order oxidation cell
Temperature Control Stability: 0.1C (0.2F) glassware and accessories separately.
Oxygen Flow Rate: 3L/h to each test cell, individually controlled Specifications
Bath Capacity: Conforms to the specifications of:
30-place model: 60 gal (227L) ASTM D943, D2274, D2893*, D4310, D6158; AOCS CD12-57*;
60-place model: 114 gal (432L) DIN 51586, 51587; ISO 4263, 12205; NF M 07-047; NF T 60-150
Electrical Requirements: Testing Capacity: 12 oxidation cells
30-place model: 220-240V 50/60Hz, Single Phase, 28A Maximum Temperature: 450F
60-place model: 220-240V 50/60Hz, Single Phase, 54A Temperature Control Stability: 0.2F (0.1C)
Other electrical configurations are available upon request. Air Flow Rate: 3L/h
Dimensions lxwxh,in.(cm) Electrical Requirements: 220-240V 50/60Hz, Single Phase, 16A
30-place model: 43x55x52 (109x140x132)
60-place model: 43x78x52 (109x198x132) Dimensions lxwxh,in.(cm) Shipping Information
30x10x43 (76x25x109) Shipping Weight: 440 lbs (199.6kg)
Shipping Information Net Weight: 345 lbs (156.5kg) Dimensions: 12 Cu. ft.
Shipping Weight: Dimensions:
30-place model: 892 Ibs (404.6kg) 30-place model: 94 Cu. ft. Solid block baths meet temperature control and other requirements of ASTM
60-place model: 995 lbs (451.3kg) 60-place model: 148 Cu. ft. and related methods. While the aluminum block design offers operating
advantages over the standard oil bath, it should be noted that many applicable
Ordering Information specifications for this test call for a liquid bath medium.
Catalog No.
K12330 30-Place Oxidation Stability Bath, 220-240V 60Hz Ordering Information
K12339 30-Place Oxidation Stability Bath, 220-240V 50Hz Catalog No.
K12300 60-Place Oxidation Stability Bath, 220-240V 60Hz K12201 12-Place Solid Block Oxidation Bath,
K12395 60-Place Oxidation Stability Bath, 220-240V 50Hz 220-240V 50/60Hz
Photograph, thermometers, and additional accessories for
oxidation stability testing appear on page 122. *Modified versions of this equipment are available for ASTM D2893
Oxidation Characteristics of Extreme Pressure Oils and AOCS CD12-57 Fat
*Modified versions of this equipment are available for ASTM D2893 Oxidation Stability-Active Oxygen Method. Information will be furnished upon request.
Characteristics of Extreme Pressure Lubricating Oils and AOCS CD12-57 Fat
Stability Active Oxygen Method. Information will be furnished upon request.
Available option for 30- and 60-place Oxidation Bathstemperature/pressure Digital Flowmeter option
is available for this unit.
recorder with built-in alarms for low pressure and over/under temperature.
Please call or write for specifications and ordering information.

121
Oxidation
K12300 60-Place Oxidation Bath
Shown with optional pressure-temperature recorder
Oxidation Cell Glassware and Accessories Iron-Copper Catalyst

For ASTM D943 and D4310
Ordering Information Ordering Information
Catalog No. Catalog No.
K12281 Oxidation Cell Assembly for ASTM D943 and D4310 K12210 Catalyst Coil
Includes oxidation cell, condenser, oxygen delivery tube, Low-metalloid steel wire and electrolytic copper wire
thermometer bracket, oil level indicator strip, syringe wound in a double spiral conforming to ASTM
sampling tube, sampling tube holder, spacer, specifications. Packed in a sealed glass tube with a
PTFE stopper and O-rings nitrogen atmosphere. Ready for use.
K122-0-18 Oxygen Delivery Tube K24000 Wire Coiling Mandrel
K122-0-19 Oxidation Test Tube Mounts on bench for winding steel and copper wire into
K122-0-20 Condenser catalyst coils meeting ASTM specifications.
K122-0-21 Thermometer Bracket K12250 Steel Wire
K122-0-22 Oil Level Indicator Strip Low metalloid steel wire, 0.0625" (1.59mm) diameter,
K122-0-23 Syringe Sampling Tube Holder for catalyst coils. Supplied in 1000 ft (304.8m) lengths.
K122-0-27 PTFE Stopper K12260 Copper Wire
K122-0-28 Syringe Sampling Spacer Electrolytic copper wire, 0.064" (1.63mm) diameter, for
K122-0-30 Syringe Sampling Tube catalyst coils. Supplied in 1000 ft (304.8m) lengths.
AS568-009-V14 O-rings 380-100-001 Silicone Carbide Paper
Used to polish steel and copper wire prior to winding
For ASTM D2274, order one each K122-0-18 Oxygen Delivery Tube, into catalyst coils. 100 grit.
K122-0-19 Oxidation Test Tube, and K122-0-20 Condenser for each cell.
For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections Thermometers
Catalog No.
Digital Flowmeter option 250-002-001 Oxidation Cell Thermometer
is available for this unit. Range: 80 to 100C. For ASTM D943 and D4310.
250-000-40C ASTM 40C Thermometer
Range: 72 to 126C. For constant temperature baths.
122
Oxidation Stability of Mineral Insulating Oils
Test Method
Determines oxidation stability of mineral transformer oils by measuring
the amount of sludge and acid formed under prescribed accelerated
aging conditions.
Oxidation Stability Bath

Conforms to ASTM D2440 specifications
Microprocessor temperature control with digital display and
overtemperature cut-off
Six-sample testing capacity
Constant temperature oil bath for testing oxidation stability of mineral
insulating oils. Immerses six oil receptacles at the required depth per
ASTM specifications at 110C 0.5C, and controls oxygen flow to each
sample at the rate of 1L/h 0.1L/h through six independent flowmeters
mounted on a common manifold. Insulated double-wall stainless steel
bath has microprocessor temperature control with C/F switchable
digital setpoint and display. Operator and equipment are protected by an
overtemperature control circuit which automatically interrupts power to
the unit when bath temperature exceeds a programmed cut-off point.
Communications software (RS232, etc.), ramp-to-set and other enhanced
features are available as extra cost options. Contact your Koehler
representative for information. Order bath thermometer drying tower and
catalyst separately.
K12100 Oxidation Stability Bath,
115V 60Hz 1
K12100 Oxidation Stability Bath
K12190 Oxidation Stability Bath,
220-240V 50/60Hz
Specifications
Conforms to the specifications of: Accessories
ASTM D2440 K12130 Copper Catalyst Coils 1
Capacity: Six samples Sealed in a glass jar with a nitrogen
Temperature Range: ambient to 260F (127C) atmosphere. Pack of 24 (12 sets)
Circulator: 120hp impeller 332-005-010 Drying Tower 1
Bath Capacity/Medium: 2.5 gal (9.5L) white technical oil 250mL with ground glass stopper
Electrical Requirements: and side tubes
115V 60Hz, Single Phase, 8.1A 332-005-011 Glass Filter Crucible 1
220-240V 50/60Hz, Single Phase, 4.2A 250-000-95C ASTM 95C Thermometer 1
Included Accessories Range: 100 to 130C
Oil Receptacle and Head (6) 355-001-001 White Technical Oil 3
1 gal container. See page 8 for specifications.
Dimensions lxwxh,in.(cm) 355-001-003 White Technical Oil 1
14x15x22 (36x38x56) 5 gal container. See page 8 for specifications.
Net Weight: 31 lbs (14.1kg)
Shipping Information For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections
Shipping Weight: 61 lbs (27.7kg) on pages 184 through 191.
Dimensions: 14.4 Cu. ft.

