QC Probs
QC Probs
QC Probs
2. If a 1.2578 g sample of Calamine, 96% Zinc Oxide was treated with 50 mL of 101230 N Sulfuric
acid, what volume of 0.9765 N sodium hydroxide would be required in the back titration?
3. A 50mL sample of calcium hydroxide solution required 19.5 mL of 0.1050 N hydrochloric acid in
a titration. Calculate the amount of calcium hydroxide in %w/v.
4. What weight of sodium hypochlorite, 95% pure, is needed to react with 244 mL of 0.0576 N
sodium hydroxide?
5. Calculate the magnesium oxide content of mom, 12.3255 g of which was heated with 50 mL of
1.0340 N sulfuric acid, producing a mixture that required 24.6 mL of 1.1255 N sodium hydroxide.
6. A 0.5003 g sample of acetic acid was titrated with 29.5 mL of 1.2345 N sodium hydroxide. A
blank was run using 37.8 mL of sodium hydroxide. What is the %P of acetic acid?
7. A 1.2025 g sample of aspirin was titrated with 26.75 mL of 0.1145 N sodium hydroxide. A blank
was run using 35.82 mL of sodium hydroxide. What is the %P of aspirin?
8. What wt of 98.5% potassium biphthalate is equal to 35 mL of 0.01 N sodium hydroxide?
9. If 25 mL of hydrochloric acid required 25.3 mL of 0.0752 N sodium hydroxide in a titration, what
volume of the hydrochloric acid solution would produce an endpoint with 0.287 g Silver chloride
(95.50%)?
10. What is the %P of 0.5319 g sodium bicarbonate if it was initially titrated with 30 mL of 1.5960 N
sodium hydroxide, and back titrated with 27.2 mL of 1.0998 N sulfuric acid?
1. What is the %P of 2.2502 g Tartaric acid if It utilized 24.2 mL of 1.2160 N sodium mwthoxide?
Each mL of 1N sodium methoxide is equivalent to 75.04 mg of tartaric acid.
2. Calculate the titer value of sodium sulfate for 0.02 N potassium hydroxide.
3. Calculate the titer values for 0.9985 N sulfuric acid of potassium bicarbonate.
4. About 0.2509 g of iodized salt was treated with 50 mL of 0.1224 N silver nitrate. The mixture
was treated with 31.2 mL of 0.0975 N ammonium thiocyanate. What is the %NaCl if each mL of
0.1 N silver nitrate is equivalent to 5.844 mg NaCl?
5. Calculate the titer value for 1.0975 N sulfuric acid of calcium carbonate.
6. About 0.7845 g sample of aspirin was titrated with 19.5 mL of 0.1355 sulfuric acid. A blank
titration was run using 25 mL of 0.1355 N sulfuric acid. What is the %aspirin content? Each mL of
0.1 N sodium hydroxide is equivalent to 18.01 mg.
7. What is the %Hg content of 0.4005 g phenylmercuruc nitrate which consumed 10.3 mL of
0.1165 N ammonium thiocyanate? Each mL of 0.1 N ammonium thiocyanate is equivalent to
10.03 mg of Hg.
8. About 1.2580 g of methenamine was boiled in 40 mL of 1.5452 N sulfuric acid. It was then back
titrated with 24.5 mL of 1.8356 N sodium hydroxide. What is the %P of the sample if each mL of
1N sulfuric acid is equivalent to 35.05 mg of C6H12N4?
9. A 4.0520 g sample of HCl, spgr 1.18, required 44.2 mL of 0.9035 N NaH in a titration. Calculate
the ff: (A) %HCl, (B) Normality, (C) Sodium carbonate titer of the sample
10. A hydrochloric acid solution has a silver chloride titer of 0.1265; what is its sodium carbonate
titer?
1. Twenty tablets of Dextromethorphan HBr were finely powdered and used for assay by non-aq
acidimetry. 100 mg of the powdered tabs consumed 12.5 mL of 0.1035 N HClO4 in a titration.
What is the %LA if the LC is 250 mg? Each mL of 0.1N HClO4 is equivalent to 35.23 mg DHBr.
2. In the assay of aluminum hydroxide tablet, compute for the content/tab if 0.5879 g of powdered
tablets required 25.6 mL of 0.0512 N sulfuric acid. Each tab weighs 0.5950 g.
3. About 0.2745 g of powdered ASA was treated with 29.5 mL of 0.1125 N sulfuric acid. A blank
titration was run using 40 mL of 0.1125 N H2SO4. What is the %ASA content if the average
weight of tablet is 100 mg? What is the %LC if each tab contains 80 mg ASA? Each mL of 0.1 N
NaOH is equivalent to 18.01 mg.
4. Twenty tablets of Tums weigh 3.1575 g. The tablets were dissolved in neutralized alcohol to
make 250 mL of the solution. About 9.6 mL aliquot portion was titrated with 7.5 mL of 0.1165 N
NaOH to bring about the endpoint. What is the amt/tab if each mL of 0.1 N NaOH is equivalent
to 50.2 mg CaCO3? Compute for the %LC if the LA is 500 mg.
5. About 512.5 mg of ammonium bromide was treated with 50 mL of 0.1105 N AgNO3. Ferric Alum
was added anf the mixture was titrated with 28.3 mL of 0.0977 N NH4SCN. What is the amt/cap
if 20 caps weigh 11.6532 g? If the LA is 300 mg, what is the %LC?
6. A 1.0035 g sample of sodium bicarbonate was treated with29.5 mL of 1.0045 N sodium
hydroxide. A blank was run using 40.2 mL of sodium hydroxide. What is the amt/tab? What is
the %LC if the LA is 650 mg? 20 tablets weighed 13.25 g.