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Drilling Fluids

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SKM 3413 - DRILLING ENGINEERING

Chapter 2 - Drilling Fluids


Assoc. Prof. Abdul Razak Ismail

Petroleum Engineering Dept.


Faculty of Petroleum & Renewable Energy Eng.
Universiti Teknologi Malaysia
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Functions of drilling fluids


• Cools & lubricates the bit & drill string
• Suspends cuttings & weighting materials when
circulation is stopped
• Supports part of the weight of the drill string
or casing
• Controls subsurface formation pressures
• Removes & transports cuttings from the
bottom of the hole to the surface

Assoc. Prof. Abdul Razak Ismail, UTM


3

Functions of drilling fluids (ctd)

• Walls the hole with an impermeable filter cake


• Minimizes sloughing & caving of the
formation.
• Helps to obtain good, downhole data for
formation analysis.
• Transmits hydraulic horse power to the bit.
• Prevent corrosion fatigue of drill pipe

Assoc. Prof. Abdul Razak Ismail, UTM


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To achieve these functions, the following side effects


must be minimized (mud should not):
• Reduce the penetration rate
• Loss of circulation
• Erode of the borehole
• Corrode the drill string
• Wear on the pump parts
• Swell the borehole creating tight spots
• Damage the subsurface formation, especially the potential pay section
• Stuck the drill pipe against the walls of the hole
• Hamper evaluation of the productive zone
• Require excessive pump pressure at the desired circulation rate
• Allow suspension & continual circulation of undesirable solids and/or
abrasive solids such as cuttings, encountered clay & fine sand

Assoc. Prof. Abdul Razak Ismail, UTM


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Advantages of having a good mud cake


on permeable formation
• Minimizes formation damage (affecting both
formation evaluation & production)
• Improves hole stability (avoiding wall stuck
pipe, swabbing & pressure surges)
• Reduces fluid loss
• Reduced contamination of formation
• Reduced sloughing & caving

Assoc. Prof. Abdul Razak Ismail, UTM


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To obtain more efficient cuttings removal:

• Increase annular fluid velocity (if too low)


• Change flow pattern
• Increase mud viscosity

Assoc. Prof. Abdul Razak Ismail, UTM


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What is “rheology”

 The study of how matter deforms and flows.


 Primarily concerned with the relationship of shear
stress and shear rate and the impact these have on
flow characteristics inside tubulars and annular
spaces.

Assoc. Prof. Abdul Razak Ismail, UTM


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Components of drilling fluid


Liquid phase
(eg. water, oil, emulsion)

Inert phase Drilling


(eg. barite, sand) Chemical phase
fluid

Colloidal phase
(eg. clay)

Assoc. Prof. Abdul Razak Ismail, UTM


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Common mud addtives


Weighting Materials Viscosifiers (Thickeners)
 Barite  Bentonite
 Hematite  Attapulgite
 Galena  Asbestos
 Calcium carbonate  Polymers
 Dissolved salts Lost-Circulation Materials
Emulsifiers  Granular
 Oil in water  Fibrous
 Water in oil  Flaked
 Slurries
Viscosity-Reducing Chemicals
 Phosphates Special Additives
 Tannates  Flocculants
 Lignites  Corrosion control
 Lignosulfonate  Defoamer
 Sodium polyacrylate  pH control
 Mud lubricant
Fluid-Loss Reducers  Antidifferential sticking material
 Starches
 CMC
 Polyanionic cellulose Acrylates
 Bentonite
 Dispersants
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Assoc. Prof. Abdul Razak Ismail, UTM
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Weighting material additives

Assoc. Prof. Abdul Razak Ismail, UTM


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Viscosifier additives

Assoc. Prof. Abdul Razak Ismail, UTM


Types of mud

OIL BASED
MUDS

Mud
types

GASES FLUIDS
WATER BASED (air, gas, mist, foam,
MUDS aerated muds)
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Assoc. Prof. Abdul Razak Ismail, UTM


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Classification of drilling fluids


(after IMCO Petroleum Services)
DRILLING
FLUIDS

Oil base Water base Pneumatic

Non- Mist or
True Invert Inhibitive Air Gas
inhibitive foam

Minimum
Lightly solids Ionic
Native Incapsulation
treated inhibition

Organic Inorganic Ca++ Na+ K+ NH4+


Assoc. Prof. Abdul Razak Ismail, UTM
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Classification of drilling fluids