123
Corrosiveness and Oxidation Stability
Corrosiveness and Oxidation Stability of
Hydraulic Oils, Aircraft Turbine Engine Lubricants,
and Other Highly Refined Oils
Test Method
Evaluates the ability of a lubricant to resist oxidation and the formation
of corrosive acid compounds by subjecting a sample to accelerated
oxidation conditions in a catalytic environment. The sample is
maintained at elevated temperature and subjected to a controlled air
flow while in the presence of a series of test specimens made of
metals commonly found in actual service conditions.
Corrosiveness and Oxidation Stability Test Apparatus

Models for ASTM, Federal and IHC test methods
Six-sample testing capability
Solid aluminum block design
Microprocessor temperature control with digital display and
overtemperature protection
Constant temperature block baths for corrosivity and oxidation stability
determinations on hydraulic oils, aircraft turbine lubricants, transmission
fluids and other highly refined oils. Insulated aluminum block provides
safe, efficient performance at operating temperatures of up to 750F
(399C). Microprocessor temperature control has C/F switchable digital
setpoint and display. Operator and equipment are protected by an
overtemperature control circuit which automatically interrupts power to
the unit should block temperature exceed a programmed cut-off point.
Communications software (RS232, etc.), ramp-to-set and other enhanced
features are available as extra cost options. Contact your Koehler
representative for information. Air flow is controlled at the specified rate
by six individually adjustable flowmeters mounted on a common manifold.
K35100 FTM 791-5307 Model with accessory glassware Includes inlet valve and outlet fitting for condenser water supply and
support rack for glassware.
Specifications Ordering Information
ASTM D4636, D5968, D6594; FTM 791-5307, 791-5308;
Corrosivity and Oxidation Stability Test Apparatus 1
IHC BT-10; DIN 51394
K35100 ASTM D4636, D5968 and FTM 791-5307 Model,
Capacity: 6 test cells
220-240V 50/60Hz
Temperature Range:125 to 750F (51.7 to 399C)
K35000 FTM 791-5308 Model,
Temperature Control Stability: 1F (0.5C)
220-240V 50/60Hz
Air Flow Rate: ASTM D4636/FTM 791-5307: 10L/h
K35300 IHC BT-10 Model,
FTM 791-5308: 3L/h and 5L/h (dual range flowmeters)
220-240V 50/60Hz
IHC BT-10: 3L/h (50mL/min.)
Electrical Requirements: 220-240V 50/60Hz, Single Phase, 15.9A
Thermometers
Dimensions lxwxh,in.(cm) 250-000-08F ASTM 8F Thermometer
3212x1412x4112 (83x37x105) Range: 30 to 760F
Net Weight: 271 lbs (122.9kg) 250-000-08C ASTM 8C Thermometer
Range: 2 to +400C
Shipping Information
Shipping Weight: 375 lbs (170.1kg)
Dimensions: 18.5 Cu. ft. on pages 184 through 191.

124
Corrosiveness and Oxidation Stability
Glassware, Test Specimens and Accessories Metal Test Specimens
Catalog No. Order Qty Catalog No.
ASTM D4636, D5968, D6594 and FTM 791-5307 Washer Shaped Specimens for ASTM D4636 Standard Procedure
K351-0-1 Sample Tube 6 and for FTM 791-5307
K351-0-2 Sample Tube Head 6 K35110 Bronze
K351-0-3 Air Tube 6 K35120 Mild Steel
K351-0-4 Thermocouple Tube 6 K35130 Aluminum Alloy
K351-0-5 Condenser, Allihn Type 6 K35140 Magnesium
K351-0-6 Oil Sampling Tube (for D4636) 6 K35150 Steel M50
K351-0-7 Spacer 36 K35160 Silver
K351-0-8 PTFE Adapter 6 K35170 Titanium
K351-0-13 Oil Sampling Tube (for D5968 and FTM 791-5307)
K351-0-14 Specimen Hanger (for D6594) Square Shaped Specimens for ASTM D4636 Alternate Procedure
K293-0-12 Thermocouple, Type J 6 and for FTM 791-5308
K29319 Digital Thermometer, 220-240V 1 K35010 Copper
Microprocessor based digital thermocouple K35020 Mild Carbon Steel
thermometer with ten-channel input. K35030 Aluminum Alloy
Monitors Type J thermocouples from sample tubes. K35040 Magnesium Alloy
K35090 Test Panel Assembly Fixture 1 K35050 Cadmium Plated Steel
Holds square-shaped metal specimens K35060 Silver
for tying with cord (for ASTM D4636 Alternate K35070 Solid Cadmium (non standard)
Procedure and FTM 791-5308) K35080 Titanium (non standard)
K35095 Test Panel Assembly Fixture 1
Holds square-shaped metal specimens Square Shaped Specimens for ASTM D5968 and D6594
for tying with cord (for ASTM D5968) K35010 Copper
K35011 Lead
FTM 791-5308 K35012 Tin
K350-0-23 Test Tube 6 K35013 Phosphor Bronze
K350-0-24 Air Tube 6
K350-0-25 Condenser 6 Rectangular Shaped Specimens for IHC BT-10
K35090 Test Panel Assembly Fixture 1 K353-0-5 Aluminum
Holds square-shaped metal specimens K353-0-6 Copper
for tying with cord. K353-0-7 Steel
K353-0-8 Brass
IHC BT-10
K353-0-1 Test Cell 6 Polishing Materials
K353-0-2 Condenser 6 380-150-001 Silicone Carbide Paper, 150-grit, Pack of 50 sheets
K353-0-3 Air Tube 6 380-240-001 Silicone Carbide Paper, 240-grit, Pack of 50 sheets
K353-0-4 Ring Rod 6 380-150-000 Silicone Carbide Grain, 150-grit, 1 lb package
125
Oxidation
Oxidation Stability of Inhibited Mineral Turbine Oils
Oxidation Stability of Straight Mineral Oil
Oxidation Stability of Mineral Insulating Oil
Oxidation Stability of Inhibited Mineral
Insulating Oils
Oxidation Test For Lubricating Oil
Test Method
Oxidation stability is determined by exposing the sample to a measured
oxygen flow at elevated temperature in the presence of metal catalysts.
Oxidation Stability Apparatus (Cigre Bath)

Conforms to IP specifications
Twelve-sample testing capability
Microprocessor programmable high accuracy temperature control
Constant temperature aluminum block type bath for oxidation stability tests in
accordance with the Institute of Petroleum (IP) testing methods.
Accommodates twelve sets of oxidation and absorption tubes. Insulated block
bath operates efficiently at temperatures of up to 200C (392F).
Microprocessor PID control provides quick temperature stabilization without
overshoot, and the bath is protected by a an overtemperature control circuit
that interrupts power should block temperature exceed a programmed cut-off
point. Dual LED displays provide actual and setpoint temperature values in
C/F format. Communications software (RS232, etc.), ramp-to-set and
other enhanced features are available as extra cost options. Contact your
Koehler representative for information. A bank of twelve flowmeters on a
K56100 Cigre Bath with K56110 Glassware movable stand regulates oxygen flow at 1 0.1L/h to each oil sample per IP
specifications. Includes soap bubble flowmeter for checking oxygen flow rate.
Ordering Information Specifications
Catalog No. Order Qty IP 48, IP 280, IP 306, IP 307, IP 335
K56100 Oxidation Stability Apparatus Testing Capacity: Twelve samples
115V 60Hz 1 Temperature Range: 80 to 200C
K56190 Oxidation Stability Apparatus Temperature Uniformity: 0.2C
220-240V 50/60Hz Air Flow Control:
K56200 Oxidation Stability Apparatus Standard Model: 1L/h to each sample
115V 60Hz IP 48 Model: 15L/h to each sample
For IP 48 Method. Electrical Requirements:
K56290 Oxidation Stability Apparatus 115V 60Hz, Single Phase, 12.1A
220-240V 50/60Hz 220-240V 50/60Hz, Single Phase, 6.3A
For IP 48 Method
Accessories Included Accessories Shipping Information
K56110 Set of Glassware
Soap Bubble Flowmeter Shipping Weight: 245 lbs (111.1kg)
Includes one each oxidation and absorption tube.
Dimensions: 16.7 Cu. ft.
For IP 48, IP 280, IP 306, IP 307, IP 335 12 Dimensions
250-000-09C ASTM 9C Thermometer Bath: dia.xh,in.(cm)
Range: 5 to +110C 17x22 (43.2x55.9)
(equivalent to IP 15C Thermometer) 1 Flowmeter Stand: lxwxh,in.(cm) For NIST traceable certified thermometers,
250-000-41C ASTM 41C Thermometer 24x8x3014 (61x20.3x76.8) please refer to the ASTM Thermometers
Range: 98 to 152C Net Weight: 186 lbs (84.4kg) sections on pages 184 through 191.
(equivalent to IP 81C Thermometer)
A liquid bath version of this equipment to perform the proposed ASTM test
for High Temperature Stability of Distillate Fuels is also available. Please
contact Koehlers Customer Service for additional information.
126
Thermal Oxidation Stability of Automotive Gear Lubricants
Test Method Ordering Information
The L-60-1 Performance Test determines the deterioration of gear Catalog No.
lubricants under severe thermal oxidation conditions. The sample K18660 L-60-1 Performance Test Apparatus, 220-240V 60Hz
lubricant is tested for 50 hours in a standardized gear box operating under K18650 L-60-1 Performance Test Apparatus, 220-240V 50Hz
a predetermined load. An elevated temperature and controlled air flow
Accessories
are maintained throughout the test and a copper catalyst is employed to
K18661 Test Kit, for one test. Includes GA34 test gear, GA50
accelerate the breakdown. At the end of the test period, various lubricant
test gear, R-14 test bearing, viton shaft seals (2),
properties are determined by standard testing methods, and the weight
O-ring seal, copper test strips (2)
loss of the catalyst is measured. The deposits that are formed on the gear
380-150-001 Silicone Carbide Paper, 150-grit (pack of 50)
box surfaces and the catalyst are examined and reported.
K18660 L-60-1
Performance Test
Apparatus
L-60-1 Performance Test Apparatus Specifications

