Manuals/700-0099-F Jerome J405 Users Manual
Manuals/700-0099-F Jerome J405 Users Manual
Manuals/700-0099-F Jerome J405 Users Manual
OPERATION MANUAL
July 2008
(800) 528-7411
(602) 470-1414
Fax (480) 804-0656
http://www.azic.com
email:
azi@azic.com - General
intl@azic.com - International
support@azic.com - Customer Support
700-0099-F
JEROME J405
Mercury Vapor Analyzer
Operation Manual
This manual contains valuable information and material developed by Arizona Instrument LLC
for use with the Jerome J405 Mercury Vapor Analyzer. No part of this manual can be reproduced
or transmitted in any form or by any means, electronic, mechanical or otherwise. This includes
photocopying and recording or in connection with any information storage or retrieval system
without the express written permission of Arizona Instrument LLC.
This manual contains details that will optimize the results and the life of your instrument. Read
and refer to the manual for complete details on operation, maintenance and troubleshooting,
special voltage inputs and data output.
The Jerome J405 is easy to operate and ready for use upon receipt from the factory.
Remove the instrument from the packing material.
The included AC adapter power supply can utilize 110V or 220V AC power, and it is not
necessary to manually select the input voltage.
The J405 contains an auto-resetting fuse that does not require care, maintenance or
replacement by the user.
AZI Customer Service 800-528-7411 or 602-470-1414 Page 5 of 60
Perform a sensor regeneration by following these steps:
¾ Connect the line cord/AC adapter power supply between the connector on the back of the
J405 and an AC power outlet or connect the external battery pack to the back of the J405.
¾ If the instrument is not already turned on, press the I/O power button to turn it on.
¾ 3UHVVWKH5,*+7DUURZEXWWRQŹWRHQWHUWKHPDLQPHQX
¾ 3UHVVWKH'2:1DUURZEXWWRQźWRPRYHWKHFXUVRUWRRegen.
¾ 3UHVVWKH5,*+7DUURZEXWWRQŹWRVHOHFWRegen from the menu.
¾ Press the ENTER/START button on the keypad to select Regen Now from the Regen
menu.
7KHLQVWUXPHQWZLOOUHVSRQGZLWK³3HUIRUP5HJHQ8VLQJ(;7(51$/32:(5"´
Press ENTER/START to proceed or ESC to exit.
7KHLQVWUXPHQWGLVSOD\ZLOOZDUQ³'R1RW'LVFRQQHFW([WHUQDO3RZHUZKLOH+HDWLQJ´
Press ENTER/START to proceed or ESC to exit.
The instrument will now begin a 45-minute regeneration cycle, indicated by
Regeneration in Progress on the display. Do not interrupt this cycle. For a complete
description of this process, see page 20.
,IDQ\HUURUPHVVDJHDSSHDUVRQWKHGLVSOD\VHHWKH³7URXEOHVKRRWLQJ´VHFWLRQ
beginning on page 35.
Ensure the instrument has been powered on for at least five (5) minutes prior to sampling.
The instrument is now ready to sample.
Press the SAMPLE BUTTON at the end
of the handle of the J405 to start a
12 second sampling cycle.
When the instrument measures mercury
vDSRUWKHȝJP3 display will be
replaced with a value.
To ensure the input to the instrument
contains no mercury vapor or
mercaptans, use a Zero Air Filter (AZI P/N Z2600 3905). The Zero Air Filter cleans the air
sample and should produce sample readings of 0.00 ȝg/m3. Therefore, use the filter to:
¾ Equilibrate the instrument to temperatures that are higher or lower than the instrument.
Sample every 15 seconds with the ILOWHULQVWDOOHGXQWLOWKHUHDGLQJLVȝJP3.
¾ Identify contamination within the unit.
¾ Confirm the presence of mercury vapor when readings are elevated. Install the filter and
verify that the readings decrease with the filter installed.
The instrument is designed for ambient air monitoring.
WARNING
DO NOT allow the probe or the LQVWUXPHQW¶VLQWDNHWREHH[SRVHGWRany liquid.
DO NOT obstruct the intake or exhaust ports of the J405, as this could cause errors
in readings and damage to the flow control system.
The instrument is not explosion proof.
Perform sensor regeneration beforHHDFKGD\¶VXVH
3HUIRUPDQRWKHUVHQVRUUHJHQHUDWLRQDIWHUHDFKGD\¶VXVH
Perform sensor regeneration after 30 days of storage or inactivity.
Call AZI Customer Service at (800) 528-7411 or (602) 470-1414 if you have any questions. If
you prefer, you may send e-mail to support@azic.com.
The Jerome J405 Mercury Vapor Analyzer is an ambient air analyzer with a range of 0.5 to 999
micrograms of mercury vapor per cubic meter (µg/m3 Hg).
CAUTION:
The Jerome J405 is for gaseous vapor use only.
DO NOT allow the probe or the instrument's intake
to be exposed to any liquid, dust
or other foreign material.
The J405 is designed to be easy to operate for quick and accurate analysis of mercury vapor
levels. It has few maintenance requirements. However, please take a moment to read this manual
before attempting operation. If you have any questions about your application or operation,
please call AZI Customer Service at (800) 528-7411 or (602) 470-1414 or e-mail
support@azic.com for assistance.
J405 Features
The heart of the J405 is the well-proven gold film sensing technology. A thin gold film, in the
presence of mercury vapor, undergoes an increase in electrical resistance proportional to the mass
of mercury vapor in the sample.
When the SAMPLE button is pressed, an internal pump pulls ambient air through a scrubber filter
(AZI P/N: 600-0262) and into the flow system.
After 2 seconds, the sample solenoid bypass opens, closing off the scrubber filter from the flow
system.
The sample air passes through the AG filter (AZI P/N: 600-0293), an acidic gas filter that
removes any acidic gases that interfere with the sensor's response to mercury. Then the sample
air is drawn over the gold film sensor. The sensor adsorbs the mercury vapor. Nine seconds after
starting, the sample solenoid bypass closes and the remainder of the sample is drawn through the
scrubber filter and the flow system. The instrument determines the amount of mercury adsorbed
and displays the measured mercury concentration on the digital meter in micrograms per cubic
meter (µg/m3) or milligrams per cubic meter (mg/m3) of mercury.
