239M Parr 4600 4700 Pressure Vessels Inst
239M Parr 4600 4700 Pressure Vessels Inst
239M Parr 4600 4700 Pressure Vessels Inst
www.parrinst.com 3
General Purpose Pressure Vessels
Explanation of Symbols
Unpack Carefully There are no user serviceable parts inside the prod-
uct other than what is specifically called out and
Unpack the equipment carefully and check all the
discussed in this manual. Advanced troubleshooting
parts against the packing list. If shipping damage
instructions beyond the scope of this manual can
is discovered, report it immediately to the deliver-
be obtained by calling Parr Instrument Company in
ing carriers. The vessel, motor, heater, and tem-
order to determine which part(s) may be replaced or
perature controller may be packed separately for
serviced.
convenience in shipping, but these parts are easily
reassembled. Examine the components closely for
any loose parts or shipping damage and be sure to Ensure that any hot surfaces have had adequate
check all layers of packing materials thoroughly so time to cool before cleaning or maintaining the
as not to overlook any parts which might otherwise reactor and/or its components.
be discarded.
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General Purpose Pressure Vessels
Vessels with a Flat PTFE or Flexible Graphite Gasket Vessels with a Metal Gasket
The closure bolts may be tightened using either an Pressure vessels with a metal gasket require a
open-end wrench for smaller vessels where the bolt uniform loading on the gasket carefully applied by
torque requirement is less or with a torque wrench tightening a ring of compression bolts with a torque
where additional loading is required for the higher wrench. The amount of torque to be applied will
operating pressures. Unless otherwise note on vary with different vessels and with the intended
documentation accompanying the product, recom- maximum working pressure. Specific sealing
mended torque values are shown alongside respec- instructions will be provided for any Parr pressure
tive model numbers in subsequent pages on this vessels with a metal gasket furnished on special
operating instruction manual. order.
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General Purpose Pressure Vessels
The ID of a pipe or pipe fitting can be enlarged to 6. Do not use oil or anti-seize lubricant on threads
accommodate a tubing feed-thru. Note that, in some or fittings if the vessel is to be used with oxygen.
cases, this may cause a reduction of the pressure
rating. The port below a female pipe connection can 7. If your vessel is equipped with a loose compres-
also be opened up to a larger size. sion ring be sure that it is in place on the head
before attaching any head fittings. The compres-
The maximum openings are shown in the table below. sion ring cannot be installed after fittings have
been screwed into the head.
Tapered Pipe Threads 8. Clean all threads and gas passages thoroughly
A
Nominal Size 1/8” 1/4” and remove all tape fragments when overhaul-
B
ing a vessel. An ultrasonic bath is excellent for
Pipe OD (A) 0.405” 0.540” cleaning metal parts, but do not place a thermo-
couple probe, pressure gage, face seals or ball
Maximum bearings in an ultrasonic bath. Periodic cleaning
1/4” 3/8” may be performed on the exterior surfaces of
Feed-thru (B)
the reactor stand with a damp cloth. All power
Maximum Exit
0.339” 0.438” should be disconnected when cleaning.
C Port (C)
11. If servicing assistance is needed, contact Parr In- Apparatus returned for testing and overhaul should
strument Company direct at the address shown be shipped prepaid to the following address:
on the back of these instructions.
Ship repair to:
Parr Instrument Company
Periodic Pressure Tests Attn: Service Department
RMA # XXXXXX
Each cylinder used in a Parr pressure vessel is tested 211 53rd Street
under hydrostatic pressure to the higher of 1.43 Moline, Illinois 61265
times the rated working pressure at room tem- USA
perature or 1.30 times the rated working pressure
corrected for temperature before it is released from An order or letter of instructions should be mailed to
the factory. Micrometer caliper measurements are the same address, as no repair work will be started
taken during this test to check the deflection of the without specific instructions and a Health & Safety
walls under pressure. Excessive deflection or failure Assurance Certification form (FX004) signed by a
of the metal to resume its original dimensions after responsible user.
pressure is released indicates that a cylinder is po-
tentially unsafe and it will be rejected. Similar tests
should be made at regular intervals during the life
of each cylinder, and particularly whenever the user
suspects that the equipment has been over-stressed
or damaged.