Conforms to ASTM D5704 and STP512A L-60-1 Performance Test Conforms to the specifications of:
specifications. Performs the L-60-1 Thermal Oxidation Stability performance test ASTM D5704; STP512A L-60-1 Performance Test
for API GL-5 gear lubricant service. Consists of a standardized gear box assembly (formerly CRC L-60 Test); FTM 791-2504
with motor drive system and digital indicating controls for all test functions. Controls and Monitors:
Gear Case and Drive System Sample Oil Temperature: C/F, digital setpoint and display, user adjustable
Two spur gears and a test bearing are operated inside a machined stainless Overtemperature Limit Control: F, user acceptable
steel case with removable window. The drive gear shaft is coupled to a heavy Heating Chamber Air Temperature:C/F
duty ball bearing motor loaded by a 45 ampere alternator. The standard Air Flow: L/h, digital setpoint and display, user adjustable
L-60-1 test gear loading value of 128 watts generator output is precisely Test Gear Load: Volts DC, Amps. DC, digital display, user adjustable
maintained by a digitally indicated load bank. All gear box components are Sample Oil Temperature Recorder: Programmable microprocessor based
easily accessible for cleaning. strip chart recorder with digital display, C/F
Temperature Control Drive Motor: 1725rpm thermally protected ball bearing type
An insulated heating case with high volume blower encloses the gear box. Alternator: 45 ampere output
Sample oil temperature is maintained at 325F 1F (162.8 0.6C) by a digital Electrical Requirements:
indicating controller with PT-RTD sensor. A built-in microprocessor based 220-240V 60Hz, Single Phase, 15A
recorder produces a test oil temperature chart for reporting purposes. 220-240V 50Hz. Single Phase, 15A
Overtemperature protection is provided by a separate PT-RTD-sensed controller.
Air Flow Control Test Cabinet: 24x24x1412 (61x61x37)
A high accuracy mass flow controller with digital indication maintains air flow Control Cabinet: 2312x2312x1738 (60x60x44)
to the gear box at a constant 1.1L/h. The self correcting controller maintains Net Weight: 330 Ibs (149.7kg)
the setpoint flow rate regardless of fluctuations in air input pressure or
temperature. Test cabinet and control cabinet are finished in chemical Shipping Information
resistant polyurethane enamel. Test cabinet has a cover for access to the gear Shipping Weight: 498 Lbs (225.9kg)
box and a removable drive motor cover. Dimensions: 29.2 Cu. ft.
127
Rust Preventing Characteristics
Rust Preventing Characteristics of Inhibited
Mineral Oil in the Presence of Water
(Standard and Horizontal Disc Methods)
Test Method
Determines a lubricants ability to prevent rusting of metal surfaces.
Suitable for steam turbine oils, gear oils, hydraulic oils and other types of
inhibited mineral oils. A steel test specimen is immersed in a heated
mixture of sample oil and water which is stirred continuously during the
test. After the test period the specimen is examined for rusting. The
standard (ASTM D665) method uses a vertical specimen; the horizontal
disc method (ASTM D3603) uses both horizontal and vertical test surfaces.
Rust Preventing Characteristics Oil Bath

Conforms to ASTM D665, D3603 and NACE TM-01-72* specifications
Accommodates six sample beakers
Microprocessor programmable high accuracy temperature control
Constant temperature bath with stirrers for rust preventing characteristics
tests. Stirs sample-water mixtures at 1000rpm and controls temperature with
0.5C ( 1F) stability. Immerses test beakers at the proper depth per ASTM
specifications.
K30160 Rust Preventing Characteristics Bath
Microprocessor PID control provides quick temperature stabilization without
overshoot, and the bath is protected by an overtemperature control circuit that
Specifications interrupts power should bath temperature exceed a programmed cut-off point.
Conforms to the specifications of: Dual LED displays provide actual and setpoint temperature values in C/F
ASTM D665, D3603, D6158; NACE TM-01-72*; IP 135; ISO 7120;
format. Communications software (RS232, etc.), ramp-to-set and other
DIN 51355**, DIN 51585; FTM 791-4011, 791-5315**; NF T 60-151
enhanced features are available as extra cost options. Contact your Koehler
Testing Capacity: Six (6) 400mL sample beakers
representative for information.
Maximum Temperature: 104C (220F)
Temperature Control Stability: 0.5C (1F) Stainless steel stirrer paddles are driven by a ball bearing type motor through
Drive Motor: 112hp induction motor an improved pulley drive-roller bearing arrangement. Paddles can be raised
Bath Medium: 11 gal (41.6L) white technical oil and lowered for placement of sample beakers in the bath. Includes test
Electrical Requirements: specimens, holders and beaker covers for ASTM D665 or D3603 testing
115V 60Hz, Single Phase, 13.0A (see specifications and ordering information). Stainless steel bath includes
220-240V 50 or 60Hz, Single Phase, 6.8A perforated support shelf for beakers and two-position cover plate that adjusts
Included Accessories for either ASTM D665 or D3603 testing. Long-lasting polyester drive belt
ASTM D665 Models (K30160, K30165, K30166) improves reliability. Drive train components are protected by a removable steel
Steel Test Specimens (6) guard. All exterior surfaces have stainless steel or chemical resistant
Type 2 Plastic Specimen Holders (6) polyurethane enamel finishes.
Plastic Beaker Covers (6)
ASTM D3603 Models (K30161, K30167, K30168)
Horizontal Disc Test Assembly (6) consisting of: Catalog No.
plastic beaker cover Rust Preventing Characteristics Oil Bath
horizontal test specimen For ASTM D665
vertical test specimen K30160 Rust Preventing Characteristics
fluorocarbon washer Oil Bath, 115V 60Hz
plastic cap K30165 Rust Preventing Characteristics
stainless steel support rods and hardware Oil Bath, 220-240V 50Hz
Dimensions lxwxh,in.(cm) K30166 Rust Preventing Characteristics
3234x1414x27 (83x36x69) Oil Bath, 220-240V 60Hz
Net Weight: 79 lbs (35.8kg) For ASTM D3603
Shipping Information K30161 Rust Preventing Characteristics
Shipping Weight: 150 lbs (68kg) Oil Bath, 115V 60Hz
Dimensions: 16.2 Cu. ft. K30167 Rust Preventing Characteristics
Oil Bath, 220-240V 50Hz
**Accessories for these test methods are available upon request.
K30168 Rust Preventing Characteristics
Oil Bath, 220-240V 60Hz
with Koehler Customer Service. *To order this equipment for the NACE TM-01-72 test please turn to page 98.
128
Rust Preventing Characteristics
K30800 Horizontal Disk Assembly K30101 Specimen with Holder K30130 Chuck
Accessories Test Specimens

