Mixing technology

An introduction
 Table of contents
Introduction Mixtures
3 Mixing – a key process with complex demands 17 Understanding key mixing challenges
17 Air incorporation and foaming
Powders
19 Lump formation
4 An overview of powder properties
19 Clogging
4 Understanding common stabilizers
5 Solubility limits of powders The right solution conquers mixing challenges
20 Preventing air incorporation and foaming
Mixtures
20 Choosing the right mixing equipment
6 Two types of mixtures and their unique properties for each specific formulation
20 Advantages of vacuum mixing
Mixtures – Suspensions
20 Advantages of rotor and stator mixing
8 Suspensions and their properties
21 Reduced air incorporation with vacuum mixers
8 Flocculation, suspension and sedimentation
21 The solubility of air in liquid
9 Achieving efficient wetting and preventing
fish eyes 21 Choosing the right temperature

10 How to make a stable suspension 22 Preventing lumping and clogging

22 Advantages of batch mixers
Mixtures – Emulsions 22 Advantages of pre-mixing
12 Emulsions and their properties 22 Choosing the right temperature
13 Emulsion components
14 Coalescence and creaming Mixing guidelines

15 How to make a stable emulsion 24 Pectin solutions

24 Long life yoghurt-based drinks
24 Milk-juice beverages
24 Recombined milk
27 Chocolate milk
27 Mayonnaise
2
Introduction
Mixing – a key process with complex demands
Mixing is the process of dissolving, emulsifying or dis- processors to have the right mixing solution from the
persing powder and liquid ingredients into a liquid me- start and ensure complete control over the many factors
dium. Mixing, a common operation in food processing, that affect mixing efficiency and end-product quality.
aims to efficiently achieve a smooth, homogenous prod-
uct with consistent quality. This overview of mixing technology covers guidelines
for producing various common consumer products and
Food processors, and consumers, insist on a perfect ingredients, important mixing parameters, formulations,
product every time. To achieve this, food processors and explains how to overcome the key challenges within
must stay in complete control of every aspect of their mixing.
production from beginning to end. Mixing is a highly
complex operation and often takes place early on in the
process of food production. Thus, it is crucial for food

The right mixing solution maximizes

product quality and operational efficiency

3
 Powders
An overview of powder properties
The handling of ingredients in powder form has many Certain powders, such as pectin, do not deliver their tionality under end-product storage conditions and they
advantages. Powder ingredients have longer shelf life functional properties unless they have reached the cor- may need to be able to be treated with high shear forces.
and are smaller, lighter and more convenient to trans- rect temperature. Pectin, for example, needs to reach This functionality may be the right mouthfeel, the right
port and store. This has lead to an increase in powder 80°C in order to be activated so that it protects the pro- consistency for keeping particles in a solution, or that the
ingredient use. teins in, for example, a milk-juice beverage. product must be able to be frozen and thawed. Stabiliz-
ers, and other powders, may also be modified to make
A wide range of ingredients are available in powder form, Stabilizers are modified to meet specific processing them easier to dissolve. These kinds of modified pow-
including starches, fibres, vitamins, proteins, emulsifiers, needs. For example they must maintain the right func- ders are called agglomerated powders.
stabilizers, spices, flavourings, probiotics, milk, and sugar.
The various powder ingredients have very different char-
acteristics, depending on what raw ingredients they are
made from, and how they are modified to fit different High Low Cold Hot
Type of powder viscous Foam Lump Dust solubility swelling swelling
processing needs and recipes. Some powders such as
aspartame, powdered milk, and tea powders are prone Aspartame • •
to foaming and require special attention. Skim milk powder •
Maltodextrine •
Understanding common stabilizers Whey powder •
Stabilizers are important functional ingredients in food
Tea powder • •
production since product consistency often plays a de-
cisive role in how consumers experience a product. But, CMC* • •
they can be very difficult to incorporate into liquids with- Pectin • • •
out lumping occurring. Cocoa powder • •
Caseinat • •
Stabilizers are based on either polysaccharides, such as
Starch • • •
potato, corn, and tapioca starches, or proteins such as
casein and egg white. Other common polysaccharide Gum agent • • •
stabilizers include pectin, guar gum, carboxylmethyl cel- *
Carboxy methyl cellulosa
lulose, and xanthan gum.