During the sample mode cycle, a sensor saturation meter on the LCD represents the percentage of
sensor saturation, or adsorbed mercury collected on the gold film. With use, the sensor becomes
saturated and needs to be cleaned. This is accomplished by a manually activated 45-minute
sensor regeneration cycle, which removes the mercury from the sensor. The solenoid bypass
closes during the sensor regeneration cycle, causing the air to pass through the scrubber filter,
providing clean air for the regeneration process. The closed loop film heat cycle ensures the
sensor is cleaned to original values. The mercury released during regeneration is absorbed by the
IORZV\VWHP¶VILQDOVFUXEEHUILOWHU$=,31=600 3930) to prevent any external contamination
from the desorbed mercury. The 45-minute regeneration process includes a cool-down phase, so
the instrument is ready for use as soon as the regeneration process finishes.
The Zero Air Filter (AZI P/N Z2600 3905) removes mercury vapor, mercaptans, and hydrogen
sulfide IURPWKHDLUVDPSOH5HDGLQJVZLWKWKHILOWHULQVWDOOHGVKRXOGEHQHDUȝJP3. For
maximum accuracy, wait 15 seconds between samples to allow the sensor to restabilize.
Because air that is cooler than the instrument will cause low readings and warmer air will cause
higher readings, the Zero Air Filter should be used to equilibrate the unit to ambient air. Repeated
sampling with clean air will not cause saturation of the gold film sensor but will equalize
temperatures faster to allow accurate analysis to begin sooner. For maximum accuracy, wait 15
seconds between samples to allow the sensor to restabilize.
The Zero Air Filter can also be used to identify contamination within the instrument. If the
UHDGLQJVGRQRWUHGXFHWRQHDUȝJP3 with the filter installed, contamination should be
VXVSHFWHG,IWKHUHDGLQJVGRGURSWRQHDUȝJP3 with the filter installed but elevate with the
filter removed, the presence of mercury vapor at the sampled location is confirmed. Again, for
maximum accuracy, wait 15 seconds between samples to allow the sensor to restabilize.
The Zero Air Filter should be inserted into the intake of the instrument when running the
instrument Warm-up. See Warm-up in the section REGEN menu on page 15 for more
information.
For more information on the use of the Zero Air Filter, contact customer service at
1-800-528-7411 or 602-470-1414.
The J405 Main Screen is depicted below, followed by explanations of the labeled items.
SYSTEM TIME ± As set in the SYSTEM menu. (See SYSTEM menu on page 17 for more
information).
BATTERY ± Indicates current charge level and charging status (See Charging Internal
Batteries on page 25)
SOUND ICON ± Indicates if the audible alarm is turned on or muted, as set in the SYSTEM
menu. (See SYSTEM menu).
SYSTEM DATE ± As set in the SYSTEM menu. (See SYSTEM menu).
The above-labeled connections are available from the back panel of the J405. If the USB option
has not been activated, the USB ports will not be present. Contact your AZI Sales Representative
for information on the USB option.
POWER CONNECTOR ± Connect the supplied AC power adapter, the optional external battery
pack (AZI P/N: 990-0214), or the optional car accessory jack (AZI P/N: 200-0170) here to
provide power to the instrument or to recharge the battery.
86%7<3(³$´32576 ± 7KH86%7\SH³$´SRUWVDUHXVHGWRFRQQHFWD86%SULQWHURU86%
memory drive for printing or saving sample data. The two ports are identical, and either can be
used. For more information, see DATA menu on page 16.
86%7<3(³%´3257 ± 7KH86%7\SH³%´SRUWLVXVHGWRFRQQHFWWKH-GLUHFWO\WRWKH
USB port of a computer, using the included USB A to B cable (AZI P/N: 200-0165). For more
information see DATA menu on page 16.
DB25F CONNECTOR ± There are multiple specialized uses for the DB25F connector. See
Instrument I/O Interface on page 27 for more information.
EXHAUST PORT ± After sampling, the sampled air is cleaned of any mercury and expelled
from the exhaust port on the back of the J405.
SAMPLE MODE
The Sample Mode setting provides the choice between auto-sampling and manual sampling. For
normal use, use manual sampling, which is the instrument default setting. If auto-sampling is
selected, the instrument will automatically sample at the interval set in SET SAMPLE
INTERVAL (below) without monitoring or attendance by the user. 8VHWKHŸDQGźDUURZVWR
toggle between Manual and Auto, and use ENTER/START to save the selection. Use the ESC
key to exit without saving changes. If auto-sampling is selected, the word Auto will appear below
WKHV\VWHPGDWHRQWKHLQVWUXPHQW¶VPDLQVFUHHQDQGZKHQWKHVDPSOHEutton is pressed, the unit
will start auto-sampling.
UNITS
Sample results can be displayed in micrograms per cubic meter (µg/m3) or milligrams per cubic
meter (mg/m3). To change the displayed units, select UNITS from the SAMPLE menu. Use the
ŸDQGźDUURZVWRWRJJOHWKHVHOHFWLRQDQGSUHVVENTER/START to save the selection. Use the
ESC key to exit without saving changes. The default selection is µg/m3, and µg/m3 is used
throughout this manual for consistency. The relationship between µg/m3 and mg/m3 is as follows:
If auto-sampling is being used (as set in SAMPLE MODE above), the sample interval
determines how often the J405 will automatically take samples. 8VHWKHŸDQGźDUURZNH\VWR
scroll through the available sample intervals of 1, 2, 5, 10, 15, 30, 45, 60, 90 and 120 minutes, and
use ENTER/START to save the selected interval. Use the ESC key to exit without saving
changes.
Up to 80 unique location presets are available using the J405. This feature is useful if sampling is
done in multiple locations and there is a need to record which readings came from which
ORFDWLRQV8VHWKHŸDQGźDUURZVWRVFUROOWKURXJKWKHOLVWRISUHVHWs until the location to be
edited is highlighted. Press ENTER/START to begin editing the name of the selected location.
8VHWKHŸDQGźDUURZVWRVFUROOWKURXJKWKHDYDLODEOHDOSKDQXPHULFFKDUDFWHUVDQGSXQFWXDWLRQ
When the desired character is displayedXVHWKHŹDUURZWRPRYHWRWKHQH[WFKDUDFWHUILHOG,ID
PLVWDNHLVPDGHWKHŻDUURZFDQEHXVHGWRUHWXUQWRWKHSUHYLRXVFKDUDFWHU:KHQWKHORFDWLRQ
has been named as desired, press ENTER/START to save the location name, and return to the
list of locations. To select an existing location from the list for the samples to be taken, use the
ŸDQGźDUURZVWRVFUROOWRWKHGHVLUHGORFDWLRQDQGSUHVVENTER/START twice. Note the
asterisk (*) located to the left of the currently selected location. The selected location name will
be stored with the sample data for all samples taken until a different location is selected instead.