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General Purpose Pressure Vessels
HEAD ASSEMBLY GUIDE
Refer to this table for more information about Head Styles Listed in Series Working Limits and Parts List section.
Head Style Description
One opening, TBD One opening, size to be determined by user
“A” Socket One Type “A” Socket opening, to be used with 4316 Gage Block Assembly 1
“B” Socket One Type “B” Socket opening, to be used with 4317 Gage Block Assembly 1
VGR Valve, gage, rupture disc, and thermocouple 2 3
Notes:
1) Reference pages 32-35 for more information about Gage Block Assemblies.
2) Number of valves varies amongst series. See individual heads for number of valves.
3) A thermowell with thermocouple is offered for most series if needed.
MATERIAL DESIGNATIONS
Series 4703-4714
Closure Recommended Bolt Torque:
Model Size Head Style
Material PTFE Gasket
4703 22 mL One opening, TBD Steel 500 PSI 15 ft - lbs
4704 22 mL “A" Socket Steel 1000 PSI 20 ft - lbs
4713 45 mL One opening, TBD Steel 1500 PSI 30 ft - lbs
4714 45 mL “A” Socket Steel 1700 PSI 40 ft - lbs
27ACHA GASKET
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
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General Purpose Pressure Vessels
Series 4740
Model Size Head Style Part No. Description Flat Gasket Seal
4740 75 mL “A” Socket 1827HC Head , "A" Socket opening
4742 25 mL “A” Socket A1828HC Cylinder, 75 mL
A1828HC2 Cylinder, 22 mL
Working Limits* 1829HCKL Gasket, Flexible Graphite
Maximum Working Pressure (T316SS) 1826HC Compression Ring
8500 psi (586 bar) @ 350 °C A33HD2 Screw Cap with compression bolts,
1850 psi (127 bar) @ 538 °C alloy steel
Maximum Working Temperature 538 °C 33HDF2 Compression Bolt for screw cap
(6 required)
*See Manual No. 294M for more information.
A33HD2CH** Screw Cap with compression bolts,
Recommended Bolt Torque: Hastelloy C
PTFE or Flexible Graphite 40HD2HA PTFE Liner, 25 mL
8500 PSI 15 ft - lbs 40HD Pyrex Liner, 75 mL
40HDHA PTFE Liner, 75 mL
1827HC HEAD
(6) 33HDF2
COMPRESSION BOLTS
1826HC
COMPRESSION RING
1829HCKL
GASKET, GRAFOIL
A33HD2
SCREW CAP
A1828HC (4740)
CYLINDER, 75mL
A1828HC2 (4742)
CYLINDER, 25mL
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
**Required for maximum working pressure of 7900 psi (544 bar) at 538 °C for vessel of T316SS
14 Parr Instrument Company
General Purpose Pressure Vessels
Series 4750
Model Size Head Style
4750 125 mL One opening, TBD
4751 125 mL “A” Socket
4752 200 mL One opening, TBD
4753 200 mL “A” Socket
4754 125 mL “A” Socket & 1/8” NPT
with thermocouple
4755 200 mL “A” Socket & 1/8” NPT
with thermocouple
Working Limits
Maximum Working Pressure (T316SS)
3000 psi (207 bar)@ 350 °C
[200 bar for CE orders]
Maximum Working Temperature 350 °C
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
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General Purpose Pressure Vessels
Series 4760-4777
Model Size Head Style Part No. Description Flat Gasket Seal
4760 300 mL One opening, TBD 453HC Head, "A" Socket opening
4761 300 mL “A” Socket 453HC5 Head, "A" Socket & 1/8” NPT
4762 450 mL One opening, TBD Head, “A” Socket & 1/8” NPT for
453HC79*
4763 450 mL “A” Socket thermowell
4764 600 mL One opening, TBD 818HC45 Head, VGR
4765 600 mL “A” Socket 452HC Cylinder, 300 mL, 3.94" deep
4766 300 mL VGR 452HC2 Cylinder, 450 mL, 5.94" deep
4767 450 mL VGR 452HC3 Cylinder, 600 mL, 7.94" deep
4768 600 mL VGR 452HC9 Cylinder, 160 mL, 2.00" deep
4772 160 mL One opening, TBD 452HC8 Cylinder, 100 mL, 2.00" deep, 2” ID