4
Solubility limits in powders Ingredient suppliers modify stabilizers in various ways
There are physical limitations on how much powder it is and use various raw materials to achieve various desired
possible to dissolve into a liquid. Some common exam- functionalities. This is why highly detailed information
ples where the limits of solubility are important to con- is required in order to make recommendations on what
sider are aspartame, lactose, and stabilizer ingredients. amounts are possible to dissolve in specific recipes. For
example, when using pectin a 5% solution can vary in
In some powders, such as aspartame, pH affects solubil- viscosity from 300cP to 3000cP.
ity. For example, a citric acid solution of 10% and with a
pH of 2 can accommodate a 5 to 8% solution of aspar- The solution with lower pH enables a higher solubility of
tame while a non-acidic solution can only accommodate aspartame. The rate/amount of aspartame that is pos-
a 1% solution of aspartame. Temperature also affects the sible to dissolve in the solution increases more quickly
solubility of aspartame. Higher temperatures allow more when the low pH is combined with a higher temperature.
aspartame to be dissolved in a solution. The high tem-
perature effect on aspartame solubility is even greater
when combined with a low pH (see diagram at right).
Aspartame is also more easily and quickly dissolved with
the help of high shear forces. Solubility, %

Stabilizers and thickeners have a critical limit where vis- 12,0

10% citric acid, pH2
cosity increases so much that the liquid can no longer
reach the inner particles in order to dissolve the pow- 8,0
der. It is therefore crucial to know the final viscosity of
an end product when working with stabilizers in powder
form. It is also very important to understand how mixing 4,0
0% acid, pH7
technique must be adapted to ensure optimal mixing
efficiency when working with stabilizer powders. 10 20 30 40 50 Temperature, °C

5
 Mixtures
Two types of mixtures and their unique properties

Continuous Dispersed phase This section describes two main types of mixtures handled in the
phase Solid Liquid mixing process. The first type of mixture is a suspension, defined
Solid Solid Gel as a mixture of solids and liquids. The second type of mixture
combines liquids with other liquids to create an emulsion.
Liquid Suspension Emulsion

Classifications of mixtures
This document will focus on suspensions and emulsions, which
Continuous phase Dispersed phase are the mixtures most commonly used in the food industry.

6
7
 Mixtures
Suspensions

Suspensions and their properties Flocculation and sedimentation

A suspension is when denser par ticles are evenly Suspensions are unstable due to electrostatic forces
dispersed in a less dense liquid. The goal in mixing between the ingredients and density differences in the
suspensions is to achieve stability. This is achieved by dispersion. These can cause separation through floc-
counteracting their naturally unstable nature. culation, where particles clump within the product, or
through sedimentation, where particles fall to the bot-
To achieve a stable suspension, it is important to under- tom of the liquid. Both flocculation and sedimentation
stand the properties of a powder as well as what hap- may complicate further processing of the food product
pens when powder and liquid meet. This understanding and potentially shorten the shelf life of a product.
enables food processors to determine the most efficient
way to introduce it into a liquid. Stability is achieved when particles remain equally dis-
persed in liquid without changing or separating over
When powder is introduced to a liquid, the liquid pen- time. It is important to achieve stability to ensure the
etrates through the pores of the powder with the help of correct shelf life and end-product quality.
capillary forces and increases the contact area between
the powder and the liquid. Then, it is necessary to add
energy in the form of heat and/or shear forces to wet
and disperse the powder as quickly and efficiently as
possible in the liquid.