Use ESC to return to the sample menu. See Retrieving Data on page 26 for more info.
Highlight SURVEY MODE in the SAMPLE menu and press ENTER/START to begin
immediate sampling in survey mode. In survey mode, after an initial two-second pause to purge
the flow system, the J405 will sample continuously. For complete information on survey mode,
see Survey Mode on page 22.
REGEN menu
The sensor saturation meter on the main screen (to the right of s. sat) indicates the current level of
saturation of the sensor with mercury.
When the sensor becomes saturated with mercury, as indicated by the sensor saturation meter, a
regeneration (REGEN) must be performed on the sensor to release the accumulated mercury,
before additional samples can be taken. See Sensor Regeneration on page 20 for more
information on the REGEN procedure.
REGEN NOW
Plug the line cord/AC adapter power supply or the external battery pack into the back of the
instrument before starting a regeneration. Highlighting REGEN NOW and pressing
ENTER/START will start the sensor regeneration process. Press ENTER/START again on the
next screen to confirm your choice, and press ENTER/START again after reading the warning
that appears. The regeneration will now begin. Do not disconnect external power during the
regeneration.
WARMUP
To ensure maximum accuracy when sampling at cleanup levels less than 3 µg/m3, the J405 must
be warmed up with the Zero Air Filter in the intake, at the location to be sampled. To run the
warm-up, insert the Zero Air Filter in the intake, highlight WARMUP and press
ENTER/START. While warming up, the pump will run and the J405 will display a 5-minute
countdown. When the warm-up finishes, remove the Zero Air Filter and begin normal sampling.
If the J405 is idle for more than 20 minutes, another warm-up is required to maintain maximum
accuracy at these low levels.
AZI Customer Service 800-528-7411 or 602-470-1414 Page 15 of 60
SET INTERVAL
If auto-sampling is being used (as set in SAMPLE MODE above), the J405 can be configured to
automatically perform sensor regenerations aWDSUHGHWHUPLQHGLQWHUYDO8VHWKHŸDQGźDUURZV
to scroll through the available intervals of 6, 12, 24 and 48 hours and Saturation, and press
ENTER/START to save the selected interval. The J405 will now automatically perform a
REGEN every 6, 12, 24, or 48 hours starting at the time set in SET HOUR below or when the
sensor is saturated, as selected. Use ESC to exit without saving.
SET HOUR
NOTE: If the sensor is saturated and a regeneration cycle is performed and completed before the
set hour, the instrument will perform another regeneration at the set hour. However, if the
regeneration cycle does not complete prior to the set hour, the regeneration at the set hour will be
skipped.
DATA menu
Sample data can be stored within the instrument, up to a maximum of twenty thousand (20,000)
data points. Data can be retrieved from the instrument in one of three ways:
1. SEND TO PC
2. SAVE TO USB MEMORY DRIVE
3. PRINT DIRECTLY TO AN AZI APPROVED PRINTER (AZI P/N: Y990-0098)
The presence of the USB icon on the main screen indicates that the USB ports are functioning
properly. The USB icon will flash during data transmission. See J405 Main Screen Display on
page 11 for the location of the USB icon. The data is stored in non-volatile memory and will not
be affected if the battery is changed or disconnected.
SEND TO PC
Before using SEND TO PC, the USB driver must be installed on the target PC, and
HyperTerminal must be configured on the target PC. The USB driver is on the CD with this
operations manual and on the AZI website at www.azic.com. See APPENDIX A ±
USB/HYPERTERMINAL SETUP on page 43 for detailed instructions on installing the USB
driver, configuring HyperTerminal, and downloading data from the J405. Once the target PC has
been configured, connect the included USB A to B cable (AZI P/N: 200-0165) between the USB
7<3(³%´3257RQWKHEDFNSDQHORIWKH-DQGWKH86%3257RIWKHWDUJHWFRPSXWHUDQG
launch HyperTerminal. On the J405, with SEND TO PC highlighted, press ENTER/START,
and all of the stored data on the J405 will be transmitted to the target computer as a comma-
delimited text file. See Retrieving Data on page 26 for more information.
Before selecting SAVE TO USB DRIVE, connect the target USB memory drive to either USB
7<3(³$´3257RQWKHEDFNSDQHORIWKH-:KHQENTER/START is pressed, all of the
stored data on the J405 will be transmitted to the target drive as a comma-delimited text file. See
Retrieving Data on page 26 for more information.
NOTE: The J405 is NOT compatible with USB memory drives that have the U3 program
pre-installed. Do not use USB memory drives that have the U3 program with the J405.
PRINT DATA
Before selecting PRINT DATA, connect an AZI printer (AZI P/N: Y990-0098) to either USB
7<3(³$´3257RQWKHEDFNSDQHORIWKH-XVLQJWKHFDEOHVXSSOLHGZLWKWKHSULQWHr. When
ENTER/START is pressed, all of the stored data on the J405 will be printed on the attached
printer. See Retrieving Data on page 26 for more information.
The J405 can store up to 20,000 data points. Selecting VIEW MEMORY USAGE will display
what percentage of the data storage area is in use. Once the data memory is full, no additional
data can be stored until the data on the instrument is deleted. If the memory is full, the unit will
continue to perform as expected, but it will indicate that the memory is full and no sample data
will be retained. The storage area can be cleared using DELETE DATA as described below.
DELETE DATA
Selecting DELETE DATA will delete all sample data stored on the J405. Prior to deletion, the
J405 will prompt the user for confirmation as a precaution.
SYSTEM menu
When the SYSTEM menu is selected from the Main Menu, the J405 will prompt for the
paVVZRUG,QSXWWKHSDVVZRUGXVLQJŸDQGźWRFKDQJHWKHDOSKDQXPHULFFKDUDFWHUDQGŹDQG
ŻWRPRYHEHWZHHQFKDUDFWHUV3UHVVENTER/START to proceed after entering the password.
