NRCC 53261
NRCC 53261
NRCC 53261
ca/irc
NRCC-53261
September 2010
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Thresholds Identification and Field Validation of the
Performance Based Guidelines for the Selection of
Hot-Poured Crack Sealants
Shih-Hsien Yang
Project Engineer
Nichols Consulting Engineers, Chtd.
501 Canal Blvd.,Suite I, Richmond, CA 94804
e-mail: syang@nce.reno.nv.us
(Former graduate student at University of Illinois at Urbana-Champaign)
Imad L. Al-Qadi 1
Founders Professor of Engineering
Ilinois Center for Transportation, Director
University of Illinois at Urbana-Champaign
205 N Mathews MC-250, Urbana, IL 61801
e-mail: alqadi@illinois.edu
Jim McGraw
Chemical Lab Director
Minnesota Department of Transportation
1400 Gervais Ave
Maplewood, MN 55109
e-mail: James.McGraw@dot.state.mn.us
J-F. Masson
Institute for Research in Construction
National Research Council of Canada
1200 Montreal Road, Ottawa, ON, K1A 0R6, Canada.
E-mail: Jean-Francois.Masson@nrc-cnrc.gc.ca
Kevin M. McGhee
Senior Research Scientist
Virginia Transportation Research Council, VDOT
530 Edgemont Road, Charlottesville, VA 22903
E-mail: Kevin.McGhee@VDOT.Virginia.gov
1
Corresponding Author
1
ABSTRACT
Hot-poured bituminous crack sealing has been widely accepted as a routine preventative
maintenance practice, and with proper installation, it is expected to extend the pavement service
life three to five years. However, the current specifications for the selection of crack sealants
correlate poorly with field performance; hence, a set of new testing methods, which are based on
sealant rheological/ mechanical properties, were developed recently. Measuring the mechanical
properties of crack sealant at low temperatures is one of the criteria introduced as part of the
developed performance-based guidelines. The main purpose of this study was to identify and
validate the low temperature selection thresholds for the newly developed performance based
guideline for selecting hot-poured bituminous crack sealants. In this study, selection criteria for
crack sealant bending beam rheometer (CSBBR) and crack sealant direct tension tester (CSDTT)
tests are identified. Two performance parameters for CSBBR test are used for the selection
criteria: stiffness at 240s and Average Creep Rate (ACR). Both parameters were identified by
comparing laboratory testing results with known sealant field performance, obtained from a
long-term study in Canada. The selection criterion for the CSDTT test is extendibility, which is
based on field values reported in the literature. The recommended selection criteria were used to
predict the field performance of 12 sealants evaluated by the National Transportation Product
Evaluation Program (NTPEP). The results show good correlation between the proposed
selection thresholds and NTPEP field sealant performance.
2
INTRODUCTION
For a material to provide acceptable performance as a hot-poured bituminous-based crack
sealant, it must resist adhesion, degradation, and cohesion failures in the range of service of
temperature at which it is expected to be used. In addition, the material should be easily and
effectively installed, and able to resist degradation from the surrounding environment. Because
of their chemical complexity, crack sealant specifications have been developed around physical
property tests that are thought relevant to their performance. The current crack sealant
specification system, found in ASTM D5329 and AASHTO M173, focuses on utilizing simple
empirical tests such as cone penetration and softening point to measure the ability of the material
to resist cohesive failures. Although the viscoelastic behavior of crack sealants is too
complicated to be described by simple empirical parameters, the used consistency tests have
served well over the years for specifying crack sealants and to ensure the consistency of sealant
properties (1).
As a result of increasing traffic, axle loading, and tire pressure, a new range of highly-
modified crack sealants have been introduced that can have quite complex behavior compared to
traditional sealant materials. The implementation of the current specification system on these
new classes of crack sealant materials revealed that the used consistency tests do not adequately
describe the linear viscoelastic properties that are needed to relate physical properties to
performance, to relate sealant chemistry to performance, and to develop a performance-related
crack sealant specification system. In addition, results of these tests were found to correlate
poorly with field performance. While some sealants provided superior field performance, they
were ranked equally to low performance sealants. The poor prediction of sealant performance
using the current specification system has been widely reported in the literature (2, 3, 4). In
summary, characterization of hot-poured crack sealants using the current specification system
does not ensure adequate or reflect actual field performance. Hence, an improved sealant
specification and selection system is urgently needed.