Creaming Sedimentation Optimal Flocculation Coalescence

8
Achieving efficient wetting and preventing fish eyes Wettability describes how much a solid is wetted by a liq-
Faster wetting prevents lumping and increases the over- uid through the force of adhesion between the solid and
all efficiency of the mixing process. However, when a the liquid phase. And cohesivity describes how tightly
high-viscosity powder such as guar gum is added to a particles are attracted to each other.
liquid too quickly and in too large amounts, the viscosity
of that solution increases and the dissolution rate slows, Powders with high cohesivity, such as some food stabiliz-
hindering the thorough wetting of particles. The product ers, are more difficult to wet and benefit therefore from
then risks the formation of fish eyes, lumps of dry powder being pre-mixed with other more easily mixed ingredi-
with an outer gelling layer. ents such as sugar before being introduced to a liquid.
This helps prevent issues such as fish eyes but also en-
How much shear force is required to prevent fish eyes sures that producers get the most possible function out
and achieve a stable suspension depends on a number of ingredients.
of factors including powder wettability and cohesivity.
Mixing temperature is also important to consider in ena-
When using certain powders, the viscosity of a solution bling a successful dissolution. At higher temperatures,
can increase during dissolution. When the viscosity of a more energy and faster molecular movement in the mix
solution increases it may lead to decreased flow in the can increase the dissolution rate.
solution, which in turn leads to slower wetting and pro-
longed mixing time.

9
 Mixtures
Suspensions
How to make a stable suspension The main types of separation in suspensions
Stoke’s law describes the separation behaviours of par- are flocculation and sedimentation
ticles in suspensions.

Creaming Sedimentation Optimal Flocculation Coalescence

d 2 (p1 - pfl)
V= g
18n
The settling velocity (V) is influenced by the particle
diameter (d), the particle density (p1), the density of the
solution (pfl) and the viscosity of the solutions (n); (g)
describes the acceleration due to gravity.

According to Stoke’s law, food processors

may improve suspension stability by:
1. Decreasing the difference in density between
the particles and the surrounding solution
2. Reducing particle size
3. Increasing the viscosity of the surrounding solution

10
11
 Mixtures
Emulsions

Emulsions and their properties

Emulsions are mixtures containing two liquid phases that
do not naturally mix, one of which is dispersed in the
other as droplets. There are two types of emulsions in
the food industry – oil-in-water emulsions and water-in-
oil emulsions. In oil-in-water emulsions, the oil phase is
the dispersed phased and water phase is the continuous
phase. This is the most common type of emulsion and
examples include mayonnaises, dressings, soups, and
sauces. In water-in-oil emulsions, which include marga-
rines and spreads, water is the dispersed phase and oil/
fat is the continuous phase.

Water in oil Oil in water

For example margarine For example mayonnaise,

and spreads dressing, soups and sauces

12
Emulsions components

Oil phase Emulsifier

The oil phase (fats and oils), provide the main flavour of Emulsifiers are the compounds that make emulsions
a product since fat carries a large amount aroma and possible by stabilizing the dispersed phase and the
flavour. continuous phase. They reduce the interfacial tensions
between the two phases. An emulsifier has one lipophilic
Water phase tail, which loves the fat phase, and one hydrophilic head,
The water phase includes water and water-soluble ingre- which loves the water phase. This makes emulsions pos-
dients such as sugar, mustard seeds, proteins, vitamins, sible by connecting two phases that do not naturally mix.
minerals, and some thickening agents.

13
 Mixtures
Emulsions

Coalescence and creaming

The main types of separation in emulsions are creaming
and coalescence, with fat separation as a result. Cream-
ing occurs when the difference in density between the
fat droplets and the surrounding liquid is too high, and
makes the fat droplets rise to the surface. By reducing
the droplet size, either through high shear mixing or ho-
mogenization, the speed at which the fat droplets rise
to the top is slowed (see Stoke’s law on page 10). Milk
is one example of an emulsion where homogenization
is necessary to reduce droplet size in order to prevent
creaming, and increase stability.

Coalescence occurs when small droplets form larger

droplets in order to decrease the contact surface to the
liquid. It is possible to prevent coalescence with the help
of emulsifiers. Emulsifiers are surface-active compounds
that adsorb at the interface of the two phases, lowering
the interfacial tension that causes coalescence.

Creaming Sedimentation Optimal Flocculation Coalescence

14
How to make a stable emulsion Continuous phase, water phase
Mixing fats and oils into water-based liquids is a major
mixing challenge, since water and oil are insoluble in
each other. Emulsification of fat into a water phase is,
however, a fundamental step in the processing of many
foods. The challenge lies in achieving a stable formula-
tion where the oil phase is finely dispersed into the water Fat particles
phase, or less commonly, water is dispersed in oil.