When the correct password is entered, the J405 will offer the option to change the password by
pressing the A key or to proceed to the SYSTEM menu by pressing ENTER/START. The
SYSTEM menu will then remain unlocked until the instrument is powered off and back on.
When sampling, if the mercury level exceeds the selected alarm level, the J405 will issue an
audible alarm and the display will read ALARM as well. Individual high and low alarm levels
can be set using this menu option8VHWKHŸDQGźDUURZNH\VWRFKDQJHWKHYDOXHRIWKH
EOLQNLQJILHOGDQGWKHŹDUURZWRPRYHWRWKHQH[WFKDUDFWHULQWKHDODUPOHYHOVHWWLQJ8VHWKH
A and B buttons to switch between the high and low alarm settings. Once the alarm level has
been set, press ENTER/START to select the highlighted alarm level as the current alarm level to
be used. Upon returning to the SET ALARM LEVELS screen, there will be asterisk next to the
currently selected alarm level (either high or low). It is recommended to set the alarm level
KLJKHUWKDQȝJP3. The alarm can be muted using AUDIBLE ALARM ON/OFF in the
SYSTEM menu.
DISPLAY MODE
Use VIEW SENSOR STATS to display the current saturation level of the sensor, the number of
regenerations performed on the sensor, and the total number of samples read by the sensor. Press
any key to exit the screen when finished.
8VHWKHŸDQGźDUURZNH\VWRFKDQJHWKHKLJKOLJKWHGILHOGDQGWKHŻDQGŹDUURZNH\VWR
move between characters within the day or year fields. Use the A and B keys to move between
the day, month, and year fields. Press ENTER/START to save the system date or ESC to exit
without saving.
AZI Customer Service 800-528-7411 or 602-470-1414 Page 18 of 60
RUN DIAGNOSTICS
Selecting RUN DIAGNOSTICS will start the J405¶s self-diagnostic procedure. As the
instrument proceeds through each diagnostic check, follow the on-screen prompts, and the
instrument will display the specific check being performed and the pass/fail result of the check. If
the check is not applicable to the current configuration of the instrument, the result field will be
blank instead of indicating pass or fail.
After viewing each result, press any key (except I/O or ESC) to move to the next diagnostic
check. (I/O should not be used during the diagnostics because I/O will power off the
instrument and ESC should only be used when specifically indicated by the instrument.)
When testing the keypad, follow the on-screen prompts to press each of the keys in turn. The
J405 will not indicate a pass/fail for this test. Instead, if all of the keys work and the
instrument proceeds to the next diagnostic test, the keypad diagnostic has passed.
When testing 80V power, press ENTER/START to pass the test and proceed to the next test.
Pressing ESC will stop the test and return a Fail.
If the 4-20mA output function of the J405 is not in use, press ENTER/START to skip through
the 4, 8, 12, 16 and 20mA checks in the diagnostic routine. If the 4-20mA output is in use, the
diagnostics can be used to verify proper operation. Refer to 4-20mA Output on page 27 for
more information.
After the last diagnostic result has beeQGLVSOD\HGWKHXQLWZLOOGLVSOD\³'RQH´DQGSUHVVLQJDQ\
key will return to the main screen of the J405.
Daily Operations
Before each day's use of the Jerome J405, perform the following steps to verify proper instrument
operation:
Press the power I/O button.
¾ The display will light up and show instrument serial number and software revision.
¾ If necessary, press ESC to clear any calibration reminders. Call AZI Customer
Service at 800-528-7411 or 602-470-1414, or e-mail support@azic.com, to schedule
instrument calibration.
¾ 7KHGLJLWDOPHWHUGLVSOD\VȝJP3.
¾ Check the battery level as indicated by the battery icon at the top center of the
instrument display.
If the battery meter is empty and flashing, refer to Charging Internal Batteries on
page 25.
If the battery meter is not empty, but is flashing, then the instrument is currently
charging the battery.
¾ To ensure the instrument's electronics have stabilized, allow a 5-minute warm up
before beginning the next step.
Perform sensor regeneration. Refer to Sensor Regeneration on page 20 for the procedure.
Ensure the instrument has been powered on for at least five (5) minutes prior to sampling.
Use the Zero Air Filter to equilibrate the instrument to ambient air temperature.
¾ ,QVWDOOWKH=HUR$LU)LOWHULQWKHLQVWUXPHQW¶VLQWDNH
¾ Sample repeatedly every 15 seconds until the readings stabilize, then remove the Zero
Air Filter.
Sensor Regeneration
Sensor regeneration is needed to clean the J405 sensor of any accumulated mercury vapor and to
prolong the life of the sensor. This simple procedure should be done:
At the beginning of the day on which the instrument is to be used.
During the day when the sensor becomes saturated.
At the end of the day before storing the instrument.
At a minimum of 30-day intervals while the instrument is in storage.
The unit can be used immediately following the sensor regeneration if necessary.
The Jerome J405 is ready for sampling.
CAUTION:
The Jerome J405 is intended for gaseous vapor use only. DO NOT
allow the probe or the instrument's intake to be exposed to liquids,
dust or other foreign material. Moisture or liquids drawn into the
instrument can damage the sensor and flow system.
Sample Mode
This mode, used for standard operation, produces optimum accuracy with the Jerome J405. See
JEROME J405 TECHNICAL SPECIFICATIONS on page 8 for the accuracy specifications.
Press the power I/O button. The display will light up and briefly show the instrument serial
number and software revision. If necessary, press ESC to clear any calibration reminders.
¾ Next, the digital meter displays 0.00 µg/m3. If the battery meter is empty and flashing,
recharge the battery. See the section Charging Internal Batteries on page 25.
To ensure the instrument's electronics have stabilized, allow a 5-minute warm up before
beginning the next step.
Press the SAMPLE button (located at the end of the handle).
At the end of the 12-second cycle, read the digital meter.
¾ The number shown on the digital meter is the meUFXU\FRQFHQWUDWLRQLQȝJP3. This
value remains displayed until the next sample is taken. The digital meter
automatically re-zeroes at the start of each sample.
When the sensor is completely saturated, the digital meter displays Sensor Regeneration
Required when sampling is attempted. No further operation is possible until a sensor
regeneration is performed. (Refer to the Sensor Regeneration procedure on page 20.)
Press the I/O button to turn the power OFF when not in use.
