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Indian Standard: Specification For Indented Wire For Prestressed Concrete

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IS : 6003.

1983
( Reaffirmed 1997 )
Indian Standard
SPECIFICATION FOR INDENTED
WIRE FOR PRESTRESSED CONCRETE

( First Revision )
Second Reprint AUGUST 1993

UDC 669-124.3-426 : 620-l : 666-982-4

Q Copyright 1983

BUREAU OF INDIAN STANDARDS


MANAK UHAVAN, 9 BAHADUR SHAH ZAFAR MARQ
NEW DELHI llooO2

Gr 3 hdJJ 1983

-
IS:6003 - 1983

lndian Standard
SPECIFICATION FOR INDENTED
WIRE FOR PRESTRESSED CONCRETE

( First Revision )
Joint Sectional Committee for Concrete Reinforcement, BSMDC 8

Chairman Representing
SHRI G. S. RAO Central Public Works Department
Members
SU~P~;~~IKR ENGINEER
( Alternate to
Shri G.‘S. Rao )
DR J. L. AJMANI The Tata Iron & Steel Co Ltd, Jamshedpur
SHRI A. N. MITRA ( Alternate )
DR ANIL KUUAR C,ement Research Institute of India, New Delhi
SHRI E. T. ANTIA The Concrete Association of India, Bombay
SHRI I’. SRINIVASAN ( Alternate )
SHRI S. BANERJEE Steel Re-Rolling Mills Association of India,
Calcutta
SHRI S. N. CHANDA Metallurgical and Engineering Consultants ( India)
Ltd, Ranchi
SRRI R. D. CHOUDHARY ( Alternate )
CHIEF ENQINEER ( D&R ) Irrigation Department, Government of Punjab,
Chandigarh
DIRECTOR ( CD ) ( Alternate )
DEPUTY DIRECTOR, S~ANDAI~DS Research, Designs and Standards Organization
(B&S)-1 ( Ministry of Railways ), Lucknow
ASSISTANT DIRECTOR, STAN-
DARDS ( B&S )-II ( Alfernate )
SHRI D. I. DESAI Gammon India Ltd, Bombay
SHRI A. L. BHATIA ( Alternate )
SHRI M. R. DOCTOR Snecial Steels Ltd. Bombay
SHRI S. G. JOSHI ( Alternate ) *
SHRI ZACHARIA GEORGE Structural Engineering Research Centre (CSIR ),
Madras -
SHRI G. V. SUKYA KUMAR ( Alternate)
SHIU V. K. GHANE~AR Structural Engineering Research Ccntre ( CSIR 1,
Roorkee
SHRI D. S. PRAKASH RAO ( Alternate )
( Continued on page 2 )

@ Cojyright 1983
BUREAU OF INDIAN STANDARDS
This publication is protected under the Indian Copyright Act ( XIV of 1957 ) and
reproduction in whole or in part by any means except with written permission of the
publisher shall de deemed to be an infringement of copyright under the said Act.
( Contimed from pago 1 )

Members Representing
SHRI V. GULATI Heatly & Gresham ( India ) Ltd, New Delhi
SHRI P. K. GUP~E National Metallurgical Laboratory ( CSIR j,
, Jamshedpur
SJXRI N. C. JAIN Stup’Consultants Ltd, Boinbay
SHRI M. C. TANDON’ ( Alternate )
SHRI M. P. JASUJA Research & Development Centre for Iron and
Steel ( SAIL ), Ranchi
Snnr A. JAYAQOP~L Engineer-in-Chief”s Branch, Army Headquarters
MAJ R. CHANDRASEKHARAN
( Alternate )
SHRI S. Y. KHAN Killick Nixon Ltd, Bombay
SHRI P. S. VENKAT ( Alternate )
SHRI M. N. KHANNA Bhilai Steel Plant ( SAIL ), Bhilai
SHRI C. DASQUPTA_( Alternate )
SHRI H. N. KRISHNA MURTHY Tor Steel Research Foundation in India, Calcutta
DR C. S. VISWANATHA ( Alternate )
SHRI S. N. MANOHAR Tata Consulting Engineers, Bombay
SHRI N. NAQARAJ (Alternate )
SHRI R. K. MATI~WR Public Works Department, Lucknow
SSRI S. N. PAL M. N. Dastur & Co (Pj Ltd, Calcutta
SHRI SALIL ROY ( Alternate )
SHRI B. K. PANTHAKY Hindustan Construction Co Ltd, Bombay
SHRI P. V. NAIK ( Alternate )
SHRI T. SEN IRC Steels Ltd, Calcutta
SHRI M. V. SHASTRY - Roads Wing, Ministry of Shipping and Transport
SHRI SHIRISH H. SHAH Tensile Steel Ltd, Bombay
SHRI M. S. PATKAK ( Alternate )
SHRI C. N. SRINIVASAN C. R. Naravana Rao, Madras
SHRI C. N. RA~HAVENDRAN (Alternate ) ’
SHRI K. S. SRINIVASAN National Buildings Organization, New Denhi
SHRI A. K. LAL ( Alternate )
SHRI G. RAYAN, Director General, ISI ( Ex-ojicio Member )
Director ( Civ’Engg )
Secretary
Srrlr~ M. N. NEELKANDHAN
Assistant Director ( Civ Engg ), ISI

