D 1223 - 93 R98 - Rdeymjm
D 1223 - 93 R98 - Rdeymjm
D 1223 - 93 R98 - Rdeymjm
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D 1223 – 93 (1998)
NOTE 1—Dimensions are given in terms of d, the distance between center of test area and receptor window.
NOTE 2—The cross-hatched rectangle in the W-W circle represents the image of the source field stop in the receptor window.
FIG. 1 Schematic Drawing of Glossmeter
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D 1223 – 93 (1998)
Average the first and second readings for each specimen. In the 10.1.2 Six of the eight papers from the interlaboratory study
absence of other information associated with the sample, were also used in the CTS-TAPPI Collaborative Reference
perform the testing sequence in both the machine and cross Program, Reports 119 through 124. Ten test determinations
directions for both the wire and felt sides of the sample. Insert were made per sample and a minimum of 36 laboratories
the standards at frequent intervals to ensure that the instrument participated. The results were comparable to those obtained in
remains in adjustment throughout the period that the gloss the interlaboratory study and are as in Table 2.
measurements are being made and again at the end of the test. 10.1.2.1 The user of these precision data is advised that it is
8.5 Calculate for the ten specimens the four averages for the based on actual mill testing or laboratory testing, or both. There
machine and cross directions and the wire and felt sides of the is no knowledge of the exact degree to which personnel skills
sample unless otherwise instructed. or equipment were optimized during its generation. The
precision provides an estimate of typical variation in test
9. Report results which may be encountered when the test method is
9.1 Report the average, maximum, and minimum gloss routinely used by two or more parties.
readings to the nearest unit for the felt side and for the wire side 10.1.3 In both the interlaboratory study and the Collabora-
of the sample. tive Reference analyses, it appears that the major contributing
factor to the precision of the data is the material variability.
10. Precision and Bias 10.2 Bias—The procedure in this test method has no bias
10.1 Precision: because the value of gloss at 75° is dependent upon the test
10.1.1 The values in Table 1 are based on an interlaboratory conditions specified in terms of this test method.
study conducted in accordance with TAPPI T 1200. Eight
papers at various gloss levels (ranging from approximately 10 11. Keywords
to 80 gloss units) were tested by eleven laboratories. Twenty- 11.1 coated paper; gloss; paper; paperboard; specular gloss;
five sheets of each paper were measured. uncoated paper
TABLE 1 Interlaboratory Study of Eight Papers Tested by
Eleven Laboratories
TABLE 2 CTS-TAPPI Collaborative Reference Program
Grand Mean Repeatability Reproducibility
(Reports 119–124)
10.94 1.84 2.22
Grand Mean Repeatability Reproducibility
26.71 3.25 4.01
29.99 3.86 4.93 27.12 3.05 4.60
42.48 5.27 7.28 30.30 4.07 5.09
60.32 8.60 9.31 42.73 4.99 7.52
66.20 4.18 5.40 59.08 7.37 8.67
72.29 9.54 9.87 66.52 3.16 6.29
80.40 5.58 6.53 80.56 5.29 6.45
ANNEXES
(Mandatory Information)
A1.1 Optical System—Referring to Fig. 1, beginning at the position of the receptor window, and the diameter of the
lamp, the dashed line indicates the path of the ray of light receptor window (11, 12).
passing through the condenser lens and the geometric center of
a rectangular aperture which becomes the effective source of A1.2 To achieve uniform weighting of the rays taking
light: through the source objective lens, through the geometric different paths through the receptor window, a light mixer (10)
center of the rectangular aperture stop and to the specimen. is interposed between the receptor window and the photode-
This axial ray of light intersects the specimen plane at a point tector. The positive lens is located adjacent to the receptor
defined as the center of the test area. (This is not necessarily the window and is arranged to collect all rays of light passing
geometric center of the illuminated area of the specimen.) With through the window and to form an image of the illuminated
a plane front-surfaced mirror as the specimen, the axial ray is specimen surface on the photodetector sensitive surface, or on
specularly reflected and passes through the center of the a diffusing screen immediately in front of this surface. No rays
receptor window. The source objective lens makes an image of other than those reflected from the specimen surface are
the source aperture at the receptor window. The distance d, the permitted to enter the receptor window.
distance from the center of the test area to the receptor window,
is used as the basis from which to specify all other dimensions. A1.3 Angle of Incidence—The axial ray intersects the
The most critical dimensions are the angle of incidence, the specimen plane at an angle of 75.0 6 0.1°.