Survey Mode
The survey mode takes samples and displays the result every 2 seconds automatically. Use this
mode to locate mercury spills or to assess areas of potentially high mercury concentrations.
Sampling in the survey mode is not as accurate.
When operating on battery power, the J405 will shut down after twenty (20) minutes of non-
usage. However, if the instrument is running in Survey Mode or Auto-Sampling mode, the
instrument will not shut off after twenty minutes. If the J405 is reading low levels of mercury in
Survey or Auto-Sampling mode, it will continue to sample until the battery runs out. However, if
the J405 is reading high levels of mercury in Survey or Auto-Sampling mode, when the sensor
reaches saturation a message will appear indicating that sensor regeneration is required, and
twenty minutes later the instrument will automatically power off.
Battery Management
With all handheld and battery powered units, there is a need to keep the batteries properly charged
and ready for use. Proper battery management will not only ensure the instrument is ready when
needed, but will also extend the life of the batteries.
There are 3 different battery management methods recommended based on the frequency of
instrument use. An additional option to ensure the instrument is ready to go at a moment¶s notice
is to purchase an AZI external battery pack (AZI P/N: 990-0214). See External battery power
on page 24 for more information on the external battery pack.
Infrequent user: Greater than one month between uses or long term storage.
For this type of user, the instrument should be fully charged and the battery should be
disconnected. Disconnect the battery by removing the front 2 screws near the intake and opening
the unit. On the front most part of the main circuit board, there is a black 4 pin connector, as
shown. Depress the safety latch
on the connector and pull it out to
disconnect the battery. Close the
instrument and replace the 2
screws in the front of the
instrument. Reverse these steps
to reconnect the battery if the
instrument is going to be used.
The time and date will need to be
reset when the battery is
reconnected for instrument use.
See SYSTEM menu on page 17 Battery
for instructions. Connection
If the instrument will be in storage for more than 4 months, it will need to be taken out of storage
and fully charged every 4 months before being placed back in storage. To do so, reconnect the
battery and connect the AC Adapter Power Supply to charge the instrument for a minimum of 8
hours. See Charging Internal Batteries on page 25 for charging instructions. After charging,
disconnect the battery before returning the instrument to storage. Again, the time and date will
need to be reset if the battery is reconnected so the instrument can be put into service.
Sample data is stored in non-volatile memory and will not be lost or affected when the battery is
disconnected or replaced.
An optional external battery pack (AZI P/N: 990-0214) is available to power the J405, but it is not
recommended for routine use. The external battery pack should be reserved for sensor
regenerations or sampling when the internal battery is nearly discharged and AC current for
recharging the internal battery pack is unavailable.
When operating using the external battery pack, the J405 will shut down after twenty (20)
minutes of non-usage. However, if the instrument is running in Survey Mode or Auto-Sampling
mode, the instrument will not shut off after twenty minutes. If the J405 is reading low levels of
mercury in Survey or Auto-Sampling mode, it will continue to sample until the battery runs out.
However, if the J405 is reading high levels of mercury in Survey or Auto-Sampling mode, when
the sensor reaches saturation a message will appear indicating that sensor regeneration is required,
and twenty minutes later the instrument will automatically power off.
Additionally, using the optional Car Accessory Cable (AZI P/N: 200-0170), the J405 may be
powered from a car accessory jack (cigarette lighter) and draw power directly from the battery of
a vehicle.
To order either of these accessories or for additional information, call AZI Customer Service at
800-528-7411, 602-470-1414, or e-mail support@azic.com.
The internal battery needs to be charged if the battery indicator icon on the main screen is
empty and flashing.
Connect the AC adapter power supply between the J405 power receptacle and an AC power
source.
The battery icon will flash during charging, and the meter in the icon will gradually refill.
¾ Complete battery recharging takes 3 hours.
¾ The J405 contains a trickle charger so it may be continually plugged into an AC power
source without damaging the battery pack.
When the batteries fail to hold a charge, the battery pack should be replaced.
¾ Battery life under normal usage is approximately 1 year, depending on the number of
charge and discharge cycles. See Replacing the Battery Pack on page 33.
Sample data can be transmitted from the J405 for analysis using the USB connections on the back
panel of the J405. Data may be transmitted directly to a PC, saved to a USB drive attached to the
J405 or printed to an AZI printer connected to the J405. See the DATA menu section above for
the specific data transmission options available.
The data is transmitted in a comma-delimited text file with a four-line header indicating the model
and serial number of the instrument, the date and time of the report, and the gas being detected.
The first line of the data indicates the contents of each data field, as shown below. The USB icon
on the main screen will flash during data transmission.
dd-MMM-yyyy,hh:mm:ss,Reading,Units,Temp-C,Type,Location
20-MAY-2006,20:50:17, 2.12, ug/m3, 25.12,N,Lab
20-MAY-2006,20:50:36, 2.48, ug/m3, 25.18,N,Lab
20-MAY-2006,20:50:55, 2.85, ug/m3, 25.37,N,Lab
20-MAY-2006,20:51:47, 2.08, ug/m3, 26.00,N,Lab
20-MAY-2006,20:52:19, 2.47, ug/m3, 26.37,N,Lab
20-MAY-2006,20:52:37, 3.01, ug/m3, 26.56,N,Lab
20-MAY-2006,20:53:01, 2.97, ug/m3, 26.87,N,Lab
20-MAY-2006,20:53:29, 2.96, ug/m3, 27.18,N,Lab
The Temp field lists the internal temperature of the instrument in degrees Celsius at the
time of sampling.
The Type field lists a single letter code that indicates the type of sample taken, as follows:
N: Normal Reading
S: Survey Mode Reading
The Location field lists the location where the sample was taken, as set using SET
LOCATION NAME in the SAMPLE menu. See the SAMPLE menu section on page 14
for more details.
The J405 I/O port is a DB-25F connector on the back of the instrument that provides numerous
specialized functions for specific industrial applications and for factory use. System integration
utilizing the 4-20mA output feature is the most common use of the I/O port.
4-20mA Output
The 4-20 mA output can be used to indicate the Hg reading level on a proportional scale from
4-20 milliamps for connection to certain industrial systems, such as SCADA. A 4 mA current
level always corresponds to a Hg reading of 0.5 µg/m3 or less, while a 20 mA current level always
corresponds to a Hg reading of 500 µg/m3. Current levels between 4 and 20 mA correspond to Hg
readings between 0.5 and 500 µg/m3 on a proportional scale, as determined by this equation:
Mercury levels above 500 µg/m3 will also result in 20mA current readings. The relationship
between the Hg concentration detected and the current level present can be represented
graphically as follows:
In this example, the 5.522mA current level displayed above would correspond to a Hg
concentration of 47.56µg/m3.
