Journal of Material Science and Mechanical Engineering (JMSME)

Print ISSN: 2393-9095; Online ISSN: 2393-9109; Volume 2, Number 8; April-June, 2015 pp. 57-62
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A Study on Effect of Preheating and Post Weld

Heat Treatment (PWHT) of Grade P91 Steel
Akhilesh Kumar Singh1, Tapas Debnath2, Vidyut Dey3 and Ram Naresh Rai4
1,2,3,4
Department of Production Engineering National Institute of Technology, Agartala Tripura (w) - 799046, India
E-mail: 1akhileshkr.singh@hotmail.com

cracking of weld[6]. Research attempts have been made to

Abstract—In the present study, bead-on-plate welds were carried understand and minimize its susceptibility to such cracking
out on P91 steel plates using Gas Tungsten Arc Welding (GTAW). regarding that Pre-heat (at 200⁰C) and Post Weld Heat
Experiment is carried out on three control input process parameters Treatment (at 760⁰C for 2 hrs.) is required to ensure that
(current, travel speed and gas flow rate) with pure argon gas,
desired hardness and microstructure are obtained. Heat
without any filler material using autogenous fusion arc
welding(GTAW) to investigate the effect of preheating and post weld treatment operations are necessary to avoid hydrogen retention
heat treatment (PWHT) on 6mm thick plate of grade P91 steel plates cracking problems in this extremely hardenable P91 steel
was used. The responses, weld bead geometry (in terms of bead material [7-8]. The present study shows that heat treatment is
width(BW), depth of penetration(DOP)), weld area(WA), and width not an optional operation in welding of A 387 Grade - P91
of Heat Affected Zone (HAZ) width have been measured with Adobe (plates). It is necessary as it improves the welding properties
Acrobat 9.0 Pro software. The measured weld quality in the form of as well as the microstructures of different weld bead zones.
weld bead geometry which played an important role in determining The study helps to understand and minimize its susceptibility
the input process parameters to analysis the weld structure and size to cracking after proper heat treatment operations. An
of weld bead geometry. It has been found that the pre-heat and post
autogenous (TIG) welding process on bead on plate welding
weld heat treatment effects the microstructure and micro-hardness of
welded specimen. was performed without the use of filler material.

Keywords: Preheat, PWHT, microstructure, micro-hardness. 2. EXPERIMENTS

1. INTRODUCTION Bead on plate welding experiment was performed on Grade P-

91 steel plates on 6 mm thick plate by Tungsten Inert Gas
Grade P91 steel, basically is a Creep Strength – Enhanced (TIG) welding. TIG welding process is generally used to
Ferritic Steel (CSEF) known as the modified 9Cr-1Mo-V, produce high quality weld joints of 9Cr-1Mo steel [9]. The
designated as P91 steel for Plate (A 387/A387M) its Standard chemical composition of Grade P-91 steel plate’s material is
Specification for Pressure Vessel Plates, Alloy Steel, shown in Table 1.
Chromium – Molybdenum [1]. Modified 9Cr-1Mo-V (P91)
steel is widely used in different high temperature components
of power- generating applications such as steam header, steam
pipes, Superheater, Pressure Vessel Plates, reheater and in
process vessels of chemical industries[2]. An advantage of
using P91steel is low thermal expansion, high thermal
conductivity, good stream corrosion resistance and excellent
creep resistance [3-4]. The modified 9Cr-1Mo-V steel plates
extremely hardenable material. However, welded P91 grade
steel components required proper application of heat treatment
because in power- generating industries P91 steels
components are used at a higher steam temperature more than
600⁰C and a steam pressure greater than 35 MPa[5].
Components are reported to show premature creep failure in
the temperature range 600- 650⁰C. Failures occur in the inter
critical heat affected zone (ICHAZ) and coarse grain region of Fig. 1: TIG welding experimental setup
HAZ (CGHAZ) of weld joints, generally known as Type IV
58 Akhilesh Kumar Singh, Tapas Debnath, Vidyut Dey and Ram Naresh Rai