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D 1223 – 93 (1998)
A1.4 Receptor Window—The diameter of the receptor gular aperture stop is located 0.6d 6 0.1d from the center of the
window is expressed in terms of the distance d, from the center test area with its plane perpendicular to the axial ray. The size
of the test area to the entrance plane of the receptor window of the stop is 0.10d 6 0.01d by 0.050d 6 0.005d, the short
and is 0.2000d 6 0.0005d and the thickness of its edge is not dimension being in the plane of incidence. No other stops or
to exceed 0.005d. The axial ray, when reflected from a plane diaphragms are permitted to intercept the incident rays of light.
front-surface mirror in the specimen position, passes through
the center of the receptor window within 0.0004d and is A1.8 Uniformity of Light in the Aperture Stop—These
perpendicular to the plane of the receptor window. tolerances are required to be the same as for the source
aperture. Based on the coordinate system described, they are:
A1.5 Position and Size of Light Source Aperture—The ȳ 5 0 6 0.05y0 (A1.4)
position of the image of the light source aperture is in the plane 2
ȳ 5 0.33y02 6 0.04y02 (A1.5)
of the receptor window with a tolerance, along the direction of
2
the axial ray, of 60.04d. The size of the rectangular image is x̄ 5 0.33x02 6 0.03x02 (A1.6)
0.100d 6 0.005d by 0.050d 60.005d, the short dimension of With the specimen aperture open, and through the use of an
the rectangle lying in the plane of incidence (that is, containing auxiliary lens, an image of the aperture stop can be formed
the incident and the specularly reflected axial ray). outside the instrument. Scanning of this image with a photom-
eter, as described in Annex A2, yields the required information
A1.6 Uniformity of Light in Source Aperture—The distri- for determining the uniformity of light distribution in the
bution of light in the source aperture is required to be uniform aperture stop.
in accordance with the following: Let the direction of the axial
ray be the z axis, the x axis perpendicular to the plane of A1.9 Spectral Conditions—The incandescent source oper-
incidence, the y axis perpendicular to the z axis and parallel to ates at a color temperature of 2850 6 100 K. The photoreceptor
the plane of incidence. Let the coordinates of the sides of the is spectrally corrected by means of a filter so as to give the
rectangular source be 6x0 and 6y0. Then, the rectangle is 2x0 combination a spectral response duplicating the CIE luminous
long and 2y0 high. The distribution of light flux in the source efficiency function, (YA) which has an effective wavelength of
aperture in the y direction is required to be so arranged as to 572 nm.
satisfy the following equation:
A1.10 Light Detector—Any combination of photodetector
*
1 y0
F~y!ydy and indicating device may be used, provided it gives a
2 y0
ȳ /y0 5 5 0 6 0.05 (A1.1) numerical indication of the light flux passing through the
y*
1 y0
0 F~y!dy receptor window accurate over the entire scale to within
2 y0
60.2 % of full scale: that is, 60.2 scale division for a scale
where F (y) is the light flux per unit area expressed as a comprised of 100 divisions. The photometric linearity may be
function of y, and further, that, established by using the procedure described by Höfert and
*
1 y0
F~y!y 2dy Loof (13).
2 2 y0
ȳ /y02 5 5 0.33 6 0.04 (A1.2)
*
1 y0 A1.11 Specimen Holder—The suction plate for holding the
y02 F~y!dy
2 y0 specimens is firmly mounted and sufficiently flat so that the
It should be recognized that for a perfectly uniform distri- image in the receptor window of a thin, flexible plastic film of
bution of light, ȳ = 0 and ȳ2 = y02/3. The light distribution in uniform thickness (for example, 0.003-in. thick, optical grade
the x direction is required to satisfy the following equation: Mylar) held by this suction plate, will not be measureably
different in position and size from that of the image formed by
*
1x
F~x!x 2dx the black glass standard as described earlier. Suction plates
2 2x
x̄ /x02 5 5 0.33 6 0.03 (A1.3)
* may be made from a solid plate which contains two shallow
1x
x02 F~x!dx
2x grooves (or a single circular groove) on the side of the plate
The data for these equations may be obtained as described in against which the specimen is held. The connection for
Annex A2, and their application is discussed in Annex A3. supplying vacuum to the grooves may be made by drilling
holes through the plate into each groove. Solid flat plates of
A1.7 Position and Size of the Aperture Stop—The rectan- brass or steel are suitable for making this type of suction plate.