(after API, “Principle of Drilling Fluids Control”, 1972, p. 67)

A. Water-base drilling muds


• Fresh-water muds (little or no chemical treatment)
1. Inhibited muds
2. Spud muds
3. Natural muds
• Chemically-treated muds (no calcium compounds added)
1. Phosphate muds
2. Organic-treated muds
a. Lignite
b. Quebracho and other extracts
c. Chrome-lignosulfonate
• Calcium-treated muds
1. Lime
2. Calcium chloride
3. Gypsum
Assoc. Prof. Abdul Razak Ismail, UTM
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Classification of drilling fluids (ctd)


(after API, “Principle of Drilling Fluids Control”, 1972, p. 67)

• Salt-water muds
1. Sea-water muds
2. Saturated salt-water muds
• Oil-emulsion muds (oil-in-water)
• Special muds
1. Low-solids oil-emulsion muds
2. Low-clay-solids weighted muds
3. Surfactant muds
4. Low-solids muds
a. Clear water
b. Polymer muds
c. Low-solids, non-dispersed muds

Assoc. Prof. Abdul Razak Ismail, UTM


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Classification of drilling fluids (ctd)


(after API, “Principle of Drilling Fluids Control”, 1972, p. 67)

B. Oil-base drilling muds


• Oil-base muds
• Invert emulsion muds (water-in-oil)

C. Gaseous drilling fluids


• Air or natural gas
• Aerated muds
• Foams

Assoc. Prof. Abdul Razak Ismail, UTM


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A. WATER-BASE MUDS
• Most widely used
• Consist of :
– Liquid phase (e.g. water, emulsion)
– Colloidal phase (e.g. clays)
– Inert phase (e.g. barite, sand)
– Chemical phase

Assoc. Prof. Abdul Razak Ismail, UTM


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Inhibited muds
• A mud having an aqueous base with a chemical
composition that tends to retard or prevent (inhibit)
appreciable hydration (swelling) or dispersion of
formation clays & shales through chemical and/or
physical means
• Includes salt-water muds, chrome lignosulfonate
muds, surfactant treated muds, etc.

Assoc. Prof. Abdul Razak Ismail, UTM


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Spud muds

• The characteristics of the mud used for


spudding-in (to start the hole) a well vary
widely over the world (some locations are
spudded-in in through conductor pipe already
cemented in the cellar & some locations
require that the length of the kelly & a few
joints of drill pipe be drilled down in order to
cement one or more joints of conductor casing)

Assoc. Prof. Abdul Razak Ismail, UTM


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Natural muds
• Composed of water & clays from the formation
drilled, with little chemical treatment & with minor
amounts of bentonite or other clays added
• Usually used to drill the surface hole & for fast
drilling below the surface casing
• In most cases, the natural muds will be chemically
treated as the depth of the well increases & will
become one of the chemically treated muds discussed
below.

Assoc. Prof. Abdul Razak Ismail, UTM


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Phosphate-treated muds
• For relatively shallow wells (7,500´ or less)
 cannot with stand temperatures > 180°F &
not effective when the mud is contaminated by
salt or calcium
• Complex phosphates are very effective in
reducing the , gel strength & filtration rate

Assoc. Prof. Abdul Razak Ismail, UTM


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Wood & bark extract treated muds


• Treatment of natural mud with caustic soda &
quebracho extract was once widely practiced
(particularly in the 1940 - 50 period)
• Gives pH of 10 - 12
• Other types of organic treatment, however, have now
largely replaced the caustic-quebracho treatment e.g.
modified hemlock bark extracts

Assoc. Prof. Abdul Razak Ismail, UTM


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Chrome lignosulfonate muds

• Used to minimize shale problems


• Can be used in high T wells e.g. up to
400 °F.

Assoc. Prof. Abdul Razak Ismail, UTM


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Calsium treated muds


• Tends to inhibit the swelling of clays & shale
 Control sloughing & hole enlargement,
excessive  increase
• The most serious problem with Ca treated
muds was severe gelation with time at high
temperatures & high pH

Assoc. Prof. Abdul Razak Ismail, UTM


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Saltwater muds
• If chlorite ion > 1% (6,000 ppm)
salt water .
• Bentonite & clays hydrate less when added to
water containing >1% salt.

