Microwave Digestion

Sample Preparation at the Highest Level
speedwave XPERT
Sample preparation
2
speedwave XPERT
Microwave-assisted pressure digestion is
used as a sample preparation technique for
reliable elemental analysis in routine and
research laboratories alike. speedwave XPERT
is a universally applicable microwave digestion
system for the preparation of organic and
inorganic sample materials that impresses with
its reliability, safety, and economy.
Reliable digestions
■ Patented sensor technologies
■ No cross contamination
■ High reproducibility
Economic and durable

■ Low running costs
■ Low material wear and long service life of the vessels
■ Corrosion protection of the oven chamber
Maximum operational safety

■ Top-loading concept and electronic lid lock
■ Permanent ventilation of the oven chamber and removal
of generated acid fumes by the fume collection system
■ Automatic regulation in case of exothermic reactions
3
speedwave XPERT
Sample preparation at the highest level
4
Reliable, durable, and economic

With its innovative sensor concept speedwave XPERT guarantees reliable
results. The long product life of the vessels saves costs.
Reliable and reproducible digestions

speedwave XPERT sets new standards with its innovative
sensor technology and high-quality components. Real-
time temperature and pressure monitoring takes
place contactless for all vessel, which can be removed
individually after digestion. The round design of the oven
chamber homogenously distributes the microwave radiation
to achieve reproducible sample digestions. Due to the
minimal surface porosity of the vessels, the risk of cross-
contamination is significantly minimized.
Long life and low operating costs

The vessels of speedwave XPERT have an outstanding life-
time of up to 10,000 digestion cycles. Low material wear
and protection of the vessels against damage by optical
pressure and temperature control also ensure that you can
significantly reduce your running costs in sample prepara-
tion. The oven chamber is protected against corrosion by a
high-quality PFA coating.
sensor technologies of speedwave XPERT

5
Simple Operation with Maximum Safety

The self-monitoring system of speedwave XPERT ensures a safe laboratory
environment. The intuitive operation makes your daily lab routine easier.
Maximum safety through real-time monitoring User comfort and ease of operation
Working under demanding conditions requires an absolutely The innovative design of speedwave XPERT builds a
reliable system. The pressure-resistant furnace with connection of convenience and function.
an electrically locked swiveling lid is equipped with an A special feature of the microwave digestion system is its
integrated exhaust system to prevent reaction gases from top-loading concept. The swiveling lid allows the vessels
escaping. The furnace chamber is permanently ventilated. to be easily loaded from above, providing optimal operator
To reduce safety risks from irregular heating, a monitoring comfort. speedwave XPERT can be operated via a 7" touch
of the reaction parameters pressure and temperature is controller with a graphical user interface, as well as via
of particular importance. Thanks to real-time monitoring mobile devices or PC/laptop.
of the internal vessel pressure automatic regulation and,
if necessary, shutdown of processes, takes place in case of
exothermic reactions.
6
The Matching Set Up for Every Digestion

Various vessel types expand the range of applications and reduce operating
costs by using high-quality material.
The speedwave XPERT vessels are

manufactured with the highest quality
standards. They are made from high-
quality TFM-PTFE and impress through
reliability and an outstanding lifetime.
■ Vessel volumes from 40 to 100 mL

■ Manual opening and closing, without
additional tools
■ Safe and controlled release of
remaining pressure after opening
All vessels are equipped with a

rupture disc, which breaks when the
overpressure exceeds the tolerance
level. This allows an immediate
termination of the digestion run in
case of exothermic reactions. Thus,
expensive consequential damage is
avoided.
Additional liner systems expand the

field of applications of existing vessel
types. The vessels can be equipped
with inserts to support digestion of
small sample quantities or complex
samples.
Overview vessel options
DAP-40X DAP-60X DAP-100X DAK-100X
Volume 40 mL 60 mL 100 mL 100 mL
Working pressure 40 bar 40 bar 40 bar 100 bar
Test pressure 50 bar 50 bar 50 bar 130 bar
Operating temperature 230 °C 230 °C 200 °C 260 °C
Maximum temperature 260 °C 260 °C 230 °C 300 °C
Sample weight* 1 g (inorganic) 2 g (inorganic) 2 g (inorganic) 3 g (inorganic)

