D2 PHASER

Diffraction Solutions

XRD
Innovation with Integrity
 Compact all-in-one
desktop design
Innovative high-end
goniometer design
Integrated PC / monitor
DIFFRAC.SUITE software
Leading detector technology

The whole world

of X-ray diffraction
on a desktop –
D2 PHASER
Status display LEDs Transport handles
What do you obtain when patented
technologies, award-winning software,
a fully functional PC with monitor and
state-of-the-art detectors meet up with
leadership in innovative X-ray diffraction?
Perfect solutions for powder diffraction.
And if it all fits onto a desktop,
it is called D2 PHASER!
What enables this evolutionary leap to take place and
how can the amazing performance of this space saving
sensation actually be explained? 1-dimensional LYNXEYE detector Internal chiller

First of all, you develop an ultra compact goniometer,

file a patent, complete the system with all the other
components for autonomous operation and package the
whole configuration together with a fully functional PC,
monitor, keyboard and mouse, into a compact housing.
Second, you use the unique DIFFRAC.SUITE software
for controlling the instrument and analyzing the data.
Since its introduction the DIFFRAC software has devel-
oped into a high performance tool for the characterization
of crystalline phases in research and industry.
USB and Ethernet connectors Integrated drawer for
Third, you use only the best components, for keyboard and mouse
example the LYNXEYE detector. This state-of-the-art and
extremely efficient 1-dimensional detector simultane-
ously captures a large angular range and radically reduces
the measurement time: hours turn into minutes.
Combining all of these incredible innovations creates a
desktop X-ray diffractometer which has the analytical
performance and functions of a large instrument, but
which is easy to transport and opens up the whole world
of powder diffraction without a lot of infrastructure.
D2 PHASER – all-in-one desktop design D2 PHASER with opened X-ray on status LEDs
D2 PHASER – never before was desktop front cover
X-ray diffraction better, smaller and more
powerful!

2 3
 Holders Holder for Holder for Low back- Airtight Holder for
with various automated clays ground holder for filter samples
cavities sample holders for environment-
preparation small sample sensitive
amounts samples

D2 PHASER – the
desktop giant!
Wishes come true – comprehensive,
unique and non-destructive characterization
of crystalline samples by means of X-ray
diffraction (XRD) with the D2 PHASER. Cement & Minerals
Raw Materials & Mining
Our D2 PHASER opens the door to modern XRD for you.
This means qualitative and quantitative phase analysis,
polymorphism investigation, the determination of
crystallinity, all the way through to structure investigation
– all of it fast, simple, efficient and with high quality.
It is not just its analytical performance that makes the
D2 PHASER so revolutionary, but also its flexibility in
handling very diverse samples. Different material
properties require different sample preparations. Geology & Ceramics
Exploration
Therefore, besides a series of standard sample holders
made from PMMA or steel, the D2 PHASER also offers
holders for small sample amounts, low-absorbing and
weakly diffracting samples, for filters, for environment-
sensitive samples and for examining materials that tend
to show a preferred orientation.

LYNXEYE fast-lane edition

Chemistry Research
What makes the D2 PHASER absolutely unique is the & Catalysts & Education
integration of the world's leading 1-dimensional detector
for X-ray powder diffraction: Our LYNXEYE.
With a performance enhancement in terms of intensity
by a factor of more than 150, the D2 PHASER is actually
playing in the top class. Additionally the LYNXEYE allows
suppression of sample fluorescence providing an excel-
lent peak-to-background ratio even for strongly fluores-
cent samples, eliminating any need for secondary
Pharmaceuticals Environment
monochromators.
D2 PHASER – slide-up front cover for sample loading, monitor remains active
D2 PHASER – X-ray diffraction in a
new dimension!
Phase identification and quantification
Degree of crystallinity determination
Phase properties (cell parameters,
crystallite size, and lattice strain)
Crystal structure analysis
Wide variety of different sample holders of
industrial standard dimension (Ø 51.5 mm)
4 5
 No No No
Plug’n On-Site Hand Carry Water High PC &
Analyze™ Ready Weight Supply Power Peripherals