Achieving a stable emulsion takes significant energy and

requires the presence of emulsifiers such as proteins or
specially designed emulsifying additives. The emulsifiers Surfactant
are surface-active molecules, meaning that one part of
the molecule orients itself into the oil phase (the lipo-
philic tail) and the other part orients itself into the water
phase (the hydrophilic head), thus forming a barrier that
stabilizes fat globules. Without a stable emulsion, fat
separates into an undesirable layer on top of the water
phase. Droplet size is also important to the stability of an
emulsion. The smaller the droplet size, the more stable
an emulsion will be. The drop size of emulsions typically
ranges from 1 to 10 µm.

15
 Efficient mixing technology secures
consistent quality and cost savings.

16
Mixtures
Understanding key mixing challenges
Air incorporation and foaming Air incorporation causes major problems in process-
One of the main challenges in mixing powders with ing and end-product quality. Air in the product may
liquids lies in preventing unwanted air and foaming. cause increased fouling in heat exchangers, cavita-
Air may be incorporated into a product by mixers tion in homogenizers, and unwanted whey formation
with whipping action or when adding ingredients in fermented products. Fouling in heat exchangers
such as powder, which tends to trap air. leads to shorter running times and increased clean-
ing time. Cavitation in homogenizers leads to higher
Air bubbles rise to the surface in a product. From maintenance costs. In terms of product quality, air
there, they escape. However, if foam-stabilizing in- in the product can cause oxidation, both during pro-
gredients such as protein are present, they stabilize cessing and in the package on the way to consumers.
into foam at the product’s surface instead. Air may Oxidation increases risk for off flavours, browning,
dissolve into products and cause foaming later in the and loss of sensitive nutrients such as vitamin C.
production process.
Air incorporation can also lead to significant product
losses in production – if the air creates large volumes
of unwanted foam in mixing tanks and other equip-
ment, since foam is nearly impossible to remove.

17
18
Lumping Clogging
The formation of lumps when mixing powders with liq- The formation of particularly large lumps in a product
uids also presents a challenge to food processors. Lump- is sometimes an issue if the cohesive powder ingredi-
ing is of particular concern when working with high vis- ent has been exposed to moisture. These large lumps
cous stabilizers and other powders, such as cocoa, that can cause clogging in equipment, reducing production
are difficult to wet. Lumps occur when a large amount of capacity and operational efficiency.
powder is added to the liquid phase all at once. When
this happens, stabilizers can form a gelling surface
around powder particles. The gelled surface prevents
the liquid from fully wetting the powder and causes the
powder to lump. The functionality of a stabilizer is not
utilized efficiently when lumping occurs, meaning that
more must be added to the recipe to achieve the same
functional results.

Powder lumping reduces the stability of a product and

may lead to sedimentation, which shortens shelf life.
Lumps may also cause sterility problems in the product
since the inner temperature of lumps may not meet the
required temperature during heat treatment.