Assoc. Prof. Abdul Razak Ismail, UTM


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Seawater muds
• On offshore & buy location, fresh water is
sometimes not available for mixing water
• Sea water contains Na, Ca, Mg ions.

Assoc. Prof. Abdul Razak Ismail, UTM


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Oil-emulsion muds
• Oil was mixed so that the oil is suspended as
individual droplets in the water phase.
• The emulsion must be stable  to prevent the oil
from suspended at top  add emulsifier.
• Advantages :
1. Improved hole condition
2. Increased bit life
3. Increased drilling rate

Assoc. Prof. Abdul Razak Ismail, UTM


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Surfactant muds
• Surface acting agent i.e. a material capable of acting
upon the surface of a material
• Mud types:
- Calcium surfactant
- Low sodium surfactant
- Saturated salt surfactant
- Sea water surfactant

Assoc. Prof. Abdul Razak Ismail, UTM


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The pH of common mud treating agents


Chemical Name pH
Barium carbonate, BaCO3 10.0
Sodium bicarbonate, NaHCO3 , baking soda 8.3
Calcium sulfate, CaSO4.1/2 H2O , gypsum-plaster 6.0
Chrome lignosulfonate 3.4 – 4.0
Sodium carbonate, Na2CO3 , soda ash 11.0
Calcium hydroxide, Ca(OH)2 , slaked lime 12.0
Sodium hydroxide, NaOH , caustic soda 13.0
Calcium lignosulfonate 7.0
Lignite 5.0
Quebracho 3.8
Sodium acid pyrophosphate, Na2H2P2O7 4.8
Sodium hexametaphosphate, (NaPO3)6 6.0
Sodium tetraphosphate, Na6P4O13 7.5
Tetrasodium pyrophosphate, Na4P2O7 9.9
Assoc. Prof. Abdul Razak Ismail, UTM
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B. OIL BASE & INVERT EMULSION MUDS


• Oil is the continuous liquid phase (e.g. diesel)
• For safety, flash point must be > 150 °F
• Application:
– protection of producing formations
– drilling deep, hot holes
– preventing differential P sticking
– coring
– packer fluids & casing packs
– mitigating severe drill string corrosion
– drilling troublesome shale

Assoc. Prof. Abdul Razak Ismail, UTM


Why use oil based muds?
Advantages: Disadvantages:
• Good rheological properties at • High initial cost
temperatures as high as 500 oF • Requires more stringent
(especially deeper well) pollution-control
• More inhibitive than inhibitive procedures
WBMs • Reduced effectiveness of
• Effective against all types of some logging tools
corrosion • Remedial treatment for
• Superior lubricating characteristics lost circulation is more
• Increase bit life & improve difficult
penetration rate • Detection of gas kicks is
• Permits rm as low as 7.5 ppg more difficult because gas
• Reduce formation damage solubility in diesel oil
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Assoc. Prof. Abdul Razak Ismail, UTM
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Why use ester based drilling fluids?


• Advantages:
– Environmental friendly
– Biodegradable
– Local product-derived from palm oil
• Limitations:
– Suitability/properties
– High cost

Assoc. Prof. Abdul Razak Ismail, UTM


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C. GASES FLUIDS
(air, gas, mist, foam, aerated muds)
• Why gases are used?
 lowest ρ: to prevent from damage & lost
circulation
• Air drilling :
a. Dry drilling or dusting
b. Mist or foam drilling: water or a special mud
is injected with a foaming agent into the air
stream
c. Stable foam drilling
d. Aerated mud drilling
Assoc. Prof. Abdul Razak Ismail, UTM
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Rheological models

Assoc. Prof. Abdul Razak Ismail, UTM


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Mud properties
• Density (mud weight) • Emulsion stability
• Viscosity • Resistivity
• Gel strength • pH
• Filtration • Lubricity
• Mud cake • Etc.