After configuring your system, the J405 Diagnostics feature can be used to test your setup. When
the 4-20mA test portion of the diagnostics is reached, the instrument will output current levels of
4, 8, 12, 16 and 20mA, and the current level displayed on the J405 should match the readout of
your 4-20mA system. See SYSTEM menu for additional info on running the diagnostics feature.
After confirming that the system is configured correctly, use the instrument as normal, and the
4-20mA signal will be output automatically by the J405.
To keep the Jerome J405 operating at peak performance, follow the maintenance schedule below
as a guide. Since maintenance is more a function of application and amount of use rather than
time, your requirements may be different from the listed schedule. Call AZI Customer Service at
800-528-7411 or 602-470-1414, or e-mail support@azic.com for additional guidance for your
environment and operation.
REFER TO
PART/COMPONENT MAINTENANCE CYCLE
PAGE
Depends on usage. See Battery Management
Charge batteries Page 25
section for guidelines.
Change .25 inch fritware Weekly or as needed Page 30
Change AG Filter1 Every 500 samples Page 31, 32
Change internal filters and
After 6 months of use or as needed Page 32
tubing1, 2
Replace Zero Air Filter2 Annually N/A
Factory calibration Annually Page 34
Appendix B,
Functional check Monthly or as needed
Page 53
Annually or as needed.
Replace batteries The battery pack contains NiMH batteries. Page 33
Please dispose of properly.
FUSE ± The J405 utilizes an auto-resetting fuse that does not require care, maintenance or
replacement by the user. If the fuse is tripped by electrical power anomalies, it will automatically
reset itself once it detects that electrical power conditions have returned to normal.
1
$*ILOWHUVFRQWDLQ6RIQROLPH)RUVDIHW\LQIRUPDWLRQVHHWKHVXSSOLHU¶V0DWHULDO6DIHW\'DWD6KHHW06'6RU
call AZI Customer Service at 800-528-7411 or 602-470-1414, or e-mail support@azic.com for a copy. Dispose of all
filters properly.
2
Zero Air Filters and scrubber filters contain Resisorb®. For VDIHW\LQIRUPDWLRQVHHWKHVXSSOLHU¶V0DWHULDO6DIHW\
Data Sheet (MSDS) or call AZI Customer Service at 800-528-7411 or 602-470-1414, or e-mail support@azic.com
for a copy. Dispose of all filters properly.
The Jerome J405's flow system is the crucial link between the sensor and the sample. For the
instrument to perform correctly, the flow system must be properly maintained. The user
maintainable components of this system are the intake filter (.25 inch fritware), an AG Filter, two
scrubber filters and connecting tubing.
Check the Preventive Maintenance on page 29 for a suggested schedule for changing fritware
and internal filters. The Tygon® tubing in the system must be free of crimps for proper flow.
Replace the .25 inch fritware filter once each week or as needed. In dusty environments, the
fritware filter may need to be replaced as often as once a day. Replacement .25-inch fritware
filters are available from AZI Consumable Sales at 800-528-7411 or 602-470-1414.
Remove the two (2) side screws from the intake end of the instrument and open the
case.
Gently pull the inner portion of the intake out of the intake port in the direction of the
arrow, as shown in Figure 1 below.
Gently push the old fritware filter disc out of the intake with a small, blunt instrument,
as shown in Figure 2 below.
Place the new fritware onto the inside end of the intake port, as shown in Figure 3
below.
Gently press the inner portion of the intake in the direction of the arrow in Figure 4 to
seat the fritware disc firmly against the inner ledge of the intake.
Once the fritware has been replaced and the inner portion of the intake reinserted,
close the case and replace the two (2) side screws removed above.
The increased sensitivity of the Jerome J405 requires the replacement of the AG filter (600-0293)
every 500 samples to ensure the accuracy of the readings. If your application will require in
excess of six (6) months to reach 500 samples, the AG filter should still be changed every six
months along with the other internal filters.
After changing the AG filter, accuracy at 1.0µg/m3 may change from ±10% to ±20%, and
accuracy at 25µg/m3 may change from ±5% to ±7%. Precision RSD is unchanged.
CAUTION:
Internal filters contain either Sofnolime or Resisorb. Used filters will
contain trace amounts of Mercury also. Use proper methods when
disposing of used filters. Call AZI Customer Service at 800-528-7411,
602-470-1414, or e-mail support@azic.com for a copy of the Sofnolime or
Resisorb MSDS or for other questions.
#3
Internal Filters
Replace the internal filters after six (6) months of use, or as needed.
¾ The AG filter should be replaced every six (6) months or every 500 samples,
whichever comes first, based on your instrument usage schedule.
Press the I/O button to turn the power OFF and unplug the power cord.
Remove the two (2) side screws from the intake end of the instrument and open the case.
Carefully disconnect the Tygon tubing from both ends of the filters and discard the old filters.
Replace the old filters with new filters, oriented as shown in the diagram above.
¾ Push the Tygon tubing as far as it will go onto the filter fittings.
¾ Note that the marked flow direction on the AG filter goes toward the sensor, or to the
left in the diagram above.
Push the filters into the mounting clips.
Remove any crimps or twists in the tubing and ensure that tubing connections are secure. If
the tubing is loose, readings may not be accurate. Replace any tubing that has deteriorated
due to heat and/or age.
Close the case and replace the screws.
If the AG filter is replaced, the new filter must be acclimated to the system by performing a
sensor regeneration, followed by twenty (20) manual samples using the sample button. See
page 20 for sensor regeneration instructions.
Dispose of all filters in accordance with state and federal environmental regulations.
The Jerome J405's gold film sensor is inherently stable and does not require frequent calibration.
The interval between calibrations depends upon the application and frequency of use; however,
the recommended interval is every 12 months.
The Jerome J405 has been factory calibrated using laboratory equipment containing NIST
traceable permeation tubes. These permeation tubes have a rated accuracy of 2%. In order to
calibrate the Jerome J405, a sophisticated calibration system is required that ensures stability of
the calibration gas source, eliminates any pressure in the calibration gas stream, and controls the
temperature of the calibration environment.
