World of Filtration Experience Ebook
World of Filtration Experience Ebook
World of Filtration Experience Ebook
Filtration
Experience
A World of Filtration Experience
Filtration Overview:
The Removal of Unwanted Solids
Filtration Overview
Mineral Filter Aids for All Industries
Industry Application
Food and Beverage Juices, beers, wines, sweeteners, oils, syrups, honey
Industrial Biodiesel, sizings, oil and solvent recovery, greases, waste oils
Diatomaceous Earth
Why Diatomaceous
Earth is an Ideal
Filter Aid
Diatomaceous Earth Filtration Applications
To understand why
Diatomaceous Earth Diatomaceous Earth filtration use crosses
makes a perfect filter many industries, from recreation to food and
aid, you’d have to look through a microscope. beverage, and pharmaceutical to automotive.
Diatoms show up in a variety of forms. The
symmetrical forms resemble honeycombs, disks, Some applications include:
rods, cylinders, and snowflakes. This porous
structure is what helps to trap solids and allow • Swimming pools
liquid to readily flow through the filter cake. This • Food Production
means it is a mechanical sieving, not a chemical (sugar, sweeteners, and gelatin)
treatment.
• Beverage Filtration
(beer, wine, and juices)
Diatomaceous Earth products are calcined and
• Biodiesel/Motor Oil Processing
flux-calcined in order to improve their properties
(soy, corn, palm oils, and animal fats)
as a filter aid. The calcination process is
performed at temperatures above 1500 degrees • Pharmaceutical manufacturing
Fahrenheit, ensuring all products are free of • Enzymes
organic matter.
Diatomaceous Earth
7000
10
6000
Permeability: Darcies
6
5000
4500
4 4200
Swi m Pool
2500 4500C
Speedex
2 Speedplus B Speedplus 375
231 341 Speedplus A
215 Superaid UF Speedflow
0
Very Sparkling Sparkling Very Clear CLEAR
<10% <25% <50% <75% <90% <100% Median Permeability, Permeability, Permeability, PCD, Micron Micron
Particle PFRV/Darcies PFRV Darcies lb/ft3 Removal Removal
Size (µ) (Range) (Calculated)
Off-White 70-85 /
341 10 16 26 41 60 410 20-35 77.5 0.61 26 <1.0 0.3
/ Pink 0.49-0.73
85-105 /
SPEEDPLUS White 8 15 24 38 51 92 30 95 0.915 26 <1.0 0.5
0.73-1.1
105-120 /
375 White 12 20 33 50 72 282 35 112.5 1.275 23.1 1-2 0.6
1.1-1.45
120-140 /
SPEEDEX White 13 23 39 66 131 1143 35-40 130 1.705 23.1 1.5-2.5 0.9
1.45-1.96
140-165 /
2500 White 16 29 50 77 119 340 40-50 152.5 2.345 23.1 <3.0 1.2
1.96-2.73
Flux Calcined
Burney, CA
140-190 /
SWIM POOL White 19 35 60 96 160 1660 -- 165 2.785 23.1 3-5 1.4
1.96-3.61
165-190 /
4200 White 8 17 28 37 43 53 55 177.5 3.27 23.1 <3.0 1.6
2.73-3.61
190-210 /
4500 White 23 41 66 106 172 948 55-60 200 4.01 23.1 <3.0 2.0
3.61-4.41
210-230 /
5000 White 22 40 68 109 170 450 60-70 220 4.85 23.1 <3.0 2.4
4.41-5.29
260-300 /
6000 White 25 46 74 107 131 177 75-90 280 7.88 23.1 5.0-6.0 3.9
6.76-9
290-340 /
7000 White 36 59 93 138 195 948 90-110 315 9.985 23.1 <7.0 5.0
8.41-11.56
Reddish < 16 /
215 4 9 20 53 160 787 10 16 0.025 N/A <0.5 0.0
Orange < 0.025
Reddish 16-24 /
SuperAid 3 7 13 23 37 92 13-15 20 0.0405 N/A <0.5 0.0
Orange 0.025-0.056
Basalt, NV
Calcined
Reddish 24-36 /
UF 3 6 13 28 65 177 14-18 30 0.095 N/A <0.5 0.0
Orange 0.06-0.13
Reddish 36-52 /
SPEEDFLOW 3 7 14 25 45 134 15-18 44 0.2 27.5 <0.5 0.1
Orange 0.13-0.27
Pink 52-65 /
231 8 12 18 29 45 84 20-23 58.5 0.35 27.5 <0.7 0.2
Orange 0.27-0.43
Diatomaceous Earth
Dicalite Flux-Calcined DE provides the highest Dicalite uses a unit termed PFRv (permeability
flow rates with the best possible clarity. Removal flow rate by volume) to measure our filter aids.
