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    LAB READINESS-LEACHING v2

    Uploaded by

    Jabin Sta. Teresa
    This experiment compares single-stage, crosscurrent, and countercurrent extraction methods for leaching NaCl from a sand mixture using water. It aims to calculate extraction efficiencies and determine advantages and disadvantages of multistage extraction vs single stage. The experiment involves preparing NaCl-sand mixtures in beakers, performing single-stage, crosscurrent and countercurrent extractions using varying water volumes, and generating a density-concentration plot to analyze results. Safety hazards include risks of silicosis from sand and injury from breaking glassware.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd

    LAB READINESS-LEACHING v2

    Uploaded by

    Jabin Sta. Teresa
    37 views7 pages
    This experiment compares single-stage, crosscurrent, and countercurrent extraction methods for leaching NaCl from a sand mixture using water. It aims to calculate extraction efficiencies and determine advantages and disadvantages of multistage extraction vs single stage. The experiment involves preparing NaCl-sand mixtures in beakers, performing single-stage, crosscurrent and countercurrent extractions using varying water volumes, and generating a density-concentration plot to analyze results. Safety hazards include risks of silicosis from sand and injury from breaking glassware.

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    LAB READINESS-LEACHING v2.docx

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    This experiment compares single-stage, crosscurrent, and countercurrent extraction methods for leaching NaCl from a sand mixture using water. It aims to calculate extraction efficiencies and determine advantages and disadvantages of multistage extraction vs single stage. The experiment involves preparing NaCl-sand mixtures in beakers, performing single-stage, crosscurrent and countercurrent extractions using varying water volumes, and generating a density-concentration plot to analyze results. Safety hazards include risks of silicosis from sand and injury from breaking glassware.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    37 views7 pages

    LAB READINESS-LEACHING v2

    Uploaded by

    Jabin Sta. Teresa
    This experiment compares single-stage, crosscurrent, and countercurrent extraction methods for leaching NaCl from a sand mixture using water. It aims to calculate extraction efficiencies and determine advantages and disadvantages of multistage extraction vs single stage. The experiment involves preparing NaCl-sand mixtures in beakers, performing single-stage, crosscurrent and countercurrent extractions using varying water volumes, and generating a density-concentration plot to analyze results. Safety hazards include risks of silicosis from sand and injury from breaking glassware.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 7

    Experiment Title: Batch Leaching of NaCl-Sand Mixture with Water

    as Solvent

    Objectives:

    • To compare single-stage, crosscurrent, and countercurrent beaker-scale extraction operation


    • To calculate single-stage, crosscurrent and countercurrent extraction efficiencies
    • To determine the advantages and disadvantages of multistage extraction
    • To compare single stage and multistage extraction

    Equipment and Materials


    • Lab Scale
    • Glass rods
    • Beakers
    • Westpal Balance
    • Salt
    • Sand

    Reagent Computation

    A. Construction of Density-Concentration Plot for NaCl solution

    1. Make 0, 4, 8, 12, 16, 20 and 25% (by weight of NaCl solution

    Basis: 20g of H2O per NaCl concentration = 20g of Sand per 100-ml Beaker
    B. Fresh Feed Preparation

    1. Prepare 150g of Sand per 1L Beaker. Make 12 samples with equal amount of
    sand label from (I- XII)

    2. Amount of salt is unknown (x) for each sample

    3. Pour 150ml of water in each Beaker

    C. Single-Stage Extraction Operation


    1. Add the following amount to each specified sample

    Beaker I – 150 ml

    Beaker II – 300ml

    Beaker III – 600ml

    D. Multi-Stage Crosscurrent Extraction Operation

    1. Add 600 ml of H2O to the following container

    Beaker IV – 2 portions of 300 ml

    Beaker V - 3 portions of 200 ml

    Beaker VI - 4 portions of 150ml

    E. Steady-State Multi-Stage Countercurrent Extraction Operation

    1. Add 600ml of H2O to each beaker from Beaker VII to Beaker X and then decant
    600ml of solution per Beaker. Label as (Decant-Beaker No.)
    Graphical Presentation of Procedures:
    Safety Hazards:

    ● Sand can cause silicosis, lung cancer, and breathing problems when handled
    improperly.
    ● Glasswares are not that strong, that can break when applied too much force on it, that
    may cause shards to scatter and may injure other students.
    ● Handling the Westphal balance, not applying too much force on one side, for it may
    break.

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