19
 The right solution conquers mixing challenges
Preventing air incorporation and foaming

The right solution overcomes the mixing challenges just injected through powder inlets positioned on the mix- forated stator. This motion creates the high shear forces
described and ensures efficient operations with longer ing tank body well below the liquid surface. The valves required to ensure that both easily dissolved ingredients,
production hours, lower maintenance costs, and safe, regulating powder flow flip open and close intermittently such as skim milk powder, as well as typically difficult to
high quality end products. in order to maintain vacuum inside the tank. Although dissolve ingredients, such as pectin and xanthan gum,
vacuum mixing minimizes air in a product, all powders dissolve efficiently and completely. The high shear forces
Choosing the right mixing equipment still trap some air in or between the powder particles, are also strong enough to emulsify oils, providing that
It is important to look at the entire processing line and making it impossible to remove it all. In order to minimize emulsifiers are present and that the oil phase is liquid.
take all measures to minimize air and foam – especially air incorporation through powder addition, it is impor-
when working with a product that is sensitive to air in- tant to optimize the opening time of the valves. It is also possible to use a rotor and stator mixing unit
corporation and foams easily. It is important to consider without vacuum, where powder is added on the liquid
the type of mixing equipment, the design of surround- Advantages of rotor and stator mixing surface. However, it is then crucial to control the mixing
ing equipment, how powder is added, and processing When not using a vacuum mixer, it is important to mini- vortex more carefully in order to prevent surface turbu-
temperature. All these factors also depend on the spe- mize mixing time and thus minimize time during which lence and to prevent the vortex from reaching down to
cific ingredients and formulation of each unique specific air could be incorporated into the product. the mixing head, both of which would incorporate air.
product. It is also important that the mixer is placed deep under
Minimizing mixing time requires an effective mixer. A the liquid surface, ensuring calm rather than turbulent
Advantages of vacuum mixing robust solution for this is a mixer that utilizes a rotor and liquid surface and thereby avoiding air being whipped
Using a vacuum mixer is an effective way to minimize stator to produce the high shear forces required to ef- into the product.
air incorporation and foaming in a product. In a vacuum ficiently dissolve, emulsify and disperse ingredients to
mixer, the mixing tank is evacuated and vacuum is cre- achieve a smooth homogenous product and effective
ated inside. The liquid surface then borders vacuum in- wetting of powder. In a mixing unit with a rotor and stator,
stead of air. Thus, whipping action inside the mixing tank liquid and powder is forced down to where the blades
does not create air bubbles. In addition, ingredients are underneath the rotor push the mixture through the per-

20
Reduced air incorporation with vacuum mixers The solubility of air in liquid at different
This shows how air incorporation is minimized by using temperatures
vacuum: Since air incorporation affects the product so profound- ppm,O2
ly, measuring how much air is incorporated in a product
1. High speed blender, like a pump and a powder and finding a solution to minimize it is important. Dis- 12,0

hopper with venturi nozzle. solved oxygen meters easily measure the dissolved air
2. High shear mixer with a rotor and stator in ppm oxygen but “free air” or volume of bubbles is 8,0
technique. much more difficult to measure. With foam resting on
3. High shear mixer with a rotor and stator top of the product, it is impossible to measure a homog- 4,0
technique combined with a vacuum. enous product sample. However, it is possible to meas-
ure changes in total volume, since foaming increases
10 20 30 40 50 Temperature, °C
volume, in order to determine how much air has been
incorporated. This graph uses this measuring technique
Air in the product, volume index
to show how air incorporation can be minimized by using
a vacuum and rotor and stator mixing unit.

Choosing the right temperature

To further minimize air incorporation, it is also impor-
tant to choose the right processing temperature for each
product. For example, it is useful to perform the mixing
process at a higher temperature since air is less soluble
in a warm environment.
1 2 3

21
 The right solution conquers mixing challenges
Preventing lumping and clogging

To prevent lumping and clogging, it is important to han- liquid surface and transporting it quickly down towards the case with pectin, for example. In some formulations
dle powder correctly, choose the right equipment with the mixing head in a controlled vortex, achieves optimal that contain fat, such as some flavoured milks, it can be
high shear forces, control how the powder is added to wetting of powder by ensuring maximum exposure to helpful to perform the mixing process at a temperature
the mix and choose the right mixing temperature. the liquid medium. Since there are no circulation loops above the fat’s melting point. In other formulations, such
around the mixer, the entire mixture in the vessel is as herb butters, it is necessary to perform the mixing
Some cohesive powders, such as stabilizers, tend to forced through the mixing head more often than in con- process at a temperature below the fat’s melting point.
lump if not stored or handled properly. Powders stored ventional systems with circulation loops. This efficiently
in a humid environment, for example, absorb moisture mixes powders with low wettability or solubility as well
and form lumps. Vacuum mixing makes it possible to as products with very high viscosity.
store and dose the powder in a separate processing hall
designed for storing and handling powders. This ensures Advantages of pre-mixing
that powders are not exposed to the humid environment These same difficult powders also benefit from being
of the mixing area and prevents related lumping and mixed with other powder ingredients, such as sugar, be-
clogging issues. fore being added to a liquid mix. This allows stabilizers,
for example, which must otherwise only be introduced
Many powders that tend to lump, such as stabilizers, are intermittently and in small amounts, to be added all at
also notoriously difficult to disperse. These difficult pow- once in a steady stream and dispersed more quickly into
ders require high shear mixing to prevent lumping and the liquid.
clogging. The mixer may be mounted either below or
inside the tank. To achieve the high shear forces required Choosing the right temperature
for full dispersion of difficult powder ingredients, it is To more easily dissolve high-viscosity powders in larger
important that the design of the tank and the rotor and amounts, it is common to process at a higher tempera-
stator are optimized. ture. Some powders with specific functional properties
may also require processing at a higher temperature
Advantages of batch mixers in order to activate these functional properties. This is
When dealing with difficult powders and highly viscous
products, batch mixers, with the mixing unit inside the
mixer tank, are the ideal solution. Dosing powder on the