A2.1 With the specimen aperture open, the image of the aperture. By scanning this image of the source with a photom-
source aperture will be formed outside the instrument and can eter of adequate sensitivity and one which has an aperture as
be observed on a viewing screen such as a piece of white paper discussed below, the required data can be obtained for deter-
or ground glass. The image of the lamp filament should be mining the uniformity of light distribution in accordance with
centered in the image of the source aperture and should fill this Eq A1.1, Eq A1.2, and Eq A1.3.
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D 1223 – 93 (1998)
A2.2 The photometer scanning aperture may be circular or should be of a size (that is, diameter or width of slit) equal to
in the form of a long, narrow slit; its size, however, as about 1⁄8 to 1⁄6 of the dimension of the rectangular source
discussed below, should be appropriately related to the size of aperture image being scanned. For scanning the image, pho-
the image of the source aperture and to the spacing of the lamp tometer readings should be obtained for at least six equally
filament windings. The use of too small a scanning aperture spaced positions for both the short and the long dimensions of
introduces an undesirably high variation in the photometer the image. The integrations indicated in Eq A1.1, Eq A1.2, and
readings, inasmuch as the photometer in this case will respond Eq A1.3 should be performed on intensity data read from a
to the local changes in light intensity caused by the windings of smoothed curve of the plot of the photometric data. The
the lamp filament. The use of too large an aperture, on the other procedure for obtaining a numerical approximation for the
hand, leads to an averaging of the intensity rather than to the integrals in Eq A1.1, Eq A1.2, and Eq A1.3 is given in Annex
measurement of its distribution. For example, in scanning an A3.
image showing eight filament windings, the scanning aperture
A3. LIGHT UNIFORMITY IN THE SOURCE APERTURE AND IN THE APERTURE STOP
A3.1 In Fig. 1, the light source is shown to be formed by A3.3 Symmetric distributions of this sort, of course, exactly
the image of a lamp filament inside a rectangular aperture. This satisfy the requirements of Eq A1.1. Sample calculations for
arrangement is not mandatory, but it is probably the easiest the approximate solutions of Eq A1.1 and Eq A1.3 are shown
way to make a light source with a precisely defined boundary. subsequently. For this illustration, the flux distribution for the
When this method is used, the light source will have point-to- ydimension of the image for either the source aperture or the
point variations in intensity because of the filament shape. aperture stop is shown in Fig. A3.1 and that for the xdimension
Such a source is certainly not uniform, although it will be in Fig. A3.2.
photometrically equivalent if the flux distribution satisfies
closely Eq A1.1, Eq A1.2, and Eq A1.3 given under geometric A3.4 Using data obtained from Fig. A3.1, Table A3.1 shows
specifications. It is, of course, possible to defocus the lamp the steps in the calculation of the summations involved in the
filament to improve the flux uniformity. Doing so, however, equation:
involves a possible risk of making the light flux nonuniform y/y0 5 @ ( F~y!~y/y0!# / @ ( R~y!# (A3.1)
over the aperture stop. If the image of the filament is focused
at or near the source aperture, however, the requirement for A3.5 Dividing the sum of the values in Column 3 by the
light uniformity at the aperture stop will likely be satisfied sum of the values in Column 2 yields y/y0 = 0.015. For this
without further effort. illustration of light distribution, the value of 0.015 meets the
specification which states that y/y0 is to lie within the range 0.0
A3.2 The requirements in Eq A1.1, Eq A1.2, and Eq A1.3 6 0.05.
can be better understood if a few typical flux distributions are
considered. First, consider Eq A1.1 for the centroid of flux
distribution with respect to the variable y. Suppose the flux per
unit area is 1 unit at y = 0 and varies linearly from about 5⁄6
unit at y = −y0 to 7⁄6unit at y = + y0. This distribution will
meet the requirements of Eq A1.1 with a little margin and will
be in perfect agreement with the requirements of Eq A1.2.
Second, consider Eq A1.2 and Eq A1.3 for the average values
of y2 and x2. These quantities are analogous to the square of the
radius of gyration of a rotating body, and the flux distribution
is analogous to the mass distribution. For this problem,
consider a flux distribution that has its maximum at the center
(x or y = 0) and tapers off linearly to a smaller value at the two
ends (x = 6x0 and y = 6y0). If the flux density at the ends
(y = 6y0) is 5⁄8 or greater, compared with its value at the center FIG. A3.1 Illustrative Data Showing Light Flux Distribution for
Short Dimension of an Image of the Source Aperture or Aperture
(y = 0), Eq A1.2 will be satisfied, and if its value at the ends Stop, or Both. Positions of Plotted Points on y/y0 Axis
(x = 6x 0) is 7⁄10 or greater of its value at the center, Eq A1.3 Correspond to the Use of a Scanning Slit Having a Width Equal
will be satisfied. to 2y0/7, or One-seventh of the Dimension Being Scanned.