Catalog No. Order Qty Catalog No.
332-002-006 Test Beaker, 400mL 6 K30110 Steel Test Specimen for ASTM D665
for ASTM D665 & D3603 Machined to ASTM specifications. Without Holder
250-000-09F ASTM 9F Thermometer K30100 Test Specimen with Type 2 Plastic Holder
Range: 20 to 230F 7 for ASTM D665
250-000-09C ASTM 9C Thermometer K30119 Test Specimen with Type 1 Plastic Holder
Range: 5 to +110C for ASTM D665
K30130 Chuck for polishing test specimens 1 K30101 Test Specimen with Type 2 PTFE Holder
Includes locknut and shaft for K30810 Horizontal Test Specimen for ASTM D3603
mounting on accessory drive motor. K30820 Vertical Test Specimen for ASTM D3603
K30150 Drive Motor K30800 Horizontal Disc Rust Test Assembly for
Drives K30130 Chuck. Mounted on base. ASTM D3603. Includes polycarbonate beaker
115V 60Hz 1 cover, two stainless steel support rods,
K30180 Drive Motor disc carrier and one each horizontal and
Similar to K30150 but for operation vertical test specimens.
on 220-240V 50Hz
380-150-002 Aluminum Oxide Cloth, 150-grit for For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections
preliminary grinding of test specimens on pages 184 through 191.
Pack of 50
380-240-002 Aluminum Oxide Cloth, 240-grit for 1
final polishing of test specimens
Pack of 50
K30140 Auxiliary Stirrer Blade - Attaches to stirrer shaft - for
testing heavier than water samples - ASTM D665.
Procedure C.
129
Corrosion of Lead by Lubricating Oils
Test Method Specifications
Measures the corrosiveness of lubricating oils to lead in the presence Conforms to the specifications of:
of a copper catalyst. Lead and copper test panels are rotated in the test FTM 791-5321
lubricant under specified test conditions, and the degree of corrosion Testing Capacity: 6 lubricant samples
is determined by the change in weight of the lead panel. Maximum Temperature: 199C (390F)
Temperature Control Stability: 0.05C (0.1F)
Lead Corrosion Test Apparatus Air Flow Control: 0.940.047L/min.
(20.1 Cu. ft./hr) six (6) flowmeters
Conforms to FTM 791-5321 specifications mounted on a common manifold
Six-sample capacity Electrical Requirements:
Microprocessor programmable high accuracy temperature control 220-240V 60Hz, Single Phase, 14.5A
Constant temperature apparatus rotates copper and lead test panels in 220-240V 50Hz, Single Phase, 14.5A
lubricant samples to determine corrosiveness to lead per FTM specifications. Included Accessories Dimensions lxwxh,in.(cm)
Panels are rotated at 600rpm in samples maintained at 163C (325F) and Copper Test Panels (6) 39x25x47 (99x64x119)
aerated at 0.94L/min. (2.0 Cu. ft./hr.). Lead Test Panels (6) Net Weight: 214 lbs (97kg)
Test panel shafts ride on ball bearing spindles driven by a 115hp motor. A Mounting Hardware for Panels
Shipping Information
counterbalanced support bar positions the drive shaft for testing or for Shipping Weight: 330 lbs (150kg)
mounting and removal of test panels. When the support bar is raised, Dimensions: 33.5 Cu. ft.
a safety microswitch automatically stops the drive motor to prevent
splashing of hot oil. Ordering Information
Fully insulated bath features double-wall stainless steel construction, with Catalog No. Order Qty
a built-in support rack to suspend test cells vertically at the proper depth. K29900 Lead Corrosion Apparatus,
Microprocessor PID control provides quick temperature stabilization without 220-240V 60Hz 1
overshoot, and the bath is protected by an overtemperature control circuit that K29990 Lead Corrosion Apparatus.
interrupts power should bath temperature exceed a programmed cut-off point. 220-240V 50Hz
Dual LED displays provide actual and setpoint temperature values in C/F
format. Communications software (RS232, etc.), ramp-to-set and other Accessories
enhanced features are available as extra cost options. Contact your Koehler K29910 Borosilicate Glass Sample Tube 6
representative for information. A 120hp stirrer thoroughly circulates the bath 250-000-16F ASTM 16F Thermometer
medium for temperature uniformity. Redundant overtemperature Range: 85 to 392F 1
protection is provided by a built-in backup thermostat. Flowmeters and 250-000-16C ASTM 16C Thermometer
valves mounted on a convenient manifold provide individual air flow Range: 30 to 200C
control for each test cell. K29920 Lead Test Panels
K29930 Copper Test Panels
Digital Flowmeter option For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections
is available for this unit. on pages 184 through 191.
Stability of Lubricating Oils (Work Factor)

Determines the stability of a lubricating oil when subjected to an endurance Conforms to the specifications of: FTM 791-3451.4
test in a journal bearing operated under prescribed conditions. After a 100 Electrical Requirements: 220-240V, 3 Phase, 50/60Hz, 20A
hour test period, the work factor is computed from measured changes in Dimensions lxwxh,in.(cm) Shipping Information
viscosity, neutralization number and carbon residue.
50x40x60 (127x102x152) Shipping Weight: 1660 lbs (753kg)
Navy Work Factor Machine Net Weight: 1378 lbs (625.1kg) Dimensions: 110 Cu. ft.
Conforms to FTM 791-3451 specifications
Complete apparatus for the Navy Work Factor stability test for lubricating oils.
Consists of bearing and journal, bearing loading device with calibrated springs,
5hp drive system with variable speed control, oil circulation system, and full Catalog No.
instrumentation. Operates the journal bearing at 2000 or 3000rpm under a K30000 Navy Work Factor Machine,
specified load. Oil system pressure is maintained at a constant 15 psig 220-240V Specify 50 or 60Hz when ordering
(103 gauge kPa) throughout the test. Includes digital displays of oil pressure K30010 Replacement Test Bearing
and temperature and a built-in strip chart recorder for hard copy test reports.
130
Copper Corrosion from Petroleum Products
Test Method Ordering Information
The Copper Strip Tarnish Test assesses the relative degree of corrosivity of Catalog No. Order Qty
petroleum products, including lubricating oils. A polished copper strip is K25330 Copper Strip Test Tube Bath, 115V 60Hz 1
immersed in 30mL of sample at elevated temperature. After the test K25339 Copper Strip Test Tube Bath, 220-240V 50/60Hz
period, the strip is examined for evidence of corrosion and a classification
K25312 Vented Cork
number from 1-4 is assigned based on a comparison with the ASTM Copper
Strip Corrosion Standards. Accessories
K25080 Copper Test Strips 17
Copper Strip Tarnish Test Apparatus 12.5x1.5-3.0mmx75mm to ASTM specifications
Conforms to ASTM D130, D6074, D6158 and related specifications
332-004-004 Test Tube, 25x150mm 17
The complete apparatus for the Copper Strip Tarnish Test for lubricating oils
332-004-002 Viewing Test Tube 17
consists of:
Test Tube Bath Protects copper strip during inspection or storage
Copper Strips K25100 ASTM Copper Strip Corrosion Standard 1
Test Tubes Colored reproductions of tarnished strips encased
ASTM Copper Strip Corrosion Test Standard in a plastic plaque
Surface Preparation Accessories 380-220-001 Silicone Carbide Paper, FEPA Grade, 220 grit
For polishing of copper strips prior to testing
Test Tube Bath Pack of 50 sheets
Accommodates 17 test tubes 380-150-003 Silicone Carbide Grain, FEPA grade, 150 grit
Temperature range to 190C (374F) For final polishing of copper strips prior to testing
Microprocessor temperature control with digital display and 1 lb package
overtemperature protection. K25000 Polishing Vise 1
Constant temperature bath immerses 16 test tubes for copper strip tarnish tests Holds copper strip firmly in place without marring the
of products not requiring a test bomb. Microprocessor temperature control has
edges. Stainless steel. mounted on a composition base
C/F switchable digital setpoint and display. Operator and equipment are
K25090 Multi-Strip Polishing Vise. Similar to K25000 but 1
protected by an overtemperature control circuit which automatically interrupts
capable of holding four strips at a time
power to the unit should bath temperature exceed a programmed cut-off point.
Welded stainless steel double-wall construction with built-in support rack. Fully 250-000-12F ASTM 12F Thermometer, Range: 5 to +215F 1
insulated. For complete specifications, please refer to page 90. 250-000-12C ASTM 12C Thermometer, Range: 20 to +102C
Bearing Compatibility of Turbine Oils