The key to improving sealant durability is to develop effective performance guidelines
for selection and application of sealants. This study makes use of the well-established methods
and equipment originally developed during the five-year Strategic Highway Research Program
(SHRP) as part of the Performance Grade (PG) system for asphalt binders. Because the
equipment utilized in the PG system are already owned by various pavement and State
transportation agencies, it makes it an attractive and economical choice to be adopted in this
research project. However, because of the high flexibility of crack sealants and the large
deformation experienced under loading, it was found that the original bending beam rheometer
(BBR) and direct tension tester (DTT) are not suitable to test crack sealant material. Therefore,
in order to use the equipment developed by SHRP, some modifications were necessary to allow
for testing hot-poured sealants (5, 6).
In addition, a unique feature of the SuperPaveTM binder specification system is that the
specified criteria of fundamental rheological properties of asphalt binder remain constant, but the
temperature at which the criteria must be met changes for the various PG grades. The tests are
performed at temperatures that are encountered by in-service pavements. The similar idea of
establishing selection threshold for crack sealant was also adopted for crack sealant bending
beam rheometer (CSBBR) test which has a specified criterion over the various sealant service
temperatures. However, for crack sealant direct tensile tester (CSDTT) test, the selection criteria
3
are varied with various sealants in service temperatures. This is due to the various loading
mechanisms between sealant and asphalt binder in the field. Therefore, this paper presents the
sealant low temperature selection thresholds and preliminary validation of these selection
thresholds using CSBBR and CSDTT tests.
OBJECTIVES
The objective of this paper is to identify the selection criteria of hot-poured crack sealant at low
temperature using CSBBR and CSDTT tests. Two performance parameters for CSBBR test are
used for the selection criteria: stiffness at 240s and Average Creep Rate (ACR). Both parameters
were identified by comparing laboratory testing results with known sealant field performance
obtained from a long-term study in Canada (7). The selection criterion for the CSDTT test is
extendibility, which is based on field values reported in the literature. The recommended
selection criteria were used to predict the field performance of 12 sealants evaluated with the
National Transportation Product Evaluation Program (NTPEP). The sealants were installed in
Minneapolis and St. Paul, Minnesota.
SEALANT MATERIALS
Fifteen laboratory-tested sealants —designated as PP, BB, AD, WW, AE, NN, MM, UU, DD,
EE, VV, AB, QQ, YY, and ZZ— five Montreal field sealants—designated A, B, E, G, and J —
and 12 NTPEP field sealants with varying chemical compositions were evaluated. The
laboratory-tested sealants were obtained from various North American manufactures and were
used to investigate the mechanical behavior of crack sealant. The laboratory-tested sealants
represent a wide array of rheological behaviors, and thus, they are expected to perform in various
environments with a low-temperature range of -4°C to -40°C. Variations in the rheological
properties can be attributed to various factors, including the source of the origin crude, the
refining and modification process, and the content of polymer, filler, and additives. There is no
field performance data available for the 15 laboratory-tested sealants. The five Montreal field
sealants were installed in the early 1990s in Montreal, Canada; they have detail performance
records and used to establish the sealant selection criteria.
Twelve types of crack sealants produced by seven manufactures were used in the study.
Sealants were installed in the U.S. Highway 169, at Delaware Avenue, between Belle Plaine and
Jordan, southwest of Minneapolis and St. Paul, in Minnesota. The sealants were installed on
September 14, 2005. The pavement condition was rated as “good” at the time of construction.
Some transverse cracks existed, but there were few longitudinal cracks. All cracks were
prepared by cutting a reservoir for the sealant using a router. Sealant installation was completed
between 10:00 a.m. and 4:00 p.m. Ambient temperature ranged from 61 to 75 °F.
4
temperatures as low as -40°C. The development of this procedure is described in detail in a
supporting document (8). Two performance parameters were suggested for use in the
specification: stiffness at 240s and average creep rate (see Figure 1) [9].
50
30
20
10
0
QQ ZZ AB UU AE NN PP
Sealant
(a)
0.5 -4°C -10°C -16°C -22°C
-28°C -34°C -40°C
0.4
Average Rate of Creep
0.3
0.2
0.1
0
QQ ZZ AB UU AE NN PP
Sealant
(b)
FIGURE 1 (a) Stiffness at 240s and (b) Average creep rate at various testing temperatures
for various sealants
5
distinguishing between various sealant types. In addition, it is worth noting that several sealants
in Figure 2 show extendibility of 90% without failure. The DT device housed in most
laboratories can only extend the material up to 92%. Therefore, it was determined to conduct the
test only up to 90% of strain, even if the specimen does not fail.