Experiment is carried out on three control input process 3.1 Pre-Heat and PWHT Welding’s
parameters(i.e. current, travel speed and gas flow rate) is
shown in Table 2. For welding, the specimen P91 steel plate In Table (3-4) show the measured dimensions of weld bead
material was cut into size of 100mm x 50mm x 6mm by geometries and bar-graph is also shown in Fig. (3&4) to
abrasive cutter with blade of thickness 1.5 mm was used to cut analysis the weld bead geometry of Pre-Heat and PWHT
the specimens at 1500 rpm. welded dimensions. Fig.3 shows Pre-Heat before welding, the
specimen C2S2G2 as the heights dimensions at bead welds
Two types of welding have been performed on P91 steel plate. (BW), weld area (WA) and width of Heat Affected Zone
First - Before welding preheating. Second - after welding post (HAZ). When current increases penetration dimension is
weld heat treatment (PWHT). In both welding’s the torch decreases toward C1S1G1 to C3S3G3.
fixed and workpiece is controlled by travel-speed machine has
been fabricated to avoid human errors during welding which Fig.4 shows the PWHT after welding, in this welding we
shown in Fig. (1). observed that when current increases WB and WA dimensions
is increases toward C1S1G1 to C3S3G3 and the heights
After welding, the specimens were cut by abrasive cutter then penetration dimensions is found at specimen C2S2G2. In both
grinded. After that polished and etched, using 5% Nital the weld processes, it can be clearly seen from the Fig. (3 and
solution, to reveal the bead geometry on the cross section. The 4) width of the heat affected zones has approximately equal
etched specimens were then photographed using a digital dimensions observed at both the specimens C1S1G1 and
camera, shown in Fig. 2 and 3 which were later used for C2S2G2.
dimension measurement.
Table 1: The chemical composition of material used

Cr M V N2 C Si M P S Ni Al
% o % % % % n % % % %
% %
P91 8.8 0.9 0.2 0.0 0.0 0.3 0.4 0.0 0.0 0.1 0.0
Steel 1 7 4 46 93 2 4 18 07 5 15
Plate
(6 mm
Thickne
ss) (C1S1G1)

Table 2: The Control Input Process Parameters

Sample Welding Current Welding Gas flow rate

No. (A) Time (l/min)
(cm/min)
1 150 15 8
2 200 17.5 10
3 250 25 12

3. RESULTS AND DISCUSSION

To recognize the weld bead geometry, the welded specimens (C2S2G2)
were cut by abrasive cutter then grinded, polished and etched
to reveal the bead geometry on the cross section.
Photographed taken from a digital camera. To recognize the
digital camera pixel intensity and image capture distance of
specimens, we pasted the (1 cm) scale on the specimen to
measure accurate dimension. The responses, dimensions
measurement of weld bead geometry (in terms of bead width,
depth of penetration), weld area, and width of Heat Affected
Zone (HAZ) have been measured with the help of Adobe
Acrobat 9.0 Pro software. Measured data is shown in Table
(3& 4) and Bar-graph shown in Fig. (3&4)
(C3S3G3)
Fig. 2: Etched cross-section of pre-heat
welding showing bead geometry

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Print ISSN: 2393-9095; Online ISSN: 2393-9109; Volume 2, Number 8; April-June, 2015
A Study on Effect of Preheating and Post Weld Heat Treatment (PWHT) of Grade P91 Steel 59

(C1S1G1)

Fig. 3: Show the measured data of Pre-Heat Welding

Table 4: Measured Data of PWHT Welding

Measured Data of PWHT Welding
Sample Width
Width Penetration Area
Number HAZ
(cm) (cm) (cm2) (cm)
C1S1G1 0.469 0.220 0.076 0.097
C2S2G2 0.513 0.286 0.113 0.095
C3S3G3 0.715 0.237 0.119 0.042
(C2S2G2)