Standard drilling fluids testing:


- API RP 13B-1 (Recommended Practice for Field Testing Water-Based Drilling Fluids
- API RP 13B-2 (Recommended Practice for Field Testing Oil-Based Drilling Fluids

Assoc. Prof. Abdul Razak Ismail, UTM


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Density or mud weight


m
•  (ppg, lb/cuft, S.G., ppb, psi/1000´)
v
• Mud balance  calibrated at 8.33 ppg (water) or
62.4 lb/cuft or 1.0 g/cc

Assoc. Prof. Abdul Razak Ismail, UTM


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Viscosity
υ A

F υ
l

υ=0

ML/T 2
shearing stress F/A L 2 M
μ   
rate of shearing strain /l L/T LT
L
Assoc. Prof. Abdul Razak Ismail, UTM
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• Water, oil, etc: Newtonian fluids (constant )


• Drilling fluids: Plastic or non-Newtonian fluids
( is not constant)
 certain value of stress
(true yield point) must be
exceeded in order to
initiate movement

Assoc. Prof. Abdul Razak Ismail, UTM


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Flow behavior of plastic and Newtonian fluids


Shearing stress or pressure

Yb, Bingham yield

Transition from plug to laminar flow

Plug flow

Yt, True yield

Rate of shear or velocity


Assoc. Prof. Abdul Razak Ismail, UTM
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(a) Marsh funnel


– The funnel is filled to the upper mark (1500 cc) with
freshly collected, well agitated mud
– Measures the time for 1 quart (946 cc)
 comparative
– Calibration: 26  0.5 sec. (water)

Assoc. Prof. Abdul Razak Ismail, UTM


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(b) Rheometer
– Determine:  µa , µp , Yb , gel or shear strength

µp = Φ600 - Φ300 cp
µa = ½ Φ600 cp
Yb = Φ300 - µp lb/100 ft2

– From these relationships:


Yb = 2(µa - µp) or
µa = µp + ½ Yb

Assoc. Prof. Abdul Razak Ismail, UTM


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• True yield point (from previous graph) is normally


defined by the following equation:
Yt = 3/4 Yb

Slope proportional to µp
Dial deflection, F

Slope proportional to µa
Plug flow

Yt, True yield

300 600
Setting, rpm
Assoc. Prof. Abdul Razak Ismail, UTM
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Gel strength
• A measure of the shearing stress necessary
to initiate a finite rate of shear
• Measured at 3 rpm using rheometer
• Reported as initial gel strength (10 sec.) &
final gel strength (10 min.)

Assoc. Prof. Abdul Razak Ismail, UTM


44

Filtration properties
• Filter press: measure the filtration, water
loss & mud cake thickness
• Using 100 psig, filter paper
• Filtrate volume: cc/30 min.
• Mud cake thickness: /32 in.
• In field testing, it is common practice to
double the 7 ½ min. filtration loss & report
this as the 30 min. figure
Assoc. Prof. Abdul Razak Ismail, UTM
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• This procedure is based on the observation that:

V 2  V1 t 2 / t1
where: V2 = filter loss at t2 , cc
V1 = filter loss at t1 , cc
t1 , t2 = filtration time, min.

• This procedure does not account for the initial spurt


(high filter loss) period which occurs before the mud
solid bridge on the filter paper

Assoc. Prof. Abdul Razak Ismail, UTM


46

For some muds the spurt loss may be considerable


volume and should be corrected as follows:
Apparent water loss
Corrected water loss
Filtrate volume, cc

0 1 2 3 4 5 30 6
Time

0 1 4 9 16 25 30 36
Time, min.
Assoc. Prof. Abdul Razak Ismail, UTM
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• Filtration loss may be corrected for T changes by:

V2  V1 1 /  2

where: V2 = corrected water loss at T2


V1 = measured water loss at T1
µ1 = viscosity of liquid phase at T1
µ2 = viscosity of liquid phase at T2
T1, T2 = temperatures in question

Assoc. Prof. Abdul Razak Ismail, UTM


48

Other mud tests


TEST APPARATUS PURPOSE
pH pH paper or pH meter Guide to chemical treatment (to measure pH of
whole mud, filtrate, and filter cake)
Filtrate Standard chemicals Determination of contaminant to select
analysis such as acid, chemical treatment
indicators, etc.
Sand content Screens, measuring Determination of sand content in the mud to
tube, centrifuge prevent abrasion of pump & drill pipe
Oil, water, Distillation kit Guide to control the desired properties (to
solids content determine oil, water & solid content)
Clay content Methylene blue test To determine the amount of clay materials in
WBM
Emulsion Electrical stability To indicate the relative strength of emulsions
stability tester having a continuous oil phase
Lubricity Lubricity tester To measure the lubricity of the muds
Resistivity Resistivity meter To measure resistivity of muds, filtrates, filter
cakes, and slurries
Assoc. Prof. Abdul Razak Ismail, UTM
49