4773 160 mL “A” Socket 457HC2 Gasket, PTFE
4774 160 mL VGR 457HC3KL Gasket, Flexible Graphite
4775 100 mL One opening, TBD 454HC Compression Ring
4776 100 mL “A” Socket A455HC Split ring, pair, with cap screws
4777 100 mL VGR 232HCFDE Cap screw for above (6 required)
A456HC Drop band with set screw
Working Limits 456HCF Set screw for above
Maximum Working Pressure A833HC Connector for thermocouple
3000 psi (207 bar) @ 350 °C A472E Thermocouple, 7-1/2”, SS
[200 bar for CE orders]
A472E2 Thermocouple, 9-1/2”, SS
Maximum Working Temperature
with PTFE confined flat gasket A472E3 Thermocouple, 11-1/2, SS
350 °C
A1453HC Thermowell
Recommended Bolt Torque: A138CA Connector for thermowell
PTFE Gasket 25 ft - lbs 2583HC Head/Cylinder Service Fixture
Flexible Graphite 35 ft - lbs
Liners
Volume Pyrex PTFE
100 mL 762HC7 762HC7HA
160 mL 762HC8 762HC8HA
300 ML 762HC 762HC4HA
450 mL 762HC2 762HC5HA
600 mL 762HC3 762HC6HA
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
16 Parr Instrument Company
General Purpose Pressure Vessels
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General Purpose Pressure Vessels
Series 4760Q-4777Q
Model Size Head Style Part No. Description O-ring Seal
4760Q 300 mL One opening, TBD 2321HC2 Head, “A" socket opening
4761Q 300 mL “A” Socket 2321HC3 Head, "A" socket & 1/8” NPT
4762Q 450 mL One opening, TBD 2340HC11 Head, VGR
4763Q 450 mL “A” Socket 2342HC Cylinder, 300 mL, 3.94" deep
4764Q 600 mL One opening, TBD 2342HC2 Cylinder, 450 mL, 5.94" deep
4765Q 600 mL “A” Socket 2342HC3 Cylinder, 600 mL, 7.94" deep
4766Q 300 mL VGR 2342HC4 Cylinder, 100 mL, 2.00” deep, 2” ID
4767Q 450 mL VGR 2342HC5 Cylinder, 160 mL, 2.00" deep
4768Q 600 mL VGR 2341HCJV O-ring, FKM
4772Q 160 mL One opening, TBD 2341HCJK O-Ring, FFKM
4773Q 160 mL “A” Socket 2195HC Split ring, pair
4774Q 160 mL VGR A456HC Drop band with set screw
4775Q 100 mL One opening, TBD 456HCF Set screw for above
4776Q 100 mL “A” Socket A833HC Connector for thermocouple
4777Q 100 mL VGR A472E Thermocouple, 7-1/2”, SS
A472E2 Thermocouple, 9-1/2”, SS
Working Limits A472E3 Thermocouple, 11-1/2, SS
Maximum Working Pressure (T316SS) A1453HC Thermowell
3000 psi (207 bar)
[200 bar for CE orders]
A138CA Connector for thermowell
Maximum Working Temperature 2587HC Head/Cylinder Service Fixture
with FKM O-ring 225 °C
with FFKM O-ring 300 °C
Liners
Volume Pyrex PTFE
100 mL 762HC7 762HC7HA
160 mL 762HC8 762HC8HA
300 ML 762HC 762HC4HA
450 mL 762HC2 762HC5HA
600 mL 762HC3 762HC6HA
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
18 Parr Instrument Company
General Purpose Pressure Vessels
288VBAD MALE CONNECTOR
A472E THERMOCOUPLE
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General Purpose Pressure Vessels
Series 4790 4790 with Flat Gasket & Split Ring
Model Size Head Style Part No. Description
4791 25 mL VGR Head, VGR (three valves) & 1/8” NPT
2432HC3
4792 50 mL VGR (General Purpose & HP vessels)
4793 100 mL VGR Fixed Head, VGR (two valves) & &
3665HC
1/8” NPT (HP/HT vessels)
Working Limits (Standard Ratings) 2430HC Cylinder, 25 mL
Maximum Working Pressure 2430HC18 Cylinder, 25 mL, 100 mL Profile (HP/HT)
(T316SS) 3000 psi (207 bar) 2430HC2 Cylinder, 50 mL
[200 bar for CE orders 2430HC19 Cylinder, 50 mL, 100 mL Profile (HP/HT)
With PTFE Flat Gasket 350 °C 2430HC3 Cylinder, 100 mL
With FKM O-ring 225 °C 429HC2 Gasket, PTFE
With FFKM O-ring 300 °C
429HC2KL Gasket, Flexible Graphite
454HC Compression Ring
Working Limits (High Pressure/High Temp.)