2
15:6003-1983

Indian Standard
SPECIFICATION FOR INDENTED
WIRE FOR PRESTRESSED CONCRETE

( First Revision )
0. FOREWORD
0.1 This Indian Standard ( First Revision ) was adopted by the Indian
Standards Institution on 14 March 1983, after the draft finalized by the
Joint Sectional Committee for Concrete Reinforcement had been approved
by the Civil Engineering Division Council.
0.2 This standard was first published in 1970 to cover the requirements for
indented hard-drawn and stress-relieved wire used in prestressed concrete
work. This revision has been taken up with a view to incorporating
modifications found necessary as a result of experience gained in using this
standard both by manufacturers and users.
0.3 In this revision, modifications have been incorporated in provisions
relating to manufacture and requirements of relaxation and susceptibility
to stress corrosion. Further SI units have been adopted in this revision and
references to related Indian Standards have been updated.
0.4 Requirements of plain hard-drawn steel wire for prestressed concrete
are covered in IS : 1785 ( Part I )-1983* and IS : 1785 ( Part II )-1983t.
0.5 In the formulation of this standard, due weightage has been given to
international co-ordination among the standards and practices prevailing
in different countries in addition to relating it to the practices in the field
in this country.
0.6 For the purpose of deciding whether a particular requirement of thi!
standard is complied with, the final value, observed or calculated, expres-
sing the result of a test or analysis, shall be rounded off in accordance with
IS : Z-19601. The number of significant places retained in the rounded off
value should be the same as that of the specified value in this standard.

*Specification for plain hard drawn steel wire for prestressed concrete: Part I Cold
drawn stress-relieved wire ( second revision ).
TSpecification for plain hard drawn stekl wire for presfressed concrete: Part II As-
drawn wire ( jirst revision ).
fRules for rounding off numerical values ( revised ).

3
IS t 6063 - 1983

1. SCOPE

1.1 This standard covers the requirements for manufacture, supply and
testing of indented hard-drawn and stress-relieved wire for use in prestressed
concrete.

2. TERMINOLOGY

2.0 For the purpose of this standard, the following definitions shall apply.

2.1 Bundle - Two or more ‘ coils ’ or a number of lengths properly bound


together.
2.2 Coil -- One continuous length of wire in the form of a coil.

2.3 Elongation - The increase in length of a tensile test piece under stress.
The elongation after fracture is conventionally expressed as a percentage of
the original gauge length of a standard test piece.

2.4 Indentation - The creation of a depression or a series of depressions


of particula; shape and dimension on the surface of the wire by some mecha-
nical process or otherwise without altering the mechanical ,and chemical
properties.

2.5 Nominal Diameter - The nominal diameter of the indented wire is


equivalent to the diameter of a plain wire having the same mass per unit
length as the indented wire.

2.6 Parcel - Any quantity of finished wire presented for examination and
test at any one time.

2.7 Proof Stress - The stress which produces a residual strain of 0.2 per-
cent of.the original gauge length ( non-proportional elongation ).

2.8 Tensile Strength - The maximum load reached in a tensile test


divided by the original cross-sectional area of the gauge length portion of
the test piece. .