We strongly recommend you take advantage of our calibration and maintenance service at
Arizona Instrument. Service includes filter replacement, component testing, and instrument
calibration to NIST traceable standards. A certificate of calibration is issued from AZI when your
instrument is factory calibrated.
Verification of Functionality
The Functional Test Kit (FTK), AZI P/N Y431 0902, is used to verify that your instrument is
functioning correctly between recommended annual factory calibrations. It allows you to have
complete confidence in the sample results. This test verifies proper instrument operation through
the introduction of a known concentration of mercury vapor into the Jerome analyzer.
If your application requires frequent verification of instrument function, this test demonstrates the
XQLW¶Vproper operation and function. Recording FTK results in an instrument log provides a
quality control/quality assurance record of instrument function between regular calibrations. If
test results fall within the expected range, you may assume the instrument is functioning
correctly.
See APPENDIX B ± J405 FUNCTIONAL TEST KIT on page 53 for more information about
the FTK procedures. Complete instructions for use are supplied with the test kit, AZI P/N Y431-
0902.
To order the FTK, contact your AZI Sales Representative at (800) 528-7411 or (602) 470-1414.
Potential interferences to the Jerome mercury vapor analyzers are rare and most of these can be
eliminated with proper maintenance procedures. However, erroneously high readings can
sometimes occur. Here are a few things to be aware of when using the instrument:
The gold film sensors used in the Jerome mercury vapor analyzers do not respond to the
following compounds:
Hydrocarbons
CO, CO2, and SO2
Water vapor (Note that water vapor condensation on the gold film can cause
irreparable harm to the sensor and must be avoided.)
The AG filter (AZI P/N: 600-0293), an acidic gas filter contained in the internal filter system,
removes the following compounds that cause the gold film sensor to respond:
Chlorine
NO2
Hydrogen Sulfide (H2S)
0RVWPHUFDSWDQVRUJDQLFVXOIXUFRPSRXQGVRU³WKLROV´
In areas containing these highly volatile compounds, the filter can quickly become saturated. In
such situations, it is recommended that these gases be allowed to dissipate before sampling for the
less volatile, more persistent mercury vapor. In addition, a special filter designed to remove
chlorine gas from the sample stream is available from Arizona Instrument and may be ordered as
Chlorine Filter, AZI P/N Z2600-3940.
Ammonia in very high concentrations can cause an off-gassing of accumulated acidic fumes from
the internal acidic gas filter, resulting in positive readings on the instrument. In these cases, the
ammonia odors are very strong. A special filter designed to remove ammonia gas from the
sample stream is available from Arizona Instrument and may be ordered as Ammonia Filter, AZI
P/N 990-0193. Again, either allow the vapors to dissipate or use the ammonia filter. Filter
replacement at regular intervals, or when unexpectedly high readings are encountered in areas of
these potential interferences, may resolve these problems.
Volatile mercury compounds in general will cause the gold film to respond. Alkyl organic
PHUFXULHVVXFKDVPHWK\OPHUFXU\DQGRWKHU³VWUDLJKWFKDLQHG´FRPSRXQGVDUHW\SLFDOO\
extremely volatile and change the electrical resistance of the gold film sensor. Any such
UHVSRQVHVVKRXOGEHFRQVLGHUHG³TXDOLWDWLYH´not quantitative. The instruments are designed and
calibrated to elemental mercury vapor only.
Inorganic mercury salts such as mercuric chloride are not very volatile. However, they may
generate some minute level of elemental mercury vapor to which the instruments will respond.
This response, again, should be considered a qualitative response only.
Spare Parts
600-0293 AG filter
For current prices and delivery information, call AZI Customer Service at
(800) 528-7411 or (602) 470-1414.
1) Insert the Jerome J405 CD in the CD-ROM drive on the target PC. The USB Driver
Installer should start automatically. If it does not start automatically, use Windows to
browse to the CD, and locate and run the file Install Driver. Then skip to Step 2 below.
If the Jerome J405 CD is not available, download the driver zip file from
http://www.azic.com and save it to your desktop. If you received these instructions
and the driver in an email, save the attached file, J405_Driver2kXP.zip to your
desktop.
Unzip J405_Driver2kXP to your desktop using WinZip or another zipfile
utility.
Double-click the "Driver Install" folder to open it.
Double-click the "Install Driver" shortcut.
2) Follow the instructions in the AZI Driver Installer wizard. Click Next.
4) Click Finish.
6) If the following dialog box appears, DO NOT connect to Windows Update to get the
GULYHU6HOHFW³1RQRWWKLVWLPH´DQGFOLFN1H[W
8) Windows may display a message indicating that the driver has not passed Windows Logo
Testing. This driver being installed is a generic Communications Port driver that is part of
Windows (usbser.s\VVRLWLVVDIHWRLJQRUHWKLVZDUQLQJ&OLFN³&RQWLQXH$Q\ZD\´WR
install the driver.
10) Windows will then indicate that the driver has been successfully installed.
2) When prompted for a name for this connection, enter J405 and click OK.
3) If HyperTerminal has not been run previously on the target PC, it will ask for an area
code, etc. Enter that information as appropriate and click OK.
5) Next, HyperTerminal will prompt for Port Settings. These settings do not apply to USB
ports, so the default values do not need to be changed. Continue by clicking OK.
7) Select Capture Text... from the Transfer menu on the main HyperTerminal window.
9) Go to the J405 and navigate to the DATA menu, then highlight Send to PC and press
ENTER/START.
10) You should see your data scrolling in the HyperTerminal window. If you do not see
anything in the HyperTerminal window, go to step 12)
12) If you did not receive any text from the J405:
See Retrieving Data on page 26 for an explanation of the fields in the data file.
If your application requires frequent verification of instrument functionality, this test will benefit
you. If the test results fall within the expected range, you may assume the instrument is
functioning properly.
Testing with the Functional Test Kit (FTK) should always be done with the instrument set to
display in micrograms per cubic meter (µg/m3). If your instrument is displaying results in
milligrams per cubic meter (mg/m3), switch to µg/m3 by selecting Units from the SAMPLE
menu, before doing any testing with the FTK. See SAMPLE menu on page 14 for more
information on changing the display units.
The J405 Functional Test Kit contains all accessories necessary to perform the functional test.