efficiencies vary depending upon customer PFRv can easily be converted to Darcies, and
application, equipment and process, however, it we report both properties to our customers
has been reported by one customer that Dicalite worldwide. It is important to note that a filter aid
Speedplus removes particles down to 0.5um! permeability value cannot be used to determine
Flux-Calcined DE is normally used on Rotary filter flow rate under process conditions in that,
Vacuum drum filters and Filter-Press equipment among other variables, it does not include the
where high solids loading, high flow rates, and dominant effect of the particulate matter which
excellent clarity are required. Flux-calcined is being filtered. In fact, changing to a faster flow
DE is also used on vertical and horizontal leaf rate filter aid will not always increase the flow
filters, and candle filters where higher flow rate on your industrial filter!
rates are required. Filter aids are classified by
permeability, which is normally expressed in For more information on grade selection for your
Darcies. A Darcy is defined as the property of process, review the DE filter aids on page 6 of
porous material which will allow a flow rate of this guide and contact our Technical Services
1ml of water under standard conditions through 1 Department.
cm2 of area under one atmosphere of pressure.
Diatomaceous Earth
Pore size directly affects the removal efficiency the permeability, the smaller the particle size,
of a filter aid. There are a number of methods and the smaller the pore size. For example,
to report the pore size of a filter aid including the permeability, particle size and pore size for
pore size by volume, and pore size by surface Dicalite Speedplus are all smaller than the same
area. Usually results are reported in Median values for Dicalite 6000. Since all DE is unique
Pore Size (MPS) which means there are an equal and has unique morphology (size and shape), it
number of pores smaller than the MPS as there follows that you cannot compare permeability,
are pores which are larger than the MPS. There particle size, and pore size from one DE supplier
are also other reporting parameters including to another. More specifically, you can compare
average pore size and maximum pore size. permeability between vendors, but the particle
Permeability, particle size, and pore size are all size and pore size will be different for the same
correlated for the same DE deposit. The slower permeability values.
SPEEDPLUS
SuperAid
SPEEDPLUS A
SPEEDPLUS B
MOOSEHEAD 341
215
231
341
375
2500
4200
4500
5000
6000
7000
SWIM POOL
SPEEDFLOW
4500C
In general, dividing the Darcy permeability value in half will result in the corresponding micron retention during filtration.
Perlite
Perlite
Perlite filter aids can be used with either Additional benefits of perlite filter aids come
pressure or vacuum filtration equipment. Perlite at the end of the filter cycle. Perlite filter cakes
generally replaces other filter aids on a one-to- remain porous and do not compact. Filter
one volume basis. For example, a cubic measure cakes built up under pressure release easier
of perlite will replace the same volume of other when perlite is used. This release facilitates
filter aids. Selection of the optimum grade and easier cleaning, potentially reduces manpower
dosage may require assistance from technical requirements and costs, and increases
services and in-plant trials. productivity. The lower weight of perlite filter
cakes may also reduce disposal costs.
Perlite
A Variety of Grades
Productivity, clarity, and flow rates may be through a cake 1cm thick at a differential
increased through the use of perlite filter aid pressure of 1atm. The higher flow grades are
grades. At Dicalite, we produce perlite filter aid especially applicable to use with highly viscous
grades ranging from 0.13Darcies to 3Darcies. liquids such as syrup, resins or gelatinous
A material with a permeability of 1Darcy passes slurries. These traits are accomplished during
1mm/second per square centimeter of a liquid the liquid’s path through the channels created
of 1cP viscosity (approximately that of water) by the jagged, interlocking particles.