3. MANUFACTURE AND CHEMICAL COMPOSITION

3.1 The wire sh 11 be cold drawn from the steel made by the open hearth,
electric duplex, L cid bessemer, basic oxygen, or a combination of these
processes. In case any other process is employed in the manufacture of
steel prior approval of the purchaser shall be obtained.
3.1.1 The ladle analysis when made in accordance with relevant parts
of IS : 228* shall show that the steel contains not more than 0.05 percent
of sulphur and not more than 0.05 percent of phosphorus.

*Meth& of chemical analysis of steels ( seco.ld reuisio.z ).

4
IS: 6003- 19S3

3.2 ‘l%e Ixu-s or wires obtained from the rolling mill shall be treated if
required to make it suitable for cold drawing and thereafter the diameter
of the wire of bar shall be successively decreased to the required diameter
by cold drawing it through a series of dies. The resultant wire shall be
indented and then subjected to straightening and stress relieving processes.

3.3 All finished wire, sul>ject to the provisions of 3.2 shall be clean and
uniformly drawn to the specified size and shape and shall be free from
splits, harmful scratches, surface flaws, piping and other defects likely to
impair its use in prestresscd concrete, and finished in a workmanlike
manner.

3.4 Unless otherwise agreed to between the purchaser and the manufacturer/
supplier, the wire shall not carry on its surface lubricants or other matter to
a degree likely to impair its adhesion to concrete. Slight rust may be
permitted, provided there is no surface pitting visible to the naked eye.

3.5 There shall be no welds in the finished wire as supplied to the purch-
aser. Any welds or joints made during manufacture to promote continuity
of operations shall be removed before supply.

4. NOMINAL SIZES AND GEOMETRICAL CHARACTERISTICS


4.1 Nominal Sizes — The nominal diameters ( see 2.5 ) of the finished
wires shall be 5“00, 4“00 and 3-00 mm.

4.2 Geometrical Characteristics — The shape and pattern of indenta-


tion shall be as mutually agreed to between th? manufacturer and the
purchaser provided the indentations are placed in two lines, diametrically
opposite and the opposite indentations are staggered so that no two indent-
ations are exactly opposite and also conform to the requirements in 4.2.1.
Two common types of indentations are illustrated in Fig. 1.

4.2.1 The pitch and the depth of indentation shall be uniform through-
out the length of wire.

5. TOLERANCES

5.1 The tolerance on the nominal diameter shall be -& 0.05 mm.
5,1.1 For purposes of determining whether the actual diameter of the
wire is within the specified tolerances, the diameter shall be determined
with a micrometer by taking two measurements at right angles to each
other at three places along a length of not less than 250 mm and the
average of these six measurements shall be taken as the diameter of the
wire.
NOTE — As the indenting is done after drawing, there are chances of the material
being compressed and this shall not be the cause of rejection.

5
c
IS: 6~3 - 1983 _

._--

1A ELLIPTICAL INDENTATIONS

l--PITCH4

18 ROUND INDENTATIONS

FIG. 1 ILLUSTRATIVESKETCH OF TYPICAL INDENTATIONSFOR


INDENTED WIRE
6. PHYSICAL REQUIREMENTS
6.0 The wire shall conform to the physical requirements specified in 6.1
to 6.5.
NOTE - Forspecial purposes, test evidence may be required to show that the
wire is not susceptible to stress corrosion. In such case, the test method shall be
mutually agreed upon between the manufacturer and the purchaser.
6.1 Tensile Btrength - Unless otherwise agreed to between the purchiser
and the manufacturer or supplier, the tensile strength of wire determined
in accordance with 7.3 and based on the nominal diameter of the, wire,
shall be as given below:
Nominal Diameter Tensile Strength
mm Mh, N/mm2
5.00 1 570
4.00 1 715
3.00 1 865
c
IS:6003-1983

6.2 Proof Stress - Unless otherwise specified, the proof stress of the wire
shall be not less than 85 percent of its minimum specified tensile strength.

6.3 Ductility - The wire shall withstand the reverse bend test specified
in 7.5.

6.4 Elongation After Fracture - Elongation after fracture, over a gauge


length of 200 mm, when determined in accordance with 7.6 shall be as
below:

Nominal Diameter Elongation Percent


mm Min
5.00 4.00
4.00 3.00
3.00 2.50

6.5 Relaxation - The relaxation stress in the wire when tested in accord-
ance with 7.7 shall not exceed 5 percent of the initial stress as specified
in 7.7 at the end of 1 000 h. Alternatively, the manufacturer shall provide
proof that the quality of wire supplied is such as to comply with this require-
ment.