See the complete list on page 38 and verify that all the parts to the kit are present.
CAUTION:
The vial and thermometer contain liquid mercury and are possible sources of mercury
contamination. Follow the instructions for handling or transferring the mercury into the
Functional Test Kit Vessel carefully.
)RUVDIHW\LQIRUPDWLRQVHHWKHVXSSOLHU¶V0DWHULDO6DIety Data Sheets (MSDS) or call AZI
Customer Service at 1-800-528-7411 or 1-602-470-1414 for assistance in obtaining the
MSDS.
Preparation
&$5()8//<SRXUWKHPHUFXU\LQWRWKHFHQWHURIWKHIXQFWLRQDOWHVWNLWYHVVHO¶VRSHQLQJ
¾ (1685(WKDWQRPHUFXU\UHVLGXHLVRQWKHRXWVLGHRIWKHYHVVHO6HHWKHVXSSOLHU¶V
Material Safety Data Sheets (MSDS) or call AZI Customer Service at 1-800-528-7411
or 1-602-470-1414 for clean-up instructions.
INSTALL the stopper assembly into the functional test kit vessel carefully, to prevent
breakage of the thermometer.
¾ PRESS the stopper assembly into the vessel to achieve a good seal.
USE the J405 instrument to verify that the outside of the vessel is not contaminated and the
mercury vapor emission level, if any, is below the OSHA TLV for mercury.
ALLOW the kit to adjust to room temperature for at least two (2) hours before using.
¾ The temperature range for the test is 18-22(C. Avoid temperature fluctuations.
CAUTION:
Do not use the FTK vessel as a portable container. If the vessel is upset or greatly
agitated, mercury droplets will cling to the thermometer stem, the rubber stopper,
the mouth of the vessel and the needle guide.
Replacing Mercury
An oxide coating will form on the drop of mercury and will cause lower readings in your testing.
Gently swirl the vessel to disturb the outer oxidized surface of the droplet. If this does not restore
higher readings, it may be necessary to replace the mercury.
CAUTION:
BE SURE NEEDLE GUIDE IS FREE OF LIQUID MERCURY.
¾ Do NOT use the syringe for measuring liquid mercury. Dispose of oxidized mercury
properly.
3UHVVWKH6$03/(EXWWRQRQWKHLQVWUXPHQWDQG³6DPSOLQJ´
DQG³3XUJLQJ´ZLOODSSHDURQWKH-GLVSlay.
Allow the FTK vessel to remain stable at room temperature for at least 2 hours.
¾ The temperature range for the test is 18(- 22(C.
¾ Temperature fluctuations during the test procedure will produce erratic results.
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¾ Refer to page 30 for instructions.
Replace the septum on the septum holder assembly.
Plug the tubing adapter end of the septum assembly firmly into the instrument's intake.
Attach a Zero Air Filter to the septum assembly.
Press power ON.
Take 3 samples.
¾ ,IWKHDYHUDJHPHWHUUHDGLQJLVJUHDWHUWKDQȝJP3, stop here. The instrument may be
contaminated. See J405 TROUBLESHOOTING on page 35.
¾ ,IWKHDYHUDJHPHWHUUHDGLQJLVOHVVWKDQȝJP3, continue to the next step.
Note the temperature of the vessel.
3UHVVWKH6$03/(EXWWRQDQG³6DPSOLQJ´DQG³3XUJLQJ´ZLOODSSHDURQWKHLQVWUXPHQW
display.
Wait 2 seconds and ZKHQ³3XUJLQJ´GLVDSSHDUVIURPWKHGLVSOD\, inject 1 cc of mercury
vapor according to the syringe technique described on page 55. Be sure all mercury vapor has
been injected before the solenoid closes.
CAUTION:
Carefully follow these instructions to minimize error.
16 104 to 136
17 114 to 150
18 123 to 161
19 135 to 175
20 148 to 192
21 157 to 205
22 172 to 224
23 187 to 245
24 201 to 265
If you do not achieve good results with the functional test procedure, check the following:
Results Solution
Typically too high Ensure the FTK vessel temperature is stable.
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from the display (approximately 2 seconds after SAMPLE is
pressed).
Ensure there is no oxidation on the mercury drop in the vessel.
Too Low Gently swirl the mercury drop in the vessel. Replace if necessary.
(QVXUHWKHLQVWUXPHQW¶VLQWDNHLVQRWEORFNHGZLWKIRUHLJQPDWWHU
Check flow with a flow meter.
Ensure syringe is calibrated to 1cc. Use a new syringe needle.
Straighten or replace crimped or blocked internal tubing.
If you find the above does not solve your problem, please call AZI Customer Service at
800-528-7411 or 602-470-1414.
Arizona Instrument LLC (seller) warrants to buyer that Jerome products delivered pursuant to this
agreement shall, at the time of delivery, and for a period of one (1) year thereafter (the Internal
Battery Pack, where applicable, is warranted for a period of ninety [90] days only), to be free
from defects in material or workmanship and shall conform to seller's specifications or such other
specifications as seller has agreed to in writing. Seller's obligations with respect to claims under
this warranty shall be limited, at seller's option, either to the replacement of defective or non-
conforming product or to an appropriate credit for the purchase price thereof subject to the
provisions of seller's Warranty Policy as amended from time to time, said Policy being
incorporated herein by reference.
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V
expense and shall be accompanied by a statement of the reason for the return and an approved
Return Material Authorization Number issued by seller. Buyer remains responsible for payment
for products not accepted for warranty adjustment, handling costs, and freight costs associated
therewith.
Notwithstanding the foregoing, no warranty shall be enforceable in the event that product has
been subjected to environmental or stress testing by buyer or any third party without written
approval of seller prior to such testing. Further, no warranty shall be enforceable if the alleged
defect is found to have occurred because of misuse, neglect, improper installation, repair,
alteration, accident, or improper return handling procedure by buyer.
Notwithstanding the foregoing, if any product covered by order(s) placed hereunder is designated
DV³GHYHORSPHQWDO´³SURWRW\SH´RU ³H[SHULPHQWDO´QRZDUUDQW\ZKDWVRHYHUH[FHSWDZDUUDQW\RI
title to component materials, will be applicable thereto and buyer shall indemnify seller for any
claims for liability asserted seller in connection therewith.
The foregoing state the entire liability of seller in connection with products supplied hereunder.