Evaluates the in-service stability of turbine lubricants by running a Conforms to the specifications of: FTM 791-3452
sample-lubricated babbit journal bearing for an extended period at high Journal Drive Motor: 5hp variable speed, with digital 0-3500rpm control.
speed under controlled conditions of load, lubricant flow and temperature. Fan cooled with thermal overload protection.
The change in various properties (viscosity, carbon residue, acidity) is Lubricant Flow: 3.8L/min. gear pump recirculating 1.9-23L/min.
measured at the end of the endurance test and the bearing is cleaned and of test lubricant to support bearing and test bearing.
examined for evidence of deposits, corrosion and other changes. Digital oil pressure circulation.
Temperature Control: Sump temperature (0-500F) with digital indication
Bearing Compatibility Tester and recording of temperature at bearing housing, sump and in-line.
Conforms to FTM 791-3452 specifications Bearing Load: Hydraulic loading device maintaining 1520 kPa (220 psig) on
Digital-indicating controls and built-in temperature recorder the loading bearing.
Tests the bearing compatibility (lacquering, deposits, corrosion) and stability
of turbine lubricants when subjected to an endurance test. Consists of bearing
200-240V 50/60Hz, 3-Phase, 20A
housing assembly with test bearing and support bearings, hydraulic loading
380V 50/60Hz, 3-Phase, 12A
device, oil circulation system with thermostatic and hydrostatic control, and
powerful 5hp variable speed drive system. Digital LCD controls monitor oil 440V 50/60Hz, 3-Phase, 10A
pressure, oil temperature and spindle rpm, and a built-in strip chart recorder Ordering Information
plots oil temperature at three different pointsat the bearing housing, in-line,
and in the reservoir. Equipped with overtemperature and low pressure cut-off Catalog No. Order Qty
switches and a cartridge oil filter for convenient flush run operation. All K29800 Bearing Compatibility Tester 1
components are mounted in a sturdy angle iron frame. A removable steel Specify electrical requirements when ordering.
guard protects drive train components. Accessories
K29801 Test Bearing
Dimensions lxwxh,in.(cm) Shipping Information
48x36x54 (122x91x137) Shipping Weight: 1582 lbs (717.6kg) For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections
Net Weight: 1300 lbs (589.7kg) Dimensions: 101.7 Cu. ft. on pages 184 through 191.
131
Cloud Point and Pour Point of Petroleum Products
Test Method
Cloud point and pour point are indicators of the lowest temperature of
utility for petroleum products. The sample is periodically examined while
it is being cooled in the cloud and pour point apparatus. The highest
temperature at which haziness is observed (cloud point), or the lowest
temperature at which movement of the oil is observed (pour point),
is reported as the test result.
Cloud and Pour Point Test Equipment

Conforms to ASTM D97, D2500 and related specifications
Compact four-place portable chamber
Mechanically refrigerated models with factory preset cold baths
Cloud and Pour Point ChamberImmerses four copper test jackets in
suitable freezing mixtures at the required depth per ASTM specifications.
Available with inlet and outlet connections for circulating refrigerated
coolant from an external source. Consists of steel exterior housing with
polyurethane enamel finish and all copper interior for corrosion
resistance. Removable composition top plate and 12" (13mm) cork
insulation around interior aid in cold retention. Supplied with copper
jackets, gaskets, disks, and thermometer holders for test jars and cooling
bath. Order test jars and thermometers separately.
K46100 Refrigerated Bench Model
Mechanically Refrigerated BathsBench-model and floor-model test
Ordering Information units with multiple four-jacket mechanically refrigerated baths, each
Catalog No. factory preset at a different temperature for convenient cloud and pour
Cloud and Pour Point Chamber point testing. Bench model has three baths, set at +32, 0 and -27F (0, -18
K46000 Cloud and Pour Point Chamber and -33C); floor model available with either four or five baths, set at +32, 0,
K46001 Cloud and Pour Point Chamber, with inlet/outlet fittings -27 and -60F (0, -18, -33 and -51C) and +32, 0, -27, -60 and -92F (0, -18,
-33, -51, and -69C) respectively. Each bath has a phenolic top plate with
Refrigerated Models: ports for thermometer and four copper test jackets. Synthetic sponge
K46100 Cloud and Pour Point Bath, Bench Model, 115V 60Hz covers over each top plate and gasketed hoods over each bath prevent
K46195 Cloud and Pour Point Bath, Bench Model, 220-240V 50Hz excessive ice accumulation around the test jackets. Cascade hermetic
K46196 Cloud and Pour Point Bath, Bench Model, 220-240V 60Hz refrigeration system provides reliable long term service. Bath interior is made
K46300 Cloud and Pour Point Bath, Floor Model, 115V 60Hz of stainless steel, cabinet is constructed of polyester-epoxy finished steel
K46395 Cloud and Pour Point Bath, Floor Model, 220-240V 50Hz housing. Floor model rides on swivel castors. Supplied with test jackets,
K46396 Cloud and Pour Point Bath, Floor Model, 220-240V 60Hz gaskets, disks, and thermometer holders for test jars and cooling baths.
K46500 Cloud and Pour Point Bath, Floor Model, 5-Bath, 115V 60Hz
K46595 Cloud and Pour Point Bath, Floor Model, 5-Bath, 220-240V 50Hz
Specifications
K46596 Cloud and Pour Point Bath, Floor Model, 5-Bath, 220-240V 60Hz
ASTM D97, D2500, D5853, D6074, D6158; IP 15, 219;
ISO 3015, 3016; DIN 51597; FTM 791-201; NF T 60-105
Accessories
332-004-001 Test Jar
Model K46100 Refrigerated Bench Model:
Clear, flat bottom jar with sample height graduation
115V 60Hz, Single Phase, 12.2A
250-000-05F ASTM 5F Thermometer, range: 36 to +120F
220-240V 50/60Hz, Single Phase, 6.9A
250-000-05C ASTM 5C Thermometer, range: 38 to +50C Model K46300/K46500 Refrigerated Floor Model:
250-000-06F ASTM 6F Thermometer, range: 112 to +70F 115V 60Hz, Single Phase, 17.7A
250-000-06C ASTM 6C Thermometer, range: 80 to +20C 220-240V 50/60Hz, Single Phase, 9.7A
K46120 Cork Disk
K46130 Foam Sponge Disc Dimensions Shipping Information
K46000: dia.xh,in.(cm) Shipping Weight:
AS568-219 Gasket, for test jar
1012x12 (27x30) K46000: 18 lbs (8.2 kg)
K460-0-8 Thermometer Holder, for test jar
K46100: lxwxh,in.(cm) K46100: 550 lbs (250 kg)
K460-1-7B Copper Jacket
30x28x35 (76x71x89) K46300/K46500: 605 lbs (275 kg)
K46300/K46500: lxwxh,in.(cm) Dimensions:
For NIST traceable certified thermometers, please refer to the ASTM Thermometers sections on 44x38x4 (112x97x115) K46000: 2.6 Cu. ft.
pages 184 through 191. Net Weight: K46100: 14.1 Cu. ft.
Custom configurations of this bath are available. Please contact Koehler Customer Service for K46000: 14 lbs (6.3 kg) K46300/K46500: 60.6 Cu. ft.
additional information. K46100: 340 Ibs (155 kg)
K46300/K46500: 392 lbs (178 kg)