6.5.1 When it is not possible’ to conduct 1 000 h relaxation test, the wire
may be accepted on the basis of 100 h relaxation test, provided the manu-
facturer furnishes proof establishing, a relation between the relaxation
stress values at 1 000 h and 100 h and provided that the relaxation stress at
100 h is not more than 3.50 percent of the initial stress as specified in 7.7.
7. TESTS
7.1 All test pieces of wire of sufficient length for the specified tests shall be
selected by the purchaser or his authorized representative either:
a) from the cuttings of lengths of wires or ends of coils of wires; or
b) if he so desires, from the coil or length of wire, after it has been
cut to the required or specified length and the test piece taken
from any part of it.

7.1.1 In neither case, the test piece shall be detached from the coil or
length or wire, except in the presence of the purchaser or his authorized
representative.

7.1.2 Before test pieces are selected, the manufacturer or supplier shall
furnish the purchaser or his authorized representative with copies of the
mill records giving the number of coils or bundles in each cast with sizes
as well as the identification marks whereby each coil or bundle of wire can
be identified.

7
IS :6003 - 1983

7.2 Test sarnples shall not be subjected to any form of heat treatment. Any
straightening which the test samples may require shall be done cold.

7.3 Tensile Test - The ultimate tensile strength shall be determined in


accordance with IS : 1521-1972*.

7.4 Test for Proof Stress - ‘Proof stress shall be determined in accord-
ance w*ith IS : 1521-1!)72*.

7.4.1 When stress at 1.0 percent extension under load method is to be


determined, an initial load corresponding to a stress of 196 N/mm% shall be
applied to the test piece and a sensitive extensometer then attached. The
dial of the extensometer shall be set to a reading equal to O*OOl mm/mm
of the gauge length to represent the extension due to the initial load.
The load shall be increased until the cxtensometer shows an extension
corresponding to 1 *O percent of the gauge length, when the load shall be
noted. The stress calculated for this load shall be not less than the value
specified for the 0.2 percent proof stress.
7.5 Reverse Bend Test - The test piece taken in accordance with 7.1
shall be capable of being bent in the following manner without showing
signs of fracture:
One end of the test sample shall be firmly gripped in a vice fitted
with radiuscd jaws. The free end of the wire shall be bent round the
appropriate r.ldius specified below through an angle of 90” and back
to the oi-iginal position; this constitutes one bend. Thereafter the test
sarrplc shall l)e bent through 90” in the opposite direction and back
through 90” and then through 90” in the reverse direction and back
through 90”, the \\-ireshall withstand 3 reverse bends without fracture.
The ,wirc shall bc tcstcd with the indentations facing the jaws. Wire
which has depth of indentation in excess of 3 percent of the nominal
wire diameter shall withstand 2 reverse bends without fracture.
Diameter of IVire Radius of Jaws
mm mm
5.00 15.0
4.00 12.5
3.00 10.0

7.6 Elongation After Fracture - The elongation after fracture shall be


determined in accordance with IS : 1521-1972*.
7.7 Test for Relaxation - If required by the purchaser, the manufac-
turer shall provide evidence from records of tests of similar wire that the
-
*Method for tensile testing of steel wire (jrst revision ).

8
i
IS :6003-1983

rekxation of load from an initial stress of 70 percent of the specified


minimum tensile strength conforms to that specified in 6.5. During the
whole period of test the temperature shall be maintained at 20 + 20C.
The initial load shall be applied in a period of 5 minutes and shall then be .
held constant for a further period of one minute. Thereafter no adjustment
of load shall be made, and load relaxation readings shall commence from
the end of the sixth minute. On no account shall the test specimen be
overstressed.

8. SAMPLING AND CRITERIA FOR CONFORMITY

8.1 Scale of Sampling


8.1.1 Lot – In any consignment, all the coils of wire of the same nominal
dimeter and manufactured at the same place under similar conditions of
production and storage shall be grouped together to constitute a lot.

8.1.2 The number of coils to be selected at random from each lot shall
depend upon the size of the lot and shall be in accordance with Table 1.

