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    MSC Syllabus

    Uploaded by

    Sanjeeb Sutradhar
    This document provides details of the M.Sc. Chemistry course "Spectroscopy-II" offered at I.K. Gujral Punjab Technical University. The course aims to provide knowledge of advanced spectroscopic techniques for molecular structure identification and analysis. It is divided into 4 units covering topics such as microwave, vibrational, Raman, photoelectron and electron paramagnetic resonance spectroscopies. The course outcomes are that students will learn fundamental and advanced concepts in various spectroscopic techniques and be able to apply them to solve structural problems in chemistry.

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    MSC Syllabus

    Uploaded by

    Sanjeeb Sutradhar
    38 views2 pages
    This document provides details of the M.Sc. Chemistry course "Spectroscopy-II" offered at I.K. Gujral Punjab Technical University. The course aims to provide knowledge of advanced spectroscopic techniques for molecular structure identification and analysis. It is divided into 4 units covering topics such as microwave, vibrational, Raman, photoelectron and electron paramagnetic resonance spectroscopies. The course outcomes are that students will learn fundamental and advanced concepts in various spectroscopic techniques and be able to apply them to solve structural problems in chemistry.

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    MSc Syllabus

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    This document provides details of the M.Sc. Chemistry course "Spectroscopy-II" offered at I.K. Gujral Punjab Technical University. The course aims to provide knowledge of advanced spectroscopic techniques for molecular structure identification and analysis. It is divided into 4 units covering topics such as microwave, vibrational, Raman, photoelectron and electron paramagnetic resonance spectroscopies. The course outcomes are that students will learn fundamental and advanced concepts in various spectroscopic techniques and be able to apply them to solve structural problems in chemistry.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    38 views2 pages

    MSC Syllabus

    Uploaded by

    Sanjeeb Sutradhar
    This document provides details of the M.Sc. Chemistry course "Spectroscopy-II" offered at I.K. Gujral Punjab Technical University. The course aims to provide knowledge of advanced spectroscopic techniques for molecular structure identification and analysis. It is divided into 4 units covering topics such as microwave, vibrational, Raman, photoelectron and electron paramagnetic resonance spectroscopies. The course outcomes are that students will learn fundamental and advanced concepts in various spectroscopic techniques and be able to apply them to solve structural problems in chemistry.

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    M.

    Sc (Chemistry), Choice Based Credit System, Batch 2018 and onwards

    I.K. GUJRAL PUNJAB TECHNICAL UNIVERSITY


    DEPARTMENT OF CHEMICAL SCIENCES
    Course Name M.Sc. Chemistry
    Subject Code: CHL414-18
    Subject Title: SPECTROSCOPY-II
    Contact Hours: L:4 T:0 P:0 Credits:4
    Examination 3
    Duration (hours)
    Objective(s): To provide knowledge of advanced spectroscopic techniques for
    identification and elucidation of structures of molecules

    Details of the Course

    Unit Contents Contact


    Hours
    I Microwave spectroscopy: Rigid and non-rigid rotator, Intensities 12
    of spectral lines, isotopic substitution effects, polyatomic linear
    and symmetric top molecules, Stark effect
    Vibrational Spectroscopy: Types of vibrations, overtones,
    combination and difference bands, Fermi resonance, group vibrations,
    Harmonic and anharmonic oscillators, absorptions of radiation by
    molecular vibrations, selection rules, force constant, frequency of
    vibrational transitions of HCl, vibrations in a polyatomic molecule,
    3N-6 and 3N-5 rules, Applications
    II Raman Spectroscopy: Introduction, vibrational-rotational Raman 10
    Spectra, selection rules, mutual exclusion principle, anisotropic
    polarizabilty, Stokes, anti-Stokes lines, vibrational Raman spectra
    of CO2 and H2O, polarised and depolarised Raman Lines.
    Mössbauer Spectroscopy: Basic principles, Spectral parameters and
    display, simple spin states (I 1/2, 3/2), higher spin states (I > 3/2),
    magnetic splitting, quadruple splitting, additive model application to
    57
    Fe, 119Sn
    III Nuclear Quadruple Resonance Spectroscopy: Introduction, 11
    experimental considerations, fundamentals of NOR spectroscopy,
    origin of EFG, measurement of energy differences between two
    nuclear spin states, the asymmetry parameter, effects of the
    magnetic field, interpretation of the spectra, application of NQR
    spectroscopy
    Photoelectron Spectroscopy-I: Introduction, photoelectron
    spectroscopy, chemical shift, X-ray photoelectron spectroscopy,
    molecular orbital diagrams of nitrogen and oxygen and their
    XPS spectra-ESCA.
    IV Photoelectron Spectroscopy-II: 12
    Ultraviolet photoelectron spectroscopy (UPS), PES spectrum of
    nitrogen sample, vibrational structure in the N2 UPS spectrum,
    chemical shifts in XPS, exchange splitting and shake up process.
    Electron Paramagnetic Resonance Spectroscopy: Principle,
    Spectral display, hyperfine splitting in isotropic systems involving
    more than one nucleus, Factors affecting magnitude of g values,
    I.K. Gujral Punjab Technical University, Kapurthala Page 38 of 77
    M.Sc (Chemistry), Choice Based Credit System, Batch 2018 and onwards

    zero field splitting and Krammer’s degeneracy, Spectrum of benzene


    radical anion, methyl radical, CH2OH, cyclopentedienyl,
    cycloheptatrienyl radical, pyrazine anion, pyrazine anion, Spectra
    of triplet states.

    Reference Books
    S.No. Author(s) Title of the Book Publisher/Year
    1 R.S. Drago Physical Methods in inorganic Affiliated East-West
    Chemistry Press (Section 1& 2)
    2nd Edition,
    Reinhold New York
    (1968)
    2 C. N. Banwell Fundamentals of Molecular McGraw-Hill, 1966
    Spectroscopy
    3 R. V. Parish NMR, NQR, EPR & Ellis Horwood,
    Mossbauer spectroscopy in London, 1990
    Inorganic Chemistry
    4 G. M. Barrow Introduction to Molecular McGraw-Hill
    Spectroscopy
    5 E. A. Ebsworth, S.Craddock Structural methods in Blackwell Scientific
    and D.W. H. Rankin Inorganic Chemistry Publications (1991)
    6 C.N.R. Rao and J.R. Ferraro Spectroscopy in Organic Vol. I, Academic
    Chemistry Press, 1971

    Course Outcomes and Mapping


    At the end of the course, the student will be able to
    CO1. Learn the fundamental and advanced concepts of Microwave, Infrared-
    Vibration-rotation Raman and infra-red Spectroscopy and their applications for
    chemical analysis
    CO2. Understand Electronic spectroscopy of different elements and simple
    molecules.
    CO3. Study the concepts and principles of Mössbauer Spectroscopy and its
    application.
    CO4. Apply Nuclear Quadruple Resonance and Electron Spin Resonance
    Spectroscopy for organic compounds analysis.
    CO5. Solve structural problems based on these techniques.
    PSO1 PSO2 PSO3 PSO4 PSO5 PSO6 PSO7
    CO1 3 3 3 1 3 3 3
    CO2 3 4 3 1 3 3 3
    CO3 3 4 2 - 3 4 3
    CO4 3 3 2 - 3 4 4
    CO5 3 5 2 2 4 4 3

    I.K. GUJRAL PUNJAB TECHNICAL UNIVERSITY

    I.K. Gujral Punjab Technical University, Kapurthala Page 39 of 77

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