22
Powerful controlled vortex
ensures maximum exposure to
liquid for optimal wetting of powder
23
and minimal air incorporation.
 Mixing guidelines

Below are mixing guidelines for some common prod- Pectin is hygroscopic and difficult to mix in water. How- fully dissolve the pectin. After this, more water, sugar,
ucts/ applications. These guidelines are general exam- ever, using a highly efficient mixer with a rotor and stator and milk ingredients are added at low temperatures.
ples and the choice of ingredients and processing equip- technique enables pure pectin to be added to water. The mix is switched to an external circulation tank, and
ment must also be considered. Dry-blending with sugar eases the mixing of pectin in cooled to minimum 40°C. Then juice is mixed with the
water even further. milk-base and pH is adjusted to circa 3.8 to 4.0. Next,
Pectin solutions high shear mixing helps pectin adsorb effectively to milk
Pectin is a common ingredient used in products such Once a pectin solution is prepared, it is heat treated to proteins and homogenization eliminates any large pro-
as yoghurt, milk-juice beverages and jams. In formulat- reach over 70°C in order to fully dissolve the pectin. A yo- tein aggregates, ensuring full pectin adsorbtion to milk
ing water-based products with pectin, a mixing vessel ghurt base mixed with a pectin solution, is homogenised proteins. This prevents proteins from aggregating dur-
is filled with hot water at 70 to 80°C. Pectin is gradually in the heating stage in order to achieve optimal stability ing final heat treatment and aseptic filling. Pectin is also
added to reach the desired concentration, up to 10% at in the final product. Pectin prevents the milk proteins suitable for acidified soy milk drinks and whey drinks.
80°C, and the pectin solution is added to the final prod- from aggregating during this heat treatment.
uct. Pectin may be added directly to a final product if the To formulate milk-juice beverages, a circa 5% pectin solu-
temperature, pH, or shear rates are sufficiently high to High acid protein drinks tion is made by dissolving pectin into 70°C to 75°C heat-
prevent immediate gelation and the final product reach- Milk-juice beverages, known as directly acidified milk ed water. Then water at 50°C is metered into the mixing
es 70°C to 80°C enabling full pectin functionality. Once drinks, are created by mixing juice and milk in varying system and milk powder, melted butter oil, and sugar are
the pectin has been dissolved and reached functionality, concentrations. Juice lowers the pH level of the product added. The rest of the mixing process follows the same
it is important to not subject the product to high shear and this requires the use of a stabilizer to protect the procedure as for milk-juice beverages with fresh milk.
force, which may lead to an undesirable breakdown in milk proteins from aggregating. Pectin is the stabilizer
product texture. most often used in directly acidified milk drinks, as well Recombined milk
as acidified soy milk and whey drinks. To achieve the best mixing results in recombined and
Long life yoghurt-based drinks reconstituted milk, the optimal mixing temperature is
Pectin is often used as a stabiliser for long life yoghurt- The formulation of milk-juice beverages with fresh milk, 45°C to 50°C since the rate of dissolution of milk pow-
based drinks. A pectin solution of 2 to 4% is added to the begins with the creation of a 5% pectin solution by dis- der is much faster at higher temperatures. The greatest
yoghurt base after fermentation. The optimal pH range solving pectin into heated water, or a heated milk base increases in dissolution rate are seen in the tempera-
for mixing is 3.8 to 4.2. at 70°C to 75°C. The solution must be heated to 70°C to ture intervals from 10°C to 30°C. Thereafter, from 30°C

24
up to 45°C, smaller increases are seen. And raising the
temperature above 50°C has not been shown to achieve
any more positive effect on the speed of powder dis-
solution. It is important to note here that when working
with products with high dry matter content, the effect of
temperature on powder dissolution rate is even stronger
than when working with products with normal milk dry
matter content.