TABLE I SAMPLE SIZE

No. OF COILS IN TEE LOT No. OF COILS TO BE SELECTED

up to 25 3
26,, 65 4
66,, 180 5
181 ,, 300 7
301 and above 10

8.2 Number of Tests


8.2.1 All the coils, selected as in 8.1.2 shall be tested for chemkal com-
position ( see 3.1.1 ), nominal diameter ( see 5.1 ), tensile strength ( see 6.1 ),
proof stress ‘( see 6.2 ), ductility ( see 6.3 ) and elongation ( see 6.4 ).
8.2.1.1 From each coil one test specimenshallbe selectedfor all tests
except nominal diameters ( see 5.1 ) and tested in accordance with the
appropriate test method.

8.3 Criteria for Conformity


8.3.1 The lot shallbe consideredas conforming to the requirementsof
thk specificationif the conditionsspecifiedunder 8.3.2 to 8.3.4 are satisfied
for alf the characteristics.
8.3.2 chemical Composition, Diam-eter, Tensile Strength and
Proof Stress — For each of the characteristics, the mean and the range

9
f

IS : 6003 - 1983

calculated from the test results shall satisfy the appropriate conditions given
below:
a) ( Mean +0*6 Range ) shall be less than or equal to the maximum
specification limit,
b) ( Mean -0.6 Range ) shall be greater than or equal to the
minimum specification limit.
NOTE - The range is the difference between the maximum and the minimum
value of the test results.

8.3.3 Elongation - An case of test for elongation after fracture, every


sample tested shall satisfy the requirements of 6.4 and the percentage
elongation for none of the samples shall fall below the value specified
in 6.4.

8.3.4 Ductility - The number of defective test specimens ( those not


satisfying the requirements of the test ) shall not exceed the corresponding
permissible number given below:

AJo. of Specimens Permissible No. of Defective


Tested Test Specimens
3 0
4 0
5 1
7 1
10 2

9. DELIVERY, INSPECTION AND TESTING FACILITIES

9.1 Unless otherwise specified, general requirements relating to the supply


of mater+ inspection and testing shall conform to IS : 1387-1967*.

9.2 No material shall be despatched from the manufacturers’ or suppliers’


premises prior to its being certified by the purchaser or his authorized
representative as having fulfilled the tests and requirements laid down in
this standard except where the bundle or coil containing the wire is marked
with the ISI Certification Mark.

9.3 The purchaser or his authorized representative shall be at liberty to


inspect and verify the steel maker’s certificate of cast analysis at the premises
of the manufacturer or supplier; when the purchaser required an actual
analysis of finished material, this shall be made at a place agreed to bet-
ween the pu.rchaser and the manufacturer or supplier.

*General requirements for the supply of metallurgical materials (first rcnision).

10
Ls:f%o3-1983

9.4 1Manufacturer’s Certificate - In the case of wires which have not


been inspected at the manufacturer’s works, the manufacturer or supplier,
as the case may be, shall supply the purchaser or his authorized represent-
ative with certificate stating the process of manufacture and also the test
sheet signed by the manufacturer giving the result of each mechanical test
and the chemical composition, if required. Each test sheet shall indicate
the number or identification mark of the cast to which it applies, corres-
ponding to the number or identification mark to be found on the meterial.

9.5 When test for susceptibility to stress corrosion and relaxation are
required to be carried out, the cost of testing shall be borne by the purch-
aser.

9.6 Unless otherwise agreed to between the purchaser and the manufac-
turer, wire shall be supplied in coils of sufficiently large diameter to ensure
that the wire runs off straight and the purchaser may specify the diameter
of the coil, if he so desires.

9.7 Coils of about 1.5 m diameter without breaks, joints and welds are
generally recommended. The mass of the coil shall be as mutually agreed
to between the purchaser and the manufacturer or supplier. Each coil shall
have at least four tight ligatures.

10. IDENTIFICATION AND MARKINGS

10.1 The manufacturer or supplier shall have ingots, billets and wires, or
coils of wires marked in such a way that all finished wire can be traced to
the cast from which they were made. Every facility shall be given to the
purchaser or his authorized representative for tracing the wires to the cast
from which they were made.