(C3S3G3)

Fig. 3: Etched cross-section PWHT welding

showing bead geometry Fig. 4: Show the measured data of PWHT Welding

Table 3: Measured Data of Pre-Heat Welding 3.2 Microstructures after TIG Welding

Measured Data Of Pre-Heat Welding The microstructures of weld bead geometry and Heat Affected
Sample Width Zone (HAZ) have been analysis by optical microscope (Lieca
Width Penetration Area Qwin software). The microstructures of Pre-Heat and PWHT
Number HAZ
(cm) (cm) (cm2) (cm) welding are shown in the Figures. (5-6).
C1S1G1 0.634 0.261 0.1164 0.118
C2S2G2 0.769 0.247 0.133 0.119
Fig.(5) shows the microstructure of Pre-Heat welding(200ᴼC)
C3S3G3 0.661 0.183 0.090 0.109 in which all the welds show ferrite as well as fresh-martensite
like structures observed in weld zone. The microstructure of
coarse grain zone, grain size is larger than the fine grain zone.
Fig. (6) Shows the overall microstructure of P91 steel in which
all the welds show at weld zone we observed delta-ferrite like
structure after PWHT (760ᴼC for 2hrs.). HAZ- including

Journal of Material Science and Mechanical Engineering (JMSME)

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60 Akhilesh Kumar Singh, Tapas Debnath, Vidyut Dey and Ram Naresh Rai

coarse grain zone and fine grain zone. The microstructure of

coarse grain zone shows martensite like structure [10-12].
The specific microstructure depends on the related thermal
profile generated by a particular welding condition [13].

(b)

(a)

(c)
Fig. 4: The microstructures of PWHT weld:

(b) (a) C1S1G1, (b) C2S2G2 and (c) C3S3G3

After performing the basic operation of welding image

measurement and microstructure the specimen is further used
for micro-hardness to analysis the mechanical properties of
welding parameter and process used.
3.3 Hardening Behaviour
Hardness is the property of a material to resist the plastic
deformation. For hardness measurement - specimen P91 steel
plate material was cut into size of 50mm x 5mm x 6mm by
abrasive cutter with blade then grinded, polished and etched,
(c) using 5% Nital, to reveal the bead geometry on the cross
Fig. 5: The microstructures of Pre-Heat weld: section. Hardness testing was carried out in a straight line 2
mm below and parallel to surface of the base plate with a
(a) C1S1G1, (b) C2S2G2 and (c) C3S3G3 constant load of 1 Kg and dwell time 10 sec. Reading were
taken 0.5 steps through the WZ, HAZ and the part of the base
material. Hardness testing was carried out according to ASTM
designation: E384 – 11, Standard Test Method for Knoop and
Vickers Hardness of Materials [14].
Fig. 7(a) shows hardness profiles across the entire Pre-heat
(200ᴼC) welded specimens. Hardness is taken from weld
centre line distances(mm). In pre-heat welding we observed
that hardness suddenly increases from weld zone toward
CGHAZ where all specimens have higher hardness value and
then decreases toward base metal. Fig. 7(b) shows hardness
profiles across the PWHT (760ᴼC for 2hrs.) weld. Hardness is
(a) higher at weld zone (WZ) region in all specimens and

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A Study on Effect of Preheating and Post Weld Heat Treatment (PWHT) of Grade P91 Steel 61

hardness decrease toward the FGHAZ and then slightly operations are necessary to avoid hydrogen retention cracking
increases toward base metal[15-17]. problems or we call Type IV cracking of weld [16]. The more
effect of heat treatments of P91 steel is investigated in a future
study.
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62 Akhilesh Kumar Singh, Tapas Debnath, Vidyut Dey and Ram Naresh Rai

[14] ASTM, Designation: E384 – 11, Standard Test Method for

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