90
80
50
40
30
20
10
0
DD MM WW NN AD PP BB
Sealant
6
PI = 100-(D+nP) (1)
where,
PI = sealant performance index;
D = percent de-bonded length of the sealant;
P = percent pull-out length; and
n = an integral that accounts for the effect of pull-out over de-bonding on performance
TABLE 1 (a) Montreal Sealant Standard Test Results; (b) Field Sealant Installations; (c)
Short- and Long-Term Sealant Performance (Failure Lengths, %) [7]
(a)
Penetration Flow Resilience Bond
Sealant (<90 dmm)*,
(<3 mm)* (>60%)* (3 cycles)*
†
A 86 0.5 57 No
B 68 0.5 64 Yes
E‡ 104 1 73 Yes
G 50 0.5 51 No
J 66 6 48 Yes
*ASTM D3405 requirements.
†1 dmm = 0.1 mm.
(b)
Temperature (°C) Air Temperature
Sealant at Start of Installation
Recommended Measured
(°C)
A 190-205 205 Overcast and -6
B 170-200 215 --
E 185-195 195 Overcast and 7
G 170-180 175 Overcast and 7
J 185-195 -- Overcast and 3
(c)
Before First Winter After First Winter After Four Years Performance
Sealant De- De- De- Index after
Pull-out Pull-out Pull-out
bonding bonding bonding Four Years
A 1 <1 12 9 11 14 33
B 5 <1 5 <1 22 1 74
E 1 <1 11 1 20 2 72
G 3 <1 24 3 36 14 8
J 1 <1 8 6 13 12 39
The n value was assigned as four in the Masson’s study (7). The suggested value was
based on the assumption of that a loss of one meter of sealant might allow the intrusion of water,
sand, and stone into the pavement, which could damage the pavement during its expansion and
7
contraction (12). This damage is more critical than de-bonding over the same length. A higher
PI value is indicative of better sealant performance. For example, the PI for sealant A was 33
and the performance was classified as “poor,” while sealant E had a PI of 72 and a performance
classification of “good.”
The five Montreal sealants were subsequently tested in the laboratory. According to the
LTTPBind, the low temperature PG of binder with 98% reliability in the region is -40°C, so all
sealants were tested at -34°C (6°C higher than the temperature grade). Sealants were tested at
four conditions: virgin (before installation), after accelerated weathering (vacuum oven aging),
after one, three, five, and nine years of field weathering. Figure 3 and Figure 4 present the
CSBBR and CSDTT test results for the five Montreal sealants.
200
150
Stiffness (MPa)
100
50
0
Virgin Oven Aged 1 yr W 9 yr W
Sealant A 21 17 42 74
Sealant B 22 25 44 28
Sealant E
Sealant G 126 120 148 176
Sealant J 602 521 115
(a)
0.4
Average Creep Rate
0.3
0.2
0.1
0
Virgin Oven Aged 1 yr W 9 yr W
Sealant A 0.30 0.33 0.29 0.28
Sealant B 0.31 0.28 0.29 0.34
Sealant E
Sealant G 0.23 0.19 0.21 0.20
Sealant J 0.16 0.16 0.28
(b)
FIGURE 3 (a) Stiffness at 240s and (b) Average creep rate of Montreal field sealants
8
25
Extendibility (%)
20
15
10
5
0
Virgin Oven Aged 1 yr W 9 yr W
Sealant A 11.3 23.1 9.5 2.0
Sealant B 21.2 92.7 2.7 16.5
Sealant E 93.0 94.4 92.5 93.5
Sealant G 0.4 0.5 0.5 0.3
Sealant J 0.7 0.3 0.4
9
recommended selection criteria were applied to the 15 laboratory-tested sealants, as shown in
Figure 5. Most of the sealants pass the threshold at two testing temperatures, with the exception
of the very stiff sealant, QQ.
50 2 C -4 C -10 C -16 C
45 -22 C -28 C -34 C -40 C
40
35
Stiffness (MPa)
30 S(-10 C)=85MPa
25
20
15
10
5
0
QQ
EE
ZZ
YY
AB
VV
UU
DD
NN
AD
BB
AE
WW
MM
PP
Sealant
(a)
2 C -4 C -10 C -16 C
0.5 -22 C -28 C -34 C -40 C
Average Rate of Creep
0.4
0.3
0.2
0.1
0
QQ
EE
ZZ
YY
AB
VV
UU
DD
NN
AD
BB
AE
WW
MM
PP
Sealant
(b)
FIGURE 5 (a) Stiffness at 240s and (b) Average creep rate of 15 laboratory-tested sealants
Researchers have shown that the maximum crack opening distance in the field can be as
high as 90% of the original crack width (13, 14, 15). The factors that affect crack opening
include pavement type, pavement location, crack configurations, and, most importantly,
pavement temperature. A pavement crack in the northern region of the North America is
generally subjected to larger crack opening distance. On the other hand, the pavement in the
southern region is generally subjected to only a few days of subzero temperature. Given these
environmental differences, the expert group suggested the selection criteria of the sealants based
on in-service temperature and corresponding extendibility, as shown in Table 2. After the
10
proposed selection thresholds were applied to the 15 laboratory-tested sealants (Figure 6), only
three sealants did not pass the criterion under the testing conditions.