A455HC Split Ring
Maximum Working Pressure
(T316SS) 5000 psi (345 bar) A456HC Drop Band
With PTFE Flat Gasket 350 °C 232HCFDE Bolt for Split Ring
With Flexible Graphite Gasket* 500 °C
*A vessel with a Fixed Head is required for effective heating to 500 °C.
4790 with O-ring Seal & Easy Close Split Ring A888HC2 R/D HOLDER ASSY
526HC SERIES R/D
Part No. Description
1379HC SCREW CAP
2902HC3 Head, VGR (three valves) & 1/8” NPT
2520HC Cylinder, 25 mL 1433HC SERIES O-RING
2520HC2 Cylinder, 50 mL
2520HC3 Cylinder, 100 mL 1443HC DIP TUBE, 25mL
1443HC2 DIP TUBE, 50mL
2521HCJV O-Ring, FKM 1443HC3 DIP TUBE, 100mL
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
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General Purpose Pressure Vessels
SERIES 4600 WORKING LIMITS AND PARTS LISTS
Series 4600-4620 Part No. Description Flat Gasket Seal
Model Size Head Style 229HC3 Head, "B" Socket
4601 1000 mL One opening, TBD 229HC6 Head, "B" Socket, thermowell
4602 2000 mL One opening, TBD 942HC59 Head, one Rupture Disc Opening
4611 1000 mL “B” Socket 1370HC30 Head, VGR, thermowell
236HC10 Cylinder, 1000 mL, 5.32" deep
4612 2000 mL “B” Socket
236HC20 Cylinder, 2000 mL, 10.44" deep
4621 1000 mL VGR, thermowell
315HC2 Gasket, PTFE
4622 2000 mL VGR, thermowell
315HC4KL Gasket, Flexible Graphite
A232HC Split Ring pair, with cap screws
Working Limits 232HCFDE Cap Screw for above (6 required)
Maximum Working Pressure A233HC Drop Band with Screw
(T316SS) 1900 psi (131 bar)
233HCF Drop Band Screw
Maximum Working Temperature 234HC Compression Ring
with PTFE confined flat gasket 350 °C
265HC12 Thermowell for 2000 mL vessel
265HC7 Thermowell for 1000 mL vessel
Recommended Bolt Torque:
48HC Thermowell Gasket, silver
PTFE Gasket 25 ft - lbs 48HCCN Thermowell Gasket, nickel
Flexible Graphite 35 ft - lbs 48HCFG Thermowell Gasket, gold plated
A472E2 Thermocouple, 9-1/2”, 1000mL
56HC SERIES
A472E6 Thermocouple, 15-1/2”, 2000mL
PRESSURE GAGE
2584HC Head/Cylinder Service Fixture
A472E2
398HC Pyrex Liner, 1000 mL
THERMOCOUPLE, 1L 398HCHA PTFE Liner, 1000 mL
A472E6
THERMOCOUPLE, 2L 399HC Pyrex Liner, 2000 mL
A888HC2 R/D HOLDER ASSY 399HCHA PTFE liner, 2000 mL
526HC /581HC STYLE R/D
366VBA_ HEX COUPLING
288VBAD MALE CONNECTOR
2X 420HC ADAPTER
260HC2 EXTENSION
208HC20
GAGE ADAPTER 1370HC30 HEAD
A232HC SPLIT RING ASSY
209HC4 234HC COMPRESSION RING
ADAPTER BUSHING
A233HC DROP BAND ASSY
315HC2 SERIES GASKET
236HC10 CYLINDER, 1L
Note: For special material vessels add material code 236HC20 CYLINDER, 2L
A122VB
STRAIGHT VALVE
2X 420HC ADAPTER
2X 420HC ADAPTER
A122VB STRAIGHT VALVE
A122VB STRAIGHT VALVE
179VBAD STREET TEE
208HC20 179VBAD STREET TEE
GAGE ADAPTER A146VB ANGLE VALVE
A146VB ANGLE VALVE
209HC4 260HC2 EXTENSION
ADAPTER BUSHING 260HC2 EXTENSION