The pH of Common Mud Treating Agents


Chemical Name pH
Barium carbonate, BaCO3 10.0
Sodium bicarbonate, NaHCO3, baking soda 8.3
Calcium sulfate, CaSO4.1/2H2O, gypsum-plaster 6.0
Chrome lignosulfonates 3.4 – 4.0
Sodium carbonate, Na2CO3, soda ash 11.0
Calcium hydroxide, Ca(OH)2, slaked lime 12.0
Sodium hydroxide, NaOH, caustic soda 13.0
Calcium lignosulfonate 7.0
Lignite 5.0
Quebracho 3.8
Sodium acid pyrophosphate, Na2H2P2O7 4.8
Sodium hexametaphosphate, (NaPO3)6 6.0
Sodium tetraphosphate, Na6P4O13 7.5
Tetrasodium pyrophosphate, Na4P2O7 9.9
Assoc. Prof. Abdul Razak Ismail, UTM
Why monitor drilling fluids ?

• To identify potential hole problems


• To identify their causes
– could be poor hole cleaning
– hole erosion
– formation damage
– sensitive formations
– pressure control problems

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Assoc. Prof. Abdul Razak Ismail, UTM
51

Mud Properties
Properties The Importance
Density  Pressure control  p = ± 200 psi (overbalance)
m
pm  X 0.433 D  0.052  m D
8.33
Mud Filtrate  Mud ability to form a thinner mud cake with low permeability on the
wall of porous medium.
 Thicker mud cake means more solid materials settled at formation wall
and more filtration lost to the formation.
 Thicker mud cake easier to collapse and cause other problem during
drilling activity such as the hole becomes smaller.
Gel Strength  The ability of mud to suspend solids (especially weighting materials,
drilled cuttings).
 Very important in suspended drilling operation.
Yield Point  The amount of pressure (shearing stress) needed to be applied to flow
the mud.
 Very important in determining pump capacity and the amount of
pressure needed to be applied to flow the mud from static positions.
Gel strength  Carrying capacity of the mud.
+ Yield Point
Thinner  The reduce mud viscosity (Yb, a, gel strength) without reducing the
mud density.
Weighting Materials  The increase mud density without causing any reaction in the mud
(inert materials).
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Assoc. Prof. Abdul Razak Ismail, UTM
52
Mud Selection Criteria
Criteria Comments
Wildcat Geological information is primary consideration.
Well type
Development Generally allow full use of optimized techniques.
Sloughing shale Formulate fluid to control sloughing.
Formation Anhydrite If minor, treat out calcium; massive anhydrite requires specialized mud
Salt If salt contamination exceeds 10,000 ppm, a salt-based mud is required

High temperatures Static BHT above 225°F reduces effectiveness of additive, problem
magnified by high clay-solids content

Lost circulation Batch treatment successful for minor or intermediate losses; special
technique required for major losses

Composition Test and treat makeup water to remove calcium and magnesium; use
flocculants to remove clay solids
Makeup water
Availability Quantity and type are important in fluid selection

Rig selection Rigs should have proper solids-removal equipment and adequate
circulating horsepower.
Nature of producing formations Type of fluid selected is dependent on rock characteristic of reservoir.
Casing program Drilling fluid(s) used may be determined by casing string depths.

Availability of products In remote, international areas, drilling fluid type may depend on
product availability.
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Assoc. Prof. Abdul Razak Ismail, UTM
53

Drilling Fluids Mistakes


• Not testing the quality of the make-up water & treating it properly
• Mixing the additives too rapidly or in an incorrect order
• Not matching the correct drilling fluid with soil type
• Mixing too low of a concentration of additives to allow them to
perform properly
• Failure to maintain slurry flow throughout the bore
• Failure to calculate the volumes of water & additives that are required
• Failure to calculate the drilling/reaming speeds so as not to outrun
fluid flow
• Poor bore planning
• Not calculating pullback rates vs. pump volume output
• Thinking that loss of fluid returns will not lead to problems
• Ignoring the importance of mud reclaiming systems and maintenance
Assoc. Prof. Abdul Razak Ismail, UTM
54

Converting field unit to laboratory unit


(ppb to g/cc)

g
454
lb lb lb g
1 1  
bbl bbl 42 gal  3785 cc 350 cc
bbl gal

lb g
 
bbl 350 cc

e.g. 12 ppb  12 g / 350 cc

Assoc. Prof. Abdul Razak Ismail, UTM

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