Product Dicalite Type Color Permeability Permeability Float PCD 40Mesh 140Mesh MPD Type of Filter Common Filtration Appli-
Production (PFRV) (Darcies) (ml) (cake density) Screen (max. Screen (max. (Median Particle Equipment cations
Facility lbs/ft3 (max) Retain %) Retain %) Size-Typical um) required
Candle/
White/ Beer body feed, Seed Coating,
FF416/416 Crawfordsville, IN PFA <35 <0.13 14 NA Trace 0.2 25-35 Pressure
Greyish Poly Filler
Leaf
Candle/
Off-
FF426/426 Crawfordsville, IN PFA 35-50 0.13-0.25 16 16-26 Trace 0.2 25-35 Pressure Beer body feed, Seed Coating
White
Leaf
Candle/
Off- Cutting Water/Oil Recycling,
FF436/436 Crawfordsville, IN PFA 50-65 0.25-0.43 22 18.5 1 7 30-35 Pressure
White Seed Coating, Texturing Paints
Leaf
Candle/
Off-
FF456/456 Crawfordsville, IN PFA 65-80 0.43-0.64 30 17 1 10 35-40 Pressure Texturing as a Filler
White
Leaf
Candle/
Off- Pressure Beet Sugar, Waste Water
FF476/476 Crawfordsville, IN PFA 80-95 0.64-0.9 35 17 2 14 40-45
White Leaf/Filter Filtration
Press
Candle/
Beet Sugar, Beer Precoat, Waste
Off- Pressure
476SP Crawfordsville, IN PFA 95-105 0.9-1.1 40 16.5 2 15 40-45 Water Filtration, Activated
White Leaf/Filter
Carbon Removal
Press
Pressure
Off-
LD1106 Crawfordsville, IN PFA 120-150 1.44-2.25 NA 11.5 3.5 50 65-80 Leaf/Filter Corn Syrups, Chemical Filtration
White
Press/RVDF
Perlite
Perlite’s low density, availability, performance, Perlite filter aids are both sterile and inert and
cost, inert nature, and environmental footprint are used for filtering liquids in the beverage,
make it an essential filtration aid in many food, and pharmaceutical industries. No tastes,
industries, including: colors or odors are imparted. Perlite meets the
standards listed in the Food Chemicals Codex
• Food Production • Beverage Filtration (published by the United States Pharmacopeia),
• Chemicals • Pharmaceutical deeming it safe for its intended use.
*The Food Chemicals Codex is regarded as a source of information on the quality and purity of food
grade substances, and is regarded as authoritative by many government agencies throughout the world.
Perlite
Rotary vacuum precoat filters are typically used for thick, difficult-to-filter liquids or when the solids
content is high. The precoat is formed on a drum with a cloth or metal-septum by recirculated a 2% to
5% filter aid slurry. A 2” to 4” cake can be applied in an hour or less.
During the operating cycle, the process fluid passes through the cake, leaving solids on the precoated
surface. A mechanically operated knife blade continuously shaves off the filterable solids and leaves a
clean filtering surface. Selection of the proper depth of cut depends mostly on the nature and quantity of
the solids. Cycle lengths vary from eight to 24 hours, determined by the depth of cut and cake thickness.
Flow rates are, for the most part, dictated by the filter aid solids and liquor viscosity. Common drum
speeds range from one to 1/5 revolutions per minute. The optimum grade and type of filter aid is the
grade that maintains the solids on the surface of the cake. Optimum clarity occurs when solids are
retained at the precoated surface.
Considerations:
The filter septum serves principally as the In most cases, the first step of filtering is the
support for the filter aid cake, and the effect formation of the precoat. This thin layer—1/16”
of the septum on the performance is sufficient to 1/8”—protects the septum and ensures clarity
to warrant careful selection. Considerations by stopping the solids at the surface. The filter
include: aid grade used for the precoat must be carefully
selected to allow the fastest possible flow, yet
• Size: It should be fine trap the solids.
enough to retain the
filter aid particles and The filter aid should be added at 10 to 25 lbs/100
allow a firm cake to be feet squared of filter area. The precoat is formed
formed quickly, while also giving a minimum by recirculating the filter aid slurry through the
resistance to flow. filter. This slurry is made from the filtered fluid or
water and a filter aid. The concentration should
• Material: It must be able to withstand chemical, be as low as possible; 0.5% is typical.
pressure, and temperature conditions existing
during filtration. The two most widely used A precoating rate of 1 GPM/foot squared is
septa are metal (24x110 Dutch Weave) and typical. Higher viscosity liquids, like honey and
cloth. syrup, require lower rates. There should be
at least 1 psi differential pressure during the
precoat process. Precoating liquid should clear
DE bridges the screen openings and forms a precoat
up within 10 to 15 minutes.