2740HC30 HEAD
2740HC30 HEAD
2245HC SPLIT RING, QC
2245HC SPLIT RING, QC
A233HC DROP BAND ASSY
A233HC DROP BAND ASSY
2741HCJV O-RING
2741HCJV O-RING
2742HC10 CYLINDER, 1L
2742HC10
2742HC20CYLINDER,
CYLINDER,1L
2L
2742HC20 CYLINDER, 2L
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General Purpose Pressure Vessels
Series 4605-4626 Part No. Description Flat Gasket Seal
Model Size Head Style 2330HC12 Head, "B" socket
4605 600 mL One opening, TBD 2330HC13 Head, "B" socket, thermowell
2300HC19 Head, VGR, thermowell
4606 1200 mL One opening, TBD
2302HC Cylinder, 600 mL
4615 600 mL “B” Socket
2302HC10 Cylinder, 1200 mL
4616 1200 mL “B” Socket 2304HC Compression Ring
4625 600 mL VGR, thermowell A2305HC Split Ring
4626 1200 mL VGR, thermowell 1278HC6F Compression Bolts 5/8–18 (8 req.)
A2313HC Drop Band
233HCF Bolt for Drop Band
2303HC Gasket, PTFE
56HC SERIES
PRESSURE GAGE
2303HC2KL Gasket, Flexible Graphite
A472E2 THERMOCOUPLE, 600mL 265HC20 Thermowell, 600 mL
A472E6 THERMOCOUPLE, 1200mL
288VBAD
265HC21 Thermowell, 1200 mL
MALE CONNECTOR 48HC Thermowell Gasket, silver
366VBA_
HEX COUPLING 48HCCN Thermowell Gasket, nickel
A888HC2 R/D HOLDER ASSY
526HC/581HC R/D 48HCFG Thermowell Gasket, gold plated
208HC15 ADAPTER, ANGLED A472E2 Thermocouple, 9-1/2”, 1000 mL
A451VB STRAIGHT VALVE
A472E6 Thermocouple, 15-1/2”, 2000 mL
209HC4
BUSHING 2585HC Head/Cylinder Service Fixture
2312HC Pyrex Liner, 600 mL
2312HC2 Pyrex Liner, 1200 mL
2312HC3HA PTFE Liner, 600 mL
2312HC4HA PTFE Liner, 1200 mL
A451VB2 ANGLE VALVE
420HC2 ADAPTER
208HC6ADAPTER
209HC4 BUSHING
2300HC19 HEAD
A2305HC
SPLIT RING ASSY
2304HC
Working Limits COMPRESSION RING
Working Limits
Maximum Working Pressure* (T316SS)
6000 psi (414 bar) @ 350 °C
5900 psi (407 bar) @ 500 °C
Maximum Working Temperature* 500 °C
491HCAD NIPPLE
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
*For alternate ratings please consult Parr Instrument Company.
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General Purpose Pressure Vessels
Series 4660
A131VB
Model Size Head Style ANGLE VALVE A131VB
ANGLE VALVE
420HC2
4661 3.78 L One opening, TBD ADAPTER
658HC
4662 3.78 L VGR, thermowell ADAPTER, VALVE
658HC
4665 7.99 L One opening, TBD ADAPTER, VALVE A754HC
SPLIT RING ASSY
4666 7.99 L VGR, thermowell 659HC
COMPRESSION RING
655HC
Working Limits GASKET
2691HCJE O-Ring, EP
56HC SERIES
A129VB Valve, Straight, 1/4"NPT (M) x 1/4"T PRESSURE GAGE
914HC LOCKNUT
Recommended Bolt Torque: 257HC28 DIP TUBE, 1 GAL
(OPTIONAL)
PTFE Gasket 257HC29 DIP TUBE, 1.5 GAL
3000 PSI 35 ft-lbs (OPTIONAL)
(≤ 350 °C)
Flexible Graphite
3000 PSI 45 ft-lbs
Gasket (≤ 500 °C)
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
*For alternate ratings please consult Parr Instrument Company.