All-in-one is every-
thing you need –
D2 PHASER
Can XRD – the best method for phase
characterization – really produce high
quality data without the need for a
corresponding infrastructure?
Yes! With our D2 PHASER a new era begins.
All that is required is a simple domestic wall socket and
you can start producing outstanding analytical results:
Plug ‘n Analyze. Since it is a desktop system it requires DIFFRAC.EVA DIFFRAC.TOPAS DIFFRAC.TOPAS
only a minimum amount of space and is in no way Quantitative Analysis Structure Analysis
Qualitative phase identification
inferior to a large system in terms of its analytical - ICDD PDF2 and PDF4 Quantitative phase analysis Indexing (LSI and LP-Search methods)
performance. Resolution, angular accuracy and data - User-defined databases - Crystalline phases
Pawley and LeBail fitting
statistics set new standards in this class of analytical - Amorphous phases
Semi-quantitative phase analysis
instruments; data quality which you can rely on and with Rietveld structure refinement
- RIR method Degree of crystallinity
which even complex questions can be answered.
- Combined XRD-XRF analysis determination Ab-initio structure determination
Our D2 PHASER is a transportable all-in-one instrument - Simulated annealing
Publication-ready reporting Spiking method
that requires no additional cooling water or PC peripherals. - Charge Flipping
This means that there is nothing to prevent it from being PONKCS method - 3D Fourier analysis
used outdoors: simply switch-on a power generator, plug Microstructure analysis
in the connector and start measuring!

D2 PHASER – X-ray diffraction tool for

everyone – everywhere!

Minimal electrical power

consumption (650 W)
No cooling water supply
No significant tube ageing –
practically endless tube lifetime
Minimal space required
6 7
 XRD on polycrystalline material – more intensity with LYNXEYE detector

Common point detector setup Scintillation

X-Ray Counter
Source In an XRD experiment
performed on polycrystal-
line material the incident
X-ray beam is diffracted by
Sample innumerous crystallites in
specific 2Theta directions.
Incident Diffracted 2Theta
D2 PHASER – data- Beam Beams To record the exact
2Theta positions a narrow
slit in front of a point Plug’n Analyze: LYNXEYE detector: Desktop design:
quality, functionality Advanced 1-D detector setup
detector is required.
A simple domestic wall Intensity increases by a Minimum space
The LYNXEYE literally
and safety without LYNXEYE
provides more than 150
integrated slits, allowing
socket is all you need
No installation
factor of more than 150
100% working strips at
requirements
Handles for convenient
more than 150 2Theta delivery – guaranteed transportation
any compromises Micro Strip
positions to be recorded
simultaneously.
No alignment Energy discrimination
for sample fluorescence
Maximum X-ray safety
with radiation level
Sensor No instrument significantly below 1µSv/h
configuration suppression
1-D scanning and snap- Clearly visible warning
Instrument alignment – a sound base for accuracy! No infrastructure shot mode; 0-D mode and operating elements
Our D2 PHASER delivers uncompromis- No pre-installation Angular coverage Angular accuracy
ingly good and reliable analyses. The requirements > 5.5° 2Theta better than ±0.02°
0.040 Angular accuracy
strict quality standards of our entire 2Theta – guaranteed
≤ ± 0.02° 2Theta over the
product range are applied to the assem- 0.030 whole angular range –
bling, testing and certified safety of the guaranteed!
D2 PHASER! 0.020 + 0.020°
Why is this important?
Delta 2Theta [°]

We give you our word: Good Diffraction Practice and 0.010 Accurate and verifiable
Best Data Guarantee! instrument alignment is
0.000 a basic requirement for
Safety assurance: -0.010
accurate and reliable phase
Each instrument always complies with the world’s identification or structure
highest statutory requirements regarding X-ray safety, -0.020
analysis.
- 0.020°
machine and electrical safety. This certainty is
obtained after stringent scrutiny by independent -0.030
LYNXEYE Detector
institutions.
-0.040 Scintillation Counter
Two independent, fail-safe safety circuits and “X-ray
20.00 40.00 60.00 80.00 100.00 120.00 140.00
On” monitors guarantee that the most recent radia-
2Theta [°]
tion and personal safety regulations are observed.

Alignment guarantee: Unrivaled resolution

The D2 PHASER is pre-aligned at delivery. Every
5000 SRM 660a
single instrument must pass our strict test procedure,
Very small peak width of
which is based on the internationally accepted refer-
less than 0.05° 2Theta
ence material corundum. The corundum reference is 4000 All-in-one analytics: X-ray source: Island-mode:
obtained by high-resolution
supplied with the instrument, so you can check your XRD measurement of
instrument at any time. FWHM = 0.0421° 2Θ LaB6 (NIST SRM 660a) Simple sample loading Common sealed Internal cooling system
3000 with LYNXEYE detector; X-ray tube design
Counts

Industrial standard High speed ethernet

Detector guarantee: 0.1° divergence and 1.5° sample holders Low power load – connection
We guarantee that our 1-dimensional LYNXEYE is ab- Soller slit. no tube ageing
2000 Theta/Theta geometry, 2 USB ports
solutely faultless! This is due to Bruker AXS’ unique
Why is this important? horizontal samples Virtually infinite
detector design. By integrating the LYNXEYE detector Good instrument resolution Fully-fledged tube lifetime
in the D2 PHASER it becomes the fastest and most is a prerequisite to resolve
1000 integrated PC Cr, Co, Cu radiation
efficient desktop diffractometer in the world. overlapping diffraction
peaks in complex powder On-site and remote
The best in its class: the D2 PHASER. operation
0 patterns.
Shake on it!