0.3 g (organic) 0.4 g (organic) 0.5 g (organic) 1 g (organic)
Options - DAQ-20H DAQ-22H
* Weights are reference values. Actual original sample weights may vary, depending on application and acid.
7
At Home in Many Industries

Due to its versatility, the speedwave XPERT is ideally suited for use in many
industries.
Food and agriculture Environment Pharma, chemistry, and metallurgy

A reproducible and efficient sample Environmental monitoring is mostly The speedwave XPERT is also used in
digestion is crucial for reliable analyses determined by standardized processes. the field of pharmaceuticals and life
to fulfill food safety requirements. The A reliable microwave digestion is science, as well as for chemical samples.
speedwave XPERT is suitable for the required in sample preparation for the Areas of application are, for example,
digestion of the following samples: analysis of emissions, water, or sludges. the digestion of
■ Beverages You can rely on speedwave XPERT for ■ Blood, hair, bones
■ Animal products the digestion of ■ Products with high fat content
■ Milk products ■ Filter/emissions ■ Cosmetics
■ Fruit ■ Sediments ■ Lactose and dextrose
■ Cereals ■ Soil and sludge ■ Polymers (e.g., PET, polyester)
■ Nutrients ■ Water and wastewater ■ Metals and alloys
■ Animal feed ■ Ash
■ Lactose ■ Minerals, rocks, and concrete
Our Portfolio for Optical Spectrometry and Mass Spectrometry
novAA 800 series contrAA 800 series ZEEnit series

The powerful entry-level AAS for routine Powerful high-end AAS for efficient and AAS with Zeeman background correction –
laboratories. sensitive multielement analysis for research proven and robust trace analysis for
and everyday lab use. demanding sample matrices.
PlasmaQuant MS series PlasmaQuant 9100 series

High-performance ICP-MS with unmatched ICP-OES spectrometer with high-resolution
sensitivity and low operating costs for trace array technology for the elemental analysis of
and ultra-trace analyses. liquid samples.
Headquarters
© Analytik Jena GmbH
Version 1.0 · en · 02/2021
888-51002-2-B
Analytik Jena GmbH Pictures: Analytik Jena GmbH, Berghof Products + Instruments GmbH
Konrad-Zuse-Str. 1 Subjects to changes in design and scope of delivery as well as further technical development!
07745 Jena ⋅ Germany
Phone +49 3641 77 70

Fax +49 3641 77 9279
info@analytik-jena.de
www.analytik-jena.de

Microwave Digestion

Uploaded by

Copyright:

Available Formats

Microwave Digestion

Uploaded by

Document Information

Original Title

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

Microwave Digestion

Uploaded by

Copyright:

Available Formats

Sample Preparation at the Highest Level

Economic and durable

Maximum operational safety

Reliable, durable, and economic

Reliable and reproducible digestions

Long life and low operating costs

sensor technologies of speedwave XPERT

Simple Operation with Maximum Safety

The Matching Set Up for Every Digestion

The speedwave XPERT vessels are

■ Vessel volumes from 40 to 100 mL

All vessels are equipped with a

Additional liner systems expand the

Overview vessel options

DAP-40X DAP-60X DAP-100X DAK-100X

Volume 40 mL 60 mL 100 mL 100 mL

Working pressure 40 bar 40 bar 40 bar 100 bar

Test pressure 50 bar 50 bar 50 bar 130 bar

Operating temperature 230 °C 230 °C 200 °C 260 °C

Maximum temperature 260 °C 260 °C 230 °C 300 °C

Sample weight* 1 g (inorganic) 2 g (inorganic) 2 g (inorganic) 3 g (inorganic)

Options - DAQ-20H DAQ-22H

At Home in Many Industries

Food and agriculture Environment Pharma, chemistry, and metallurgy

Our Portfolio for Optical Spectrometry and Mass Spectrometry

novAA 800 series contrAA 800 series ZEEnit series

PlasmaQuant MS series PlasmaQuant 9100 series

Phone +49 3641 77 70

You might also like