28 Parr Instrument Company
General Purpose Pressure Vessels
Series 4676-4677 56HC SERIES PRESSURE GAGE
A707HC2 R/D HOLDER ASSY
Model Size Head Style 708HCP SERIES R/D
Note: For special material vessels add material code for head, cylinder and/or internal fittings per page 12.
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General Purpose Pressure Vessels
Series 4678-4679
Model Size Head Style 56HC SERIES PRESSURE GAGE
4678 10 L One opening, TBD A472E5 THERMOCOUPLE
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General Purpose Pressure Vessels
4316 & 4317 GAGE BLOCK ASSEMBLIES
A888HC2 Rupture Disc Assembly and Series 526HC Rupture Discs, Alloy 600 (See Manual 231M)
Part No. Description
526HCPD 1000 psi
526HCPF 2000 psi
526HCPG 3000 psi
526HCPH 5000 psi
526HCPJ 8000 psi
526HCPL 12000 psi
A888HC2 Rupture Disc Assembly
49HC2 Orifice Cone
527HC Orifice ring
433HC4 Safety Head Outlet
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General Purpose Pressure Vessels
Gage Block Assembly Drawing
A2599HC2 155VB
TRANSDUCER COOLING STREET TEE
BODY ASSEMBLY (OPTIONAL)
526HC_ 433HC4
RUPTURE DISC SAFETY HEAD
123VB2 8VB2 112VB4AK 4VB3 OUTLET 1/4 NPTM
VALVE PACKING VALVE PACKING
HANDLE NUT NEEDLE GASKET
40HC 366HC
BUSHING BUSHING
325HC 326HC
COMPRESSION COMPRESSION
NUT NUT
SEE NOTE 1 SEE NOTE 1
365HC
51HC TUBE, INLET
TUBE, INLET
326HC
COMPRESSION
NUT
SEE NOTE 1
35HC 366HC
COMPRESSION BUSHING
NUT
SEE NOTE 2
40HC
BUSHING
4316 4317
"A" SOCKET "B" SOCKET
CONNECTION CONNECTION
NOTES:
1) APPLY ANTI-SEIZE COMPOUND SPARINGLY TO THREADS AND TORQUE TO 20 LBS/FT.
2) APPLY ANTI-SEIZE COMPOUND SPARINGLY TO THREADS AND TORQUE TO 15 LBS/FT.
A1906EP_
SERIES
PRESSURE
TRANSDUCER
(OPTIONAL)
593HC SERIES
PRESSURE GAGE
A2599HC2
TRANSDUCER COOLING
BODY ASSEMBLY
(OPTIONAL)
A1357E SERIES
THERMOCOUPLE
155VB
STREET TEE
(OPTIONAL)
A411VB2AD
MALE CONNECTOR
1/16T/1/8NPT BT
A147VB 154VB2
STRAIGHT ELBOW 49HC2 302VBAD
VALVE (OPTIONAL) ORIFICE CONE FEMALE CONNECTOR
(OPTIONAL) 3/8T - 1/4 NPTF
527HC
6VBAA 126VB ORIFICE RING
PACKING LANTERN RING
COVER
325HC
COMPRESSION
NUT
SEE NOTE 1
51HC49
TUBE
35HC
COMPRESSION
40HC NUT
BUSHING SEE NOTE 2
NOTES:
1) APPLY ANTI-SEIZE COMPOUND SPARINGLY TO THREADS AND TORQUE TO 20 LBS/FT.
2) APPLY ANTI-SEIZE COMPOUND SPARINGLY TO THREADS AND TORQUE TO 15 LBS/FT.
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239M R11 04/18/17