10.1.1 Each bundle or coil containing the wires may also be suitably
marked with the IS1 Certification Mark in which case the concerned test
certificate shall also bear the Standard Mark.
NOTE- The use of the Standard Mark is governed by the provisions of the Bureau of
Indian Standards Act, 1986 and the Rules and Regulations made theretinder. The Standard
Mark on products covered by ad Indian Standard conveys the assurance that they have been
produced to comply with the requirements of that standard under a well defined system of
inspection, testing and quality control which is devised and supervised by BIS and operated
by the producer. Standard marked products are also continuously checked by BIS for
conformity to that standard as a further safeguard. Details of conditions under which a
licence for the use of the Standard Mark may be granted to manufacturers or producers may
be obtained from the Bureau of Indian Standards.

11
BUREAU OF INDIAN STANDARDS

Headquarters :
Manak Bhavan, 9 Bahadur Shah Zafar Marg. NEW DELHI 110002
Telephones : 331 01 31 Telegrams : Manaksanetha
331 13 75 (Common to all Offices)
Regional Offices : Telephone
Central : Manak Bhavan. 9. Bahadur Shah Zafar Matg, 331 01 31
NEW DELHI 110002 i 331 13 75
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t Western : Manakalaya, E9 MIDC. Marol. Andheri (East). 632 92 95
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Branch Offices :
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Printed at Dee Kav Printers. New Delhi. India


4
AMENDMENT NO. 1 JULY 1988

TO

IS:6003-1983 SPECIFICATION FOR INDENTED WIRE


FOR PRESTRESSED CONCRETE

(First Revision)

(Page 5. clause 3.2, first sentence) -


Substitute the following for the existing matter:

'The wire rods obtained from the rolling mill shall


be heat treated if required to make it suitable for
cold drawing and thereafter the diameter of the
wire rod shall be successively decreased to the
required diameter by cold drawing it through a
series of dies.'

(Page 8, clause 7.4) - Add the following at the


end:

'Klternatively, s,tress at 1.0 percent extension


under load method as specified in 7.4.1 may be
determined.'

(Page 9, clause 8.2.1.1, line 2) - Delete the


words 'except nominal diameters= 5.1)'.

(RSMDC 8)

prifltsd at b.rcly hinten. New bclhi, India


AMENDMENT NO. 2 DECEMBER 1993
TO
IS 6003 : 1983 SPECIFICATION FOR INDENTED WIRE
FOR PRESTRESSED CONCRETE
( First Revision )
(Page 4, clause 2.1 ) - Delete and renumber the subsequent clauses as 2.1
to 2.7.
(Page 5, clause 5.1.1 andNote ) -Add new clause 5.1.2 as follows:
‘5.1.2 Where the diameter measurements (taken in two directions at right angles
in the same plane) show an ovality of not more than half of the total diameter
tolerance, no checks on section by weighing shall be necessary. Where ovality is
more than half of the total diameter tolerance, check on section by weighing shall
be made. Nominal mass and tolerance on nominal mass of the finished wire shall
be as given below:

Nominal Diameter Nominal Mass Tolerance


mm g/m g/m
8.00 395 k-5.9
7.00 302 k4.3
5.00 154 k3.1
4.00 98.9 k2.0
3.00 55.5 +1.5
2.50 38.5 +1.25

( Page 7, clause 6.2 ) - Delete ‘Unless otherwise specified’ from the


beginning of this clause.

( Page 8, clause 7.7 ) - Delete ‘If required by the purchaser’ from the
beginning of the clause.
(Page 10, clause 8.3.4) -Rewrite as follows:

‘8.3.4 Ductility - In case one or more of the test pieces first selected fail to
pass this test, hvice the number of samples originally tested shall be selected for
testing. All the samples so tested shall satisfy the requirement of this test. Should
any of the test piece from these additional samples fail, the material represented
by the samples shall be considered as not having compiled with this standard.’
(Page 11, clause 9.4, line 6 ) - Delete ‘if required’.
(Page 11, clause 9.6 ) - Add the following para at the end:
‘It is necessary to protect the wires against damage and contamination during
transport and storage. The coils of wire shall be packed as agreed to between the
purchaser and the manufacturer.’

(CED54)
Reprography Unit, BIS, New Delhi. India

2
AMENDMENT NO. 3 MARCH 1997
TO
IS 6003 : 1983 SPECIFICATION FOR INDENTED
WIRE FOR PRESTRESSED CONCRETE
( Fi’rsl Revision )
( Page 4, chrrse 3.1.1, lines 2 and 3 ) - Substitute ‘0.040 percent’ for ‘0.05
percent’.

(CED54)

ReprographyUnit, BIS, New Delhi, India

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