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D 1223 – 93 (1998)
TABLE A3.1 Steps in the Calculation of the Summations of
Eq A3.1
y/y0 F(y) F(y) (y/y0)
0.1 86.0 8.6
−0.1 86.0 −8.6
0.3 84.0 25.2
−0.3 83.0 −24.9
0.5 79.0 39.5
−0.5 77.0 −38.5
0.7 73.0 51.1
−0.7 68.0 −47.6
0.9 65.0 58.5
−0.9 58.0 −52.2
( = 759.0 ( = 11.1
FIG. A3.2 Illustrative Data Showing the Light Flux Distribution for
Long Dimension of an Image of the Source Aperture or Aperture
Stop, or Both. Positions of the Plotted Points on x/x0 Axis TABLE A3.2 Steps in the Calculation of the Summations in
Correspond to the Use of a Scanning Slit Having a Width Equal Eq A3.2
to 2x0/8 or One-eighth of the Total Length. x/x0 (x/x0)2 F(x) F(x) (x/x0)2
0.1 0.01 84.0 0.84
−0.1 0.01 87.0 0.87
A3.6 Using data obtained from Fig. A3.2, Table A3.2 shows 0.3 0.09 78.0 7.02
the steps in the calculation of the summation involved in the −0.3 0.09 86.0 7.74
equation: 0.5 0.25 69.0 17.25
−0.5 0.25 84.0 21.00
x 2/x02 5 @ ( F~x!~x/x0! 2# / @ ( F~x!# (A3.2) 0.7 0.49 57.0 27.93
−0.7 0.49 80.0 39.20
0.9 0.81 43.0 34.83
A3.7 Dividing the sum of the values in Column 4 by the −0.9 0.81 74.0 59.94
sum of the values in Column 3 yields x2/x02 = 0.292. For this ( = 742.0 ( = 216.62
illustration of light distribution the value of 0.292 does not
meet the specification which requires x2/x02 to lie within the
range of 0.33 6 0.03. Consequently, the uniformity of light distribution would have to be improved.
REFERENCES
(1) The Institute of Paper Chemistry, Instrumentation Studies V, “Report (8) Budde, W., and Dodd, C. X., “Stability Problems in Gloss Measure-
on Gloss,” Paper Trade J. 104(1): 42 (Jan. 7, 1937); Instrumentation ments,” J. Coatings Technology 52: 44 (1980).
Studies VI. Paper Trade J.104(2): 42 (Jan. 14, 1937). (9) The Institute of Paper Chemistry, Instrumentation Studies XII,
(2) Hunter, R. S., “Method of Determining Gloss,” J. Research Natl. “Effect of Relative Humidity on Physical Properties with Respect to
Bureau of Standards, 1937; 18, 19 (R.P. 958). the Hysteresis Effect in Changes from One Humidity to Another,”
(3) Harrison, V. G. W., “The Definition and Measurement of Gloss,” Paper Trade J. 104(15): 45 (April 15, 1937).
Cambridge, England, W. Heffer and Sons, Ltd., 145 pages. (10) Hunter, R. S., “Standardization of Test for Specular Gloss of Paper,”
(4) Wink, W. A., Delevanti, C. H., Jr., and Van den Akker, J. A., Tappi 41(8): 385 (1958).
Instrumentation Studies, LXXVII, “Goniophotometric Study of High- (11) Zabel, L. W., and Wink, W. A., “A Study of the Effects of
Gloss Papers,” Tappi 36(12): 163A (1953). Instrumental Variables on 75° Specular Gloss,” Tappi 37(10): 474
(5) Hunter, R. S., and Lofland, C. A., “Gloss Test for Waxed Paper,” (1954).
Tappi 39(12): 833 (1956). (12) Hammond, H. K. III, and Hsia, J. J., “Evaluation of Instrument
(6) Hunter, R. S., “Method of Evaluating the Gloss of Ink Films,” Tappi Tolerances for 75° Gloss,” Tappi 58(11): 143 (1975).
46(7): 162A (1963). (13) Höfert, H., and Loof, H., “Calibration of the Photometric Scale of a
(7) Budde, W., “The Calibration of Gloss Reference Standards,” Metro- Reflectance Photometer,” Zeitschrift für Instrumentenkunde 72(5):
logia 16: 89 (1980). (1964) (in German).
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