132
Automated Cloud Point and Pour Point of Petroleum Products
Test Method
For Petroleum Products, cloud point and pour point of a petroleum product
is an index of the lowest temperature of its utility for certain applications.
The specimen is cooled at a specified rate and examined periodically. The
highest temperature at which a cloud is first observed at the bottom of the test
jar is recorded as the cloud point. The lowest temperature at which movement
of the specimen is observed is recorded as the pour point.
Automatic Cloud Point and Pour Point Analyzer with

Integrated Panel PC
Cloud Point Analyzer conforms to ASTM D2500, D5771, D5772, D5773
and related test methods
Pour Point Analyzer conforms to ASTM D97, D5853, D5950 and related
test methods
KLA-3-TS
Stand alone system with Integrated Touch Screen Panel PC Automatic Cloud & Pour Point
Direct Cooling system eliminates the need for solvent cooling baths Analyzer with Touch Screen
One-stage cooling system provides temperatures as low as -45C and
a two-stage cooling system down to -80C of rapid cooling, approaching -80C bath temperatures in approximately 15
Cloud Point measured by light pulsed emission on I.R spectrum minutes, and utilizes less electricity than standard cooling systems. The
through a coaxial fiber optic rapid cooling feature combined with a consistent cooling profile system
Pour Point measured by two PT100 detection probes placed on the provides repeatable results with high test reproducibility.
surface of the product and a mechanical moving arm bringing the test
jar to a horizontal position Multiple Configuration SystemThese automated sample cooling and
physical property measurement systems can be configured with one, two,
Cloud Point DetectionThe cloud point detection system provides automated three, four and six test positions with one of five possible analytical heads at
sample testing with the accuracy and repeatability in accordance with ASTM each position: cloud point, pour point, cloud & pour point, cold filter
D2500, D5771, D5772, D5773 and related international test methods. The plugging point and freezing point. Standard and customized multiple
sophisticated dynamic measuring system emits a light pulse every 1C from a configuration systems are readily available.
coaxial fiber optic cable positioned above the test sample. The light pulse is then
reflected off the silver bottom test jar to an optical sensor. The advanced software Specifications
package analyzes the response of the light pulse. The initial appearance of Conforms to the specifications of: Resolution: 0.06C
crystallization is monitored by light scattering, signifying the cloud point of the KLA-1-TS: ASTM D2500, D5771, Accuracy: 0.1C
sample. All clear and transparent oils are readily measured by the detection D5772, D5773; DIN 51597; IP 219, Repeatability / Reproducibility: as
system, regardless of sample color. IP 444, IP 445, IP 446; ISO 3015 per standard test methods or better
KLA-2-TS: ASTM D97, D5853, Data Storage: < 60,000 analyses
Pour Point DetectionThe pour point detection system provides automated D5950; IP 15, IP441; ISO 3016 Electrical Requirements:
sample testing with the accuracy and repeatability in accordance with ASTM D97, KLA-3-TS: ASTM D97, D2500, 115V 15% / 60Hz
D5853, D5950 and related international test methods. The automated operation D5771, D5772, D5773, D5853, 220V 15% / 50 to 60Hz
involves removing the sample from the cooling jacket at 3C intervals and tilting D5950; DIN 51597; IP 15, IP 219,
it to a 90 angle as prescribed by the test method until no flow is observed. Dimensions WxDxH,in.(cm)
IP441, IP 444, IP 445, IP 446; 26 x 2334 x 3112 (66x60x80)
Contact of the cold sample with the two PT100 detection probes positioned just ISO 3015, ISO 3016
above the surface liquid level when the test jar is tilted identifies sample flow. The Net Weight: 176.5 lbs (80kg)
Temperature Range:
test jar is automatically returned to the cooling jacket and sampled again until no One-Stage: +60C to -45C
flow is detected for 5 seconds. The pour point result is then reported at 3C Two-Stage: +60C to -80C
higher than the temperature at which the sample ceased to flow in accordance
with the test method. Ordering Information
Integrated Panel PC and Software PackageThe Automated Cloud and Pour Catalog No.
Point Analyzers are complete standalone systems featuring an integrated panel KLA-1-TS Auto Cloud Point Analyzer, Touch Screen (One-stage)
PC with an advanced software package. The 6.4 TFT/LCD touch screen display KLA-1-TS/2 Auto Cloud Point Analyzer, Touch Screen (Two-stage)
has a resolution of 640x480 with a 262K color scheme. All analytical parameters KLA-2-TS Auto Pour Point Analyzer, Touch Screen (One-stage)
are graphed and displayed in real time as well as recorded in Microsoft Excel KLA-2-TS/2 Auto Pour Point Analyzer, Touch Screen (Two-stage)
compatible file format. The software monitors the operation and performance of KLA-3-TS Auto Cloud & Pour Point Analyzer, Touch Screen (One-stage)
all the analyzer components for proper data measurement, including the solenoid KLA-3-TS/2 Auto Cloud & Pour Point Analyzer, Touch Screen (Two-stage)
valves, cooling system, pressure sensors, and the Platinum resistance PT100 Please specify voltage requirements when ordering.
Class A temperature probe. Accessories
Cooling SystemFor various user applications, the automated cloud and pour KLA-PT100-CAL Calibration Decade Box - PT100 Simulator
point systems are available with either one-stage cooling for temperatures as low KLA-DB-KIT Set of Connectors and Cables
as -45C or two-stage cooling for temperatures as low as -80C. The direct Extended Cooling Range down to -100C Available Upon Request.
cooling system features integrated gas CFC free motors compressors thus
eliminating the need for a solvent cooling bath. The direct system is capable
133
Dielectric Breakdown Voltage of Insulating Oils
Test Method
The majority of high-voltage transformers, cables, switchgears,
transducers, capacitors, and rectifiers use insulating oils for insulating
electrically live parts and to carry off thermal energy. The quality of
the insulating oil must be checked at regular intervals to ensure a
long equipment service life. The most important requirement of an
insulating oil is a high dielectric strength. Determination of the
dielectric breakdown voltage of insulating oils provides an early
detection method for any reduction in the insulating properties.
Automatic Portable Dielectric Breakdown Tester

Conforms to ASTM D877, D1816 and related test specifications
Output voltage: 75kV
Features 2.8 ultra bright color display for optimal readability and mobility
Built-in printer offers direct evaluation and reporting of results
Internal battery, external 12V power supply
Automatic Vernier function for electrode gap spacing
Measurement of Silicone based oils
Internal temperature measurement of oil sample
Bluetooth PC Connectivity and USB Flashdrive Capability
Specifications
ASTM D877, D1816; BS EN 60156; CEI EN 60156; IEC 156; VDE 0370 Pt. 5 K16175 Automatic Portable Dielectric Tester
Output Voltage: Up to 75kV rms symmetrical
Voltage measurement accuracy: 0 - 75kV 1kV Dimensions WxHxD,in.(cm)
Voltage slew rate: 0.5 - 10kV/s 16.9x11x9.85 (43x28x25)
Resolution (displayed): 0.1kV Net Weight: 48.5 lbs (22kg)
Power Supply: 85V - 264V, 47Hz - 63Hz, 12V external supply
Power consumption: 60VA Shipping Information
Internal rechargeable battery: 1 x 12V / 7.2Ah Shipping Weight: 54.5 lbs (24.7kg)
Switch-off time on flashover: < 5s Dimensions: 25x21x19in. (63.5x53.4x48.3cm)
Measurement of oil temperature: 0 - 100C / 32 - 212F
Temperature Resolution: 1C / 1.8F Ordering Information
Display: 2.8 color (ultra bright)
Catalog No.
Selectable Programs: ASTM D1816-04-1mm, ASTM D1816-04-2mm,
K16175 Automatic Dielectric Breakdown Tester, 0-75kVAC,
ASTM D877-02A, ASTM D877-02B, IEC 156/95
100-240V 50/60Hz
Customer-specific programs: Unlimited
PC Software: Included Accessories
Printer: Dot Matrix Hard Copy Output K16175-4 Transport Case
Interface: Bluetooth K16175-5 Test Vessel complete with electrodes for ASTM D1816
USB: USB memory stick K16175-6 Test Vessel complete with electrodes for ASTM D877
Operating Temperature: -5C - 45C (23F - 113F) K16175-23 IEC156 Test Cell with VDE Electrode
Storage Temperature: -20C - 60C (-4F K16175-24 IEC156 Test Cell with Sphere Electrode
K16175-12 Spacer Gauge, 1mm
Included Accessories K16175-13 Spacer Gauge, 2mm
Calibration Sheet AC Power Cable Integrated Battery K16175-14 Spacer Gauge, 2.5mm
User Manual PC Software Integrated Printer
134
Coking Tendency of Oil
K50100 Panel Coker
Test Method Specifications Dimensions lxwxh,in.(cm)