70
-28 C Grade
Extendibility(%)
60
50 -22 C Grade
40
-16 C Grade
30
20 -10 C Grade
10
-4 C Grade
0
QQ EE ZZ YY AB VV UU DD AE MMWWNN AD PP BB
Sealant
FIGURE 6 Extendibility of 15 laboratory-tested sealants
11
Adhesion and cohesion failures were determined through visual inspection. The percent
length of adhesion/cohesion/infiltration is used to evaluate water infiltration. The percentage of
cracks that would allow water infiltration, measured as the percentage of the overall crack length
where water could bypass the sealant and enter the crack either through complete adhesion or
cohesion failure, was determined by the following equation:
Lf
%L = (2)
Ltotal
where,
%L = Percent length of the crack allowing water infiltration;
Lf = Total length of the crack sealant field evaluation section allowing the Infiltration of
water (inches);
Ltotal = Total length of the crack sealant field evaluation section (inches).
12
According to the ASTM specifications, three sealants were predicted to pass (3405, D-
3405, and Beram 195) and nine sealants were predicted to fail. If one compares the ASTM
specification prediction to the field performance survey, only three predictions were correct
(Meadows 3405, Roadsaver 515MN, and Beram 3060LM). On the other hand, using the
proposed test corresponding parameters, their thresholds correlate well with sealant field
performance. It has to be noted that the results are based on sealants installed at one climatic
region. To further validate the proposed tests and the selection thresholds, performance data of
sealants installed at various climatic regions are needed.
13
TABLE 4 Laboratory Test Results of NTPEP Sealants
(a)
Standard Crack Sealant Performance Grade
S 240 ACR
Criteria Result
<25 MPa >0.31mm/mm/s >85%
Temp (oC) -34 -34 -34
Deery 101ELT 5 0.44 >90 Pass
Deery 3723 7 0.45 >90 Pass
Meadows 3405-M 6 0.38 >85 Pass
Meadows 3405 23 0.37 >85 Pass
Roadsaver 522 6 0.4 -- Pass
Roadsaver 515MN 13 0.43 >85 Pass
Dura-Fill 3405 12 0.39 >85 Pass
Dura-Fill 3725 8 0.34 -- Pass
Right Pointe D-3405 17 0.38 26 Fail
Beram 195 16 0.33 >85 Pass
Beram 3060 LM 13 0.37 2.47 Fail
Elastoflex 63LM 26 0.33 2.36 Fail
(b)
Standard ASTM D6609 Type II
Cone Penetration Flow Resilience Bond
Criteria Result
(<90 dmm)*, † (<3 mm)* (>60%)* (3 cycles)*
Temp (C) 25°C 60°C 25°C -29°C
Deery 101ELT 103 2 55 P Fail
Deery 3723 87 3 58 P Fail
Meadows 3405-M 131 1 59 P Fail
Meadows 3405 86 0 62 P Pass
Roadsaver 522 90 5 49 P Fail
Roadsaver 515MN 64 2 52 P Fail
Dura-Fill 3405 79 2 57 P Fail
Dura-Fill 3725 109 0 52 P Fail
Right Pointe D-3405 73 0 73 P Pass
Beram 195 76 0 60 P Pass
Beram 3060 LM 112 1 47 P Fail
Elastoflex 63LM 103 0 56 P Fail
14
shows good correlation between low temperature performance grade sealant specification and
field performance. This study clearly shows the validity of the proposed tests and selection
criteria for hot-poured crack sealants at low temperature.
ACKNOWLEDGEMENTS
This study is based on work supported by the Federal Highway Administration and the U.S.–
Canadian Crack Sealant Consortium under pool fund award # TPF5 (045). Virginia serves as the
leading state; the Virginia Transportation Research Council of the Virginia Department of
Transportation managed the project. The contribution of the participating states, industries, and
provinces is greatly appreciated. The contents of this paper reflect the views of the authors, who
are responsible for the facts and the accuracy of the data presented herein. The contents do not
necessarily reflect the official views or policies of the pool fund-participating departments of
transportation or the Federal Highway Administration. This paper does not constitute a standard,
specification, or regulation. Special thanks are extended to Jim McGraw and MNDOT for
providing field performance survey of NTPEP sealants.
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