29.90 30.10 30.30 30.50 30.70 30.90

2Theta [°]
8 9
 The ultimate in
ease of use –
D2 PHASER with
DIFFRAC.SUITE
1 X-ray analysis has never been easier!
1 Even inexperienced users produce perfect
3 measurements from the very beginning thanks
to the DIFFRAC.SUITE Easy-mode.
This is how X-ray analysis works in the Easy-mode:
4 Select COMMANDER plug-in, enter measurement time
and angular range and start. That’s all!
2 If a method has already been defined, it goes even faster:
2
Select START JOBS, click on Method and off you go!
It goes without saying that the software solutions of our
Easy-mode Expert-mode DIFFRAC.SUITE go beyond this. In Expert-mode the full
1 Real-time measurement 3 Full access to all settings: scope of functions is available. Using the COMMANDER,
display - User management CONFIGURATION and TOOLS plug-in the expert has control
- Database maintenance over administration of experimental databases, user rights
2 Straightforward selection
- Instrument configuration and all the way through to the Audit Trail. Everything on the
of scan parameters:
- Service tools system works in a safe, simple and reliable way.
- Angular range
- Step size 4 Full access to all
- Measurement time instrument parameters:
DIFFRAC.SUITE – performance made-to-measure:
- Drives easy for anyone to operate, full functionality
- Detector settings and control for experts. Integrated within a
- Generator settings networked world.
Our D2 PHASER is fully network capable. This enables
XRD experts in the central laboratory to access the data that All-in-one analysis
has been collected, no matter if they are next door or at the
other end of the world. Use the D2 PHASER where it is
needed – on-site – and you will save time and money!
The D2 PHASER is a full-blown diffractometer: its
measured data is fully compatible with all of our
Compatible with the entire DIFFRAC.SUITE solutions. The familiar world of
Bruker AXS’ Diffraction Solutions search/match and structure databases, EVA, TOPAS,…
family all of this is available to the XRD specialist for identifying,
quantifying and determining the characteristics of the
Fully network capable
crystalline phases.
Support of different user levels
and modes D2 PHASER – Welcome to the world of
Bruker AXS!
EVA – powerful phase identification
TOPAS – sophisticated quantitative
10 phase and structure analysis 11
 aim 02437
Technical Data

Geometry Theta / Theta

Max. useable angular range -3 … 160 ° 2Theta
(depending on detector)

Bruker AXS is continually improving its products and reserves the right change specifications without notice.
Accuracy ± 0.02° throughout the entire measuring range
Achievable peak width < 0.05°
Alignment Not needed, factory aligned
X-ray wavelengths Cr / Co / Cu, standard ceramic sealed tube

DOC-B88-EXS017. © 2013 Bruker AXS. Printed in the Federal Republic of Germany.

X-ray generation 30 kV / 10 mA
Detectors Scintillation counter
1-dimensional LYNXEYE
Instrument type Portable, desktop
Exterior Dimension 61 x 60 x 70 cm (h x d x w)
24.02” x 23.62” x 27.56”
Weight 95 kg
Power supply 90 – 250 V
External cooling water supply None
Computer Built-in
Optional additional PC connected via LAN interface
Interfaces 2 x USB and 1 x LAN

D2 PHASER™, US 7,852,983 B2 patent,

EU patent pending;
LYNXEYE™ EP 1 510 811 B1 patent.
DIFFRAC is a registered trademark of the
US Office of Patents and Trademarks.
Goniometer EP 2 112 505 A1.

Bruker AXS GmbH Bruker AXS Inc.

Karlsruhe . Germany Madison, WI . USA
Phone +49 (0)721-50997-0 Phone +1 (800) 234-XRAY
Fax +49 (0)721-50997-5654 Phone +1 (608) 276-3000
info@bruker-axs.de Fax +1 (608) 276-3006
info@bruker-axs.com
www.bruker.com