COA - Potassium Iodate

Certificate of Analysis – Certified Reference Material
Certipur® Potassium iodate
Product no.: 1.02404.0100

Lot no.: 192404P
Description of CRM: Potassium iodate
Expiry date: 2024/07/31

Storage: +15°C to +25°C tightly closed in the original container and protect from light and
moisture
Composition: Potassium iodate
Associated uncertainty, U=k .u

Analyte Certified value as mass fraction
(k=2) as mass fraction
Mass fraction 99.89 % ±0.09 %
Metrological traceability: Directly traceable to the suitable primary standard NIST SRM Potassium
dichromate 136f.
Measurement method: The certified mass fraction was determined by potentiometric titration with
sodium thiosulfate as titration solution. The certified value is based on a
molecular mass M = 213.995 g/mol dried substance.
Intended use: This volumetric standard is intended for standardisation of volumetric solutions
related to the chapter reagents of the Pharmacopoeia.
Instructions for handling The volumetric standard Potassium iodate must be dried at 130 °C for 2 hours
and correct use: before use.
By within-unit homogeneity studies a minimum weigh-in quantity of 100 mg was
determined.
Accreditation: Merck KGaA, Darmstadt, Germany is accredited by the German accreditation
authority DAkkS as registered reference material producer D-RM-15185-01-00
in accordance with ISO 17034 and registered calibration laboratory
D-K-15185-01-00 according to DIN EN ISO/IEC 17025.
Certificate issue date: September 3, 2019
Dipl.-Ing. Ayfer Yildirim

ISO 17034 ISO/IEC 17025 (Responsible QC Laboratory Manager)
Merck KGaA, 64271 Darmstadt, Germany, Tel.: +49 (0)6151 72-2440

EMD Millipore Corporation, 400 Summit Drive Burlington MA 01803, USA, Tel. +1-978-715-4321
Sigma-Aldrich Canada Co. or Millipore (Canada) Ltd., 2149 Winston Park, Dr. Oakville,
Ontario, L6H 6J8, Phone: +1 800-565-1400
Certificate Page 1 of 2 Certificate version 01

Health and safety Please refer to the Safety Data Sheet for detailed information about the nature of
information: any hazard and appropriate precautions to be taken.
Certification process details:

Certipur® Volumetric standards are prepared from high purity salts. Characterisation of Certipur® Volumetric
standards is carried out by the accredited quality control (QC) laboratory at Merck KGaA, Darmstadt, Germany
according to DIN EN ISO / IEC 17025 by measuring the mass fraction by potentiometric titration.
Homogeneity and stability studies are performed with the material according to the requirements of ISO 17034 and
ISO Guide 35.
Associated uncertainty:
The associated uncertainty UCRM reported with the certified values is calculated as combined expanded uncertainty
UCRM=k·uCRM in accordance with GUM and EA-4/02, with k=2 as the coverage factor for a 95% coverage probability.
The combined uncertainty uCRM is derived from combination of the squared uncertainty contributions:
u CRM = u 2 Characteri sation + u 2 Homogeneit y + u 2 Stability
ucharacterisation: is the uncertainty in accordance with DIN EN ISO/IEC 17025 which includes the
contributions of the primary reference material and the measuring system.
uhomogeneity: is the between-bottle variation in accordance with ISO 17034. The assessment
of homogeneity is performed by analysis of a representative number of
systematically chosen sample units.
ustability: is the uncertainty obtained from short-term and long-term stability in accordance
with ISO 17034. The stability studies are the basis for the quantification of the
expiry date of this volumetric standard for the unopened bottle.
For more detailed information please read the certification report on our website.
Certificate of analysis revision history:

Certificate version Date Reason for version
01 September 03, 2019 Initial version
The vibrant M, Supelco, Certipur and Sigma-Aldrich are trademarks of Merck KGaA, Darmstadt, Germany or its affiliates.
Detailed information on trademarks is available via publicly accessible resources.
© 2018 Merck KGaA, Darmstadt, Germany and/or its affiliates. All Rights Reserved.
Certificate Page 2 of 2 Certificate version 01

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Certificate of Analysis – Certified Reference Material

Certipur® Potassium iodate

Product no.: 1.02404.0100

Expiry date: 2024/07/31

Associated uncertainty, U=k .u

Mass fraction 99.89 % ±0.09 %

Dipl.-Ing. Ayfer Yildirim

Merck KGaA, 64271 Darmstadt, Germany, Tel.: +49 (0)6151 72-2440

Certificate Page 1 of 2 Certificate version 01

Certification process details:

Certificate of analysis revision history:

Certificate Page 2 of 2 Certificate version 01

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