Determines the tendency of finished oils to form coke when in contact Conforms to the specifications of: Test Unit: 32x18x21 (81x46x53)
with surfaces at elevated temperatures for short periods. A sample of oil FTM 791-3462 Control Cabinet:
is mechanically splashed against an aluminum test panel at elevated Maximum Temperature: 18x12x18 (46x30x46)
temperature. After a specified test period, the amount of coke deposited on Test Panel: 400C (752F) Net Weight:
the panel is determined by weight. Sample Oil: 210C (410F) Test Unit: 50 lbs (22.7kg)
Temperature Control: Separate Control Cabinet: 25 lbs (11.3kg)
Panel Coking Test Apparatus controls for test panel and oil
temperature, with digital C/F Shipping Information
Conforms to FTM 791-3462 specifications digital setpoint and display Shipping Weight: 135 lbs (61.2kg)
Suitable as a screening test prior to performing engine tests Splashing Rate: 0-1800rpm, Dimensions: 26.7 Cu. ft.
Digitally controlled panel coking apparatus for finished lubricating oils, with digital display
consisting of mechanical splasher, splash chamber and sample oil reservoir Timer: 0-99.9 hr variable countdown
Test panel temperature and oil sump temperature are individually controlled by Flowmeter Range: 0.2-1.0L/hr Digital Flowmeter option
separate heaters with digital-indicating controllers. Mechanical splasher has a Oil Reservoir Capacity: 0.35 liter is available for this unit.
variable speed 0-1800rpm drive motor with digital indicating control. A high Electrical Requirements:
115V 60Hz, 8A
accuracy variable area flowmeter permits introduction of a corrosive acidic
atmosphere to increase the severity of the test. Equipped with a digital
countdown timer. Hinged safety cover has a port for fume removal and a
220-240V 50/60Hz, 5A ! Software compatible, inquire
safety interlock switch that interrupts power to the drive motor when the
cover is lifted.
K50100 Panel Coking Test Apparatus,
115V 60Hz
with cyclic timer 115V 60Hz
with cyclic timer 220-240V 50/60Hz
220-240V 50/60Hz
Accessories
K50101 Aluminum Test Panel 1
K50102 Stainless Steel Test Panel (Type 321) 1
135
Evaporation Loss of Lubricating Oils by the Noack Method
Test Method
For determining the evaporation loss of lubricating oils, particularly engine
oils. High temperatures can evaporate oil which may contribute to oil
consumption in an engine and can lead to a change in the properties of an
oil. A measured quantity of sample is placed in an evaporation crucible that
is then heated to 245.2C with a constant flow of air drawn through it for 60
minutes. The loss in mass of the oil is determined.
Automatic Non-Woods Metal Noack Evaporative

Apparatus
Conforms to ASTM D5800, Procedure B
6.5 Integrated Touch Screen Panel PC
Integrated Vacuum Pump with automatic electronic control system
Direct sample temperature measurement via PT100 probe
K44100 Automatic Non-Woods Metal Noack Evaporative Apparatus Equipped with high resistant Kalrez valve, inlet filter to remove
product residuals
USB port for connection to an external printer and/or external PC
Included Accessories Dimensions lxwxh,in.(cm) Storage capacity for more then 60,000 analysis
Integrated Touch Screen Panel PC 15.75x17.72x17.72 (40x45x45) CE Marked
Integrated Vacuum Pump Net Weight: 48.5 lbs (22 kg)
The Automatic Non-Woods Metal Noack Evaporative Apparatus tests for the
Inlet Filter
evaporation loss tendencies of lubricating oils at temperatures of up to 275C.
Evaporation Crucible
The newly designed electrically heated aluminum block allows for testing
Test Ball (10)
without the use of hazardous Woods Metal. The Noack tester is equipped with
Nozzle Cleaner
an Electronic regulator allowing for automatic control of temperature and
Crucible Holder
differential pressure. The system is managed by an integrated 6.5 Touch
Protective Gloves
Screen Panel PC by means of the Noack Evaluation Software run by a
Hook Wrench
Windows based operating system. The Evaluation Software is capable of
Pliers
recording all analytical parameters, allowing for user customizable parameters,
methods and result reports as well as printing graphs and test results.
Catalog No. Specifications
K44100 Automatic Non-Woods Metal Noack Conforms to the specifications of:
Evaporative Apparatus 115V 60Hz ASTM D5800 Procedure B; IP 421; DIN 51581
K44190 Automatic Non-Woods Metal Noack Capacity: 1 Sample
Evaporative Apparatus 220V 50/60Hz Temperature Range: 225C to 275C
Temperature Resolution: 0.01C
Accessories Temperature Accuracy: 0.2C
K44100-SFW Noack Evaluation Software Repeatability/Reproducibility: Meets or Exceeds ASTM D5800
K44100-1 Glassware Accessory Set Ambient Temperature: Max. 35C
Includes: 2L Glass Bottle (2), Rubber Stopper (4), Relative Humidity: Max 80%
Glass Delivery Tubes, Silicon Connection Tubing Heater Power: 420W
K44100-2 Stand for Glass Bottles with Inclined Manometer, Electrical Requirements:
0-50mm H2O 115V 60Hz
K44100-3 Noack Reference Oil, 1 Liter 220V 50/60Hz
KLA-DB-KIT Set of Calibration Connectors and Cables
KLA-PT100-CAL Calibration Decade Box PT100 Simulator
136
Additional Accessories
Additional equipment, materials and/or reagents are required to perform some Sludging Tendencies of Inhibited Mineral Oils............Pages 119-122
of the test procedures in the preceding pages. Please refer to the applicable
ASTM D4310
test method for further information, or contact Koehler for assistance.
Syringe, 50mL Flexible Tubing
Foaming Characteristics of Lubricating Oils................Pages 108-110 Acetone Detergent
n-Heptane Hydrochloric Acid
ASTM D892; IP 146; DIN 51566; FTM 791-3211, 791-3213
Chromic Acid Oxygen
Air Supply Toluene Filter Holder Membrane Filters
Acetone Isopropanol Separatory Funnel Weighing Bottle, 60mL
Desiccant Cotton Forceps Drying Oven
Water Separability of Petroleum Oils Nitrogen Vacuum Source
and Synthetic Fluids................................................................Page 111 Desiccant Bags Flushing Tube
Isopropanol Rubber Policeman
ASTM D1401; ISO 6614; DIN 51599; FTM 791-3201
Oxidation Characteristics of Extreme Pressure
Precipitation Naphtha Acetone Lubricating Oils...............................................................Pages 119-122
Nochromix Distilled Water
Cotton ASTM D2893
Demulsibility Characteristics of Lubricating Oils.................Page 112 Drying Tower