The addition of the filter aid to the fluid is Clarity is considered by many engineers to be
referred to as body feed. Carefully choosing the most important measure of efficiency in filter
the type, grade, and quantity of filter media is aid filtration. A high-quality filter aid is critical for
important to obtain the highest filtration flow rate uniform results day after day. Selection of the
consistent with the clarification required. particular type and grade of filter aid having the
correct particle size and distribution is a major
Filter aid dosage varies with the solids content factor. Other considerations include:
and other variables specific to each application.
In general, a dosage of 1/2 of the percent of • The quantity of filter aid to be used
solids by weight is adequate. Bodyfeed can be • Flowrate needed to meet plant production
added directly to the tank of fluid to be filtered schedules
or dosed from a slurry tank into the filter inlet. • Equipment limitations
• General filtration conditions
70
60
particles down to 3-5 microns; (well
Microns
N The human eye cannot see particles smaller than 35-40 microns
Types of Filters
Pressure Filter
Types of Filters
Vertical Leaf Filter
Filter Press
DMG Satisfies the World’s thirst for DE and Perlite Filter Aids
While you’re deciding which filter aid best meets
your needs, consider which supplier will meet We help guide you to success by
your needs, too. Dicalite Management Group is focusing on the below requirements:
the leading vertically integrated mineral filter aid
supplier in North America and Europe. Our team 1. Economy
has helped companies all around the globe 2. Faster flow rate
choose the right mineral filter aid for nearly 100 3. Longer filter cycle
years. DMG operates the largest filter aid plant in 4. Better clarity
all of Europe and the fourth oldest continuously 5. Uniformity
running mine in Nevada.
British Columbia
KEY
Alberta
Saskatchewan
Washington Ontario
Manitoba Quebec
Sales & Marketing
Maine
Montana 866-728-3303
North Dakota Minnesota
marketing@dicalite.com
Oregon
VT
NH
Idaho Gary Smith
Wisconsin
South Dakota MA 208-409-8661
New York
Wyoming Michigan CT
RI
gsmith@dicalite.com
British Colum
NJ
Pennsylvania
Nevada Nebraska Iowa Donna Frassrand Chatfield
770-262-0396
Ohio MD
Utah Illinois
Indiana DE dfrassrand@dicaperl.com
Colorado West Washington
Virginia Virginia Brian Colbert
Kansas
California Missouri
Kentucky 905-302-5824
bcolbert@dicaperl.com
Oklahoma North Carolina
Tennessee
Arizona
New Mexico
Arkansas South Don Verrico
Carolina 610-517-903
Georgia
Oregon
Alabama dverrico@dicaperl.com
Idah
Texas
Mississippi Shelby McArthur
530-335-5451,
Louisiana Florida
smcarthur@dicalite.com
Nevada
Dicalite has 16 facilities across North America and Europe: four mines and 12 facilities that refine,
process, manufacture, and package our products. With an unequaled number of geographically California
dispersed processing sites and large ore reserves, DMG is able to provide better, faster, and
consistent service for our customers.
Ar
When you choose Dicalite Management Group for your filtration needs, you get:
1. Multi-Layered Help Along the Way: Our dedicated sales and technical services
teams work together to provide you with the right mineral recommendation to ensure
your product is free of contaminants and unwanted solids.
2. Variety: DMG offers Diatomaceous Earth, perlite, and cellulose in a complete range
of grades.
4. Technical Assistance: Our technical services team is always ready to support your
filtration needs and answer any questions that may arise.
6. The right product for your needs: DMG stands by our product recommendations, so
in-plant trials are encouraged with the support of our technical team.