The high temperature also enables the milk components

to establish full dissolution on a molecular level more
quickly since the molecules move faster, something that
cannot be achieved with a mixing unit alone, no matter
how efficient it is. However, it is very important to use an
efficient mixer in combination with the right processing
temperature, to minimize the time it takes to establish
equilibrium. In an efficient mixer, the first phase of dis-
solution is achieved almost instantly when the product
passes through it. Further, recombining and reconstitut-
ing at a higher temperature also ensures less air incor-
poration than if the mixing process is performed at a
lower temperature.

When recombining and reconstituting milk at a higher

temperature, it is crucial to be aware of the risk of micro-
biological growth in the product if it is held for too long
at the higher temperature.

25
26
Mixing guidelines

Chocolate milk The right mixing temperature and mixing process is also Then, an emulsifier, such as egg powder or starch must
Chocolate milk is produced by mixing either fresh pas- important. It is most efficient to mix the cocoa, sugar be added to the water phase. Finally, oil is slowly added
teurised milk, or recombined pasteurised milk, with co- and other additives such as stabilizers, at 55°C with one to the mixture. In order to achieve a stable emulsion,
coa powder and sugar. And it is usually stabilized, with tenth of the total amount of milk in a recipe. This way, it is important to minimize the oil droplet size. This is
for example carrageenan, to prevent the sedimentation the cocoa undergoes a higher mixing intensity than if it achieved with a high shear rotor and stator.
of cocoa particles during storage. The content of cocoa is mixed with total amount milk right away. In addition,
powder in chocolate milk is usually in the range of 1.5 to cocoa dissolves more fully and quickly in warm milk than This mixing technology is valid for:
2% and a dark, alkalized cocoa powder with a fat content in cold milk. After this pre-mixed slurry is complete, it Hot-hot emulsification: The hot oil phase and the water
of 22 to 24% is normally used for chocolate milk. The pH is then cooled down and/or mixed with the remaining phase are combined under vacuum at a high tempera-
of the cocoa powder should be as close as possible to milk before further heat treatment and packaging. Tra- ture (70°C to 85°C) and emulsified.
the pH of the milk. ditional recommendations call for pre-pasteurisation of
the cocoa slurry. Hot-cold emulsification: The hot phase and the cold wa-
The quality of the milk required for making chocolate ter phase are combined under vacuum and emulsified at
milk is the same as for milk intended for pasteurisation Mayonnaise the mixing temperature.
or UHT sterilization without flavouring additives. The The amount of fat and vegetable oil used in a mayon-
quality of cocoa powder can vary greatly but to mini- naise formulation depends on the fat content desired in Cold-cold emulsification: The water phase and the oil
mize sedimentation and bacteriological problems, the the final product. For example, the production of may- phase are kept cold and are combined and emulsified
powder must be finely ground and have a low content onnaise with lower fat content requires more powder in- under vacuum.
of shell particles. gredients and emulsifiers to stabilize the emulsion and
achieve desired properties.
A common challenge when working with cocoa powder
is that it tends to float on the surface of the milk and is dif- In mayonnaise production, the water phase is stabilized
ficult to wet. An efficient mixer conquers this challenge to increase viscosity by dispersing powder ingredients,
since the mixing head forces all product in the mixing such as starch. The starch used to increase viscosity may
vessel down and through the mixing unit. be either cold swelling or hot swelling starch. If the starch
is hot swelling, the water phase and starch must be heat-
ed to above the swelling point.

27
 © 2011, Tetra Pak Processing Systems, Lund, Sweden, br20559en, 2011-07
Tetra Pak, and protects what’s good
are trademarks belonging to the Tetra Pak Group.