Chromic Acid or equivalent detergent cleaning solution
ASTM D2711 and DIN 51353 Air Supply
Centrifuge Centrifuge Tubes
Distilled Water 1,1,1-Trichloroethane Oxidation Stability of Mineral Insulating Oils ......................Page 123
Oxidation Stability of Steam Turbine Oils and ASTM D2440
Inhibited Mineral Insulating Oils by Rotating Bomb......Pages 114-118 n-Heptane Oxygen
ASTM D2112, D2272; IP 229 Potassium Hydroxide Solution Toluene
Isopropyl Alcohol Chloroform
Liquid Detergent Oxygen
Acid Free Filter Paper p-Naphtolbenzein Indicator
Potassium Hydroxide Petroleum Spirit
Acetone Hydrochloric Acid Oxidation Stability of Inhibited Mineral Turbine Oils ..........Page 126
Chloroform Isopropanol
IP 280
Oxidation Stability of Gasoline Automotive Engine Oils
Oxygen Alkali Blue Indicator
by Thin-Film Oxidation Uptake (TFOUT).......................Pages 114-118
Phenolphthalein Heptane
ASTM D4742 Hydrochloric Acid Potassium Hydroxide
Liquid Detergent Acetone Toluene Dichloromethane
n-Hexane Oxygen Ethanol Sulfuric Acid
Potassium Hydroxide Air Supply Membrane Filters Evaporating Dish
Isopropanol Water Burette Air Oven
Filtration Apparatus Conical Flask, 500mL
Oxidation Stability of Distillate Fuel Oil
(Accelerated Method).....................................................Pages 119-122 Oxidation Stability of Straight Mineral Oil............................Page 126
ASTM D2274 IP 306
Drying Oven Filter Assembly Filtering Crucibles Porcelain Crucibles
Membrane Filters Beaker, 200mL Burette Oxygen
Hot Plate Isooctane Alkali Blue Indicator Phenolphthalein
Oxygen Water Supply n-Heptane Hydrochloric Acid
Acetone Methanol Potassium Hydroxide Toluene
Toluene Chloroform Ethanol
Sulfuric Acid Acetone
Oxidation Characteristics of Inhibited Mineral Oils.......Pages 119-122
Membrane Filters Forceps
ASTM D943; DIN 51587 Petri Dishes Filtration Apparatus
Desiccant Bags Acetone Oven Isopropanol
Abrasive Cloth Glass Syringes, 10 and 50mL
Distilled Water Flexible Tubing
Detergent n-Heptane
Hydrochloric Acid Isopropanol
Oxygen Nitrogen
Gloves
137
Additional Accessories (Continued)
Oxidation Stability of Mineral Insulating Oil ........................Page 126 Rust Preventing Characteristics of Inhibited Mineral Oil
IP307 in the Presence of Water
(Standard and Horizontal Disc Methods) .....................Pages 128-129
Filtering Crucibles Porcelain Crucibles
Burette Oxygen ASTM D665, D3603; NACE TM-01-72; IP 135; ISO 7120; DIN 51355,
Alkali Blue Indicator Phenolphthalein DIN 51585; FTM 791-4011, 791-5315
Heptane Hydrochloric Acid Oven Naphtha
Potassium Hydroxide Toluene Isooctane Synthetic Sea Water
Chloroform Ethanol Distilled Water Precipitation Naphtha
Sulfuric Acid Acetone Petroleum Spirit 60/80
Isopropanol Membrane Filters Corrosion of Lead by Lubricating Oils...................................Page 130
Forceps Petri Dishes FTM 791-5321.1
Filtration Apparatus Oven
Air Supply Analytical Balance
Oxidation Stability of Inhibited Mineral Insulating Oils ......Page 126 Forceps Petroleum Naphtha
IP 335 Acetone Steel Wool
Porcelain Crucibles Burette Cotton
Oxygen Alkali Blue Indicator Bearing Compatibility of Turbine Oils ...................................Page 131
Phenolphthalein Solution n-Heptane FTM 791-3452
Hydrochloric Acid Potassium Hydroxide
Toluene Chloroform Test Equipment for:
Ethanol Membrane Filters, 5.0 m ASTM D445 Kinematic Viscosity (refer to Viscosity Section)
Forceps Petri Dishes ASTM D524 Ramsbottom Carbon Residue (refer to Page 53)
Filtration Apparatus Oven ASTM D974 Total Acid Number
Sulfuric Acid Acetone Copper Corrosion From Petroleum Products........................Page 131
Isopropanol
ASTM D130
Thermal Oxidation Stability of Automotive
Filter Paper Cotton Wool
Gear Lubricants .......................................................................Page 127
Isooctane Stainless Steel Forceps
ASTM 5704; STP12A L-60-1 Performance Test (formerly CRC L-60 Test); Stoddard Solvents
FTM 791B Method 2504
Cloud Point and Pour Point of Petroleum Oils.............Pages 132-133
Oakite 811 Pentane
ASTM D97, D2500; IP 15, 219; ISO 3015, 3016; DIN 51597; FTM 791-201
Stoddard Solvent Toluene
Reference Oils Air Supply Methanol Sodium Sulfate
Absorbent Cotton Tweezers Solid Carbon Dioxide Petroleum Naphtha
Heptane Organic Cleaning Solvent Calcium Chloride Acetone
Ethanol Sodium Chloride
Corrosiveness and Oxidation Stability of Hydraulic Oils,
Aircraft Turbine Engine Lubricants Coking Tendency of Oil ...........................................................Page 135
and Other Highly Refined Oils.......................................Pages 124-125 FTM 791-3462
ASTM D4636; FTM 791-5307, FTM 791-5308; IHC BT-10, DIN 51394 Emery Paper
Air Supply Cotton Petroleum Ether
Analytical Balance n-Heptane Evaporation Loss of Lubricating Oils (Noack Test) ..............Page 136
Centrifuge and Tubes Acetone
ASTM D5800; DIN 51581; IP 421
Microscope Nitric Acid
Oven (optional) Sodium Hydroxide Balance Naphtha
Forceps Sodium Phosphate Toluene
Sodium Dichromate Sulfuric Acid
Brush Distilled Water
Nochromix
138

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Test Methods Page Test Methods Page

Digital Flowmeter option

D892 and D6082 Dual Twin Foaming Characteristics Test

K43092 Dual-Twin Foaming Characteristics Apparatus

Digital Flowmeter option

Test apparatus for ASTM D6082 Sequence IV

Test apparatus for ASTM D892 and D6082

! Software compatible, inquire

K88500 Air Release Value Apparatus

Test Method Specifications Included Accessories

! Software compatible, inquire

Included Accessories (for the pressure measurement systems)

A convenient carriage arrangement allows the oxidation vessels to be inserted

Bath temperature is controlled within ASTM specified limits by an electronic

For verifying bath temperature in accordance with ASTM and

Oxidation Pressure Vessel Accessories Catalog No.

Oxidata pressure measurement equipment is now available for the RPVOT

High Temperature Convertible Oxidation Bath

Digital Flowmeter option

Oxidation Stability Apparatus

For product specifications and ordering information:

Digital Flowmeter option

! Software compatible, inquire

Oxidation Cell Glassware and Accessories Iron-Copper Catalyst

Oxidation Stability Bath

Digital Flowmeter option

Corrosiveness and Oxidation Stability Test Apparatus

Digital Flowmeter option

Oxidation Stability Apparatus (Cigre Bath)

L-60-1 Performance Test Apparatus Specifications

Rust Preventing Characteristics Oil Bath

Accessories Test Specimens

Stability of Lubricating Oils (Work Factor)

Bearing Compatibility of Turbine Oils

Cloud and Pour Point Test Equipment

! Software compatible, inquire

Automatic Cloud Point and Pour Point Analyzer with

Automatic Portable Dielectric Breakdown Tester

K50100 Panel Coker

Test Method Specifications Dimensions lxwxh,in.(cm)

Automatic Non-Woods Metal Noack Evaporative

Demulsibility Characteristics of Lubricating Oils.................Page 112 Drying Tower

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