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भारतीय मानक IS 1202 : 2021

Indian Standard

तार और बिटुमिनी सामग्री

की परीक्षण विधियाँ — आपेक्षिक गुरुत्व
ज्ञात करना
( दसू रा पनु रीक्षण )

Methods for Testing Tar and

Bituminous Materials —
Determination Of Specific Gravity
( Second Revision )

ICS 75.140

© BIS 2021

भारतीय मानक ब्रयू ो

B U R E A U O F I N D I A N S TA N D A R D S
मानक भवन, 9 बहादरु शाह ज़फर मार्ग, नई िदल्ली – 110002
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI-110002
         www.bis.gov.in  
www.standardsbis.in

December 2021  Price Group 3

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Bitumen, Tar and Related Products Sectional Committee, PCD 06

FOREWORD
This Indian Standard (Second Revision) was adopted by the Bureau of Indian Standards after the draft finalized
by the Bitumen, Tar and Related Products Sectional Committee had been approved by the Petroleum, Coal and
Related Product Division Council.
This standard was originally published in 1958 as ‘Methods for testing tar and bituminous materials —
Determination of Specific gravity and subsequently revised in 1978. ‘Methods for testing tar and bituminous
materials’ was originally published as series of 22 standards in the form of a booklet, as listed below:
IS No. Title

1201 : 2004 Sampling

1202 : 1978 Determination of specific gravity
1203 : 1978 Determination of penetration
1204 : 1978 Determination of residue of specified penetration
1205 : 1978 Determination of softening point
1206 (Part 1) : 1978 Determination of viscosity: Part 1 Industrial viscosity
1206 (Part 2) : 1978 Determination of viscosity: Part 2 Absolute viscosity
1206 (Part 3) : 1978 Determination of viscosity: Part 3 Kinematic viscosity
1207 : 1978 Determination of equiviscous temperature (EVT)
1208 : 1978 Determination of ductility
1209 : 1978 Determination of flash point and fire point
1210 : 1978 Float test
1211 : 1978 Determination of water content dean and stark method
1212 : 1978 Determination of loss on heating
1213 : 1978 Distillation test
1214 : 1978 Determination of matter insoluble in benzene (WITHDRAWN due to toxic
nature of benzene)
1215 : 1978 Determination of matter insoluble in toluene
1216 : 1978 Determination of solubility in carbon disulphide trichloroethylene
1217 : 1978 Determination of mineral matter ash
1218 : 1978 Determination of phenols
1219 : 1978 Determination of naphthalene
1220 : 1978 Determination of volatile matter content
However, the Committee responsible for the formulation of standards in the field of bitumen, tar and related
products decided to publish these Indian standards separately for each test so as to make it user friendly.
Accordingly, second revision of the standard, was taken up to formulate individual standard on determination
of specific gravity. In this revision, the term-specific gravity term has been redefined as the ratio of the mass of
a given volume of the substance to the mass of an equal volume of water, at the same temperature. Formula for
calculation of density, based on specific gravity measurements has also been provided.
The Composition of the Committee responsible for formulation of this standard is given at Annex A.
In reporting the results of a test or analysis made in accordance with this standard, if the final value, observed or
calculated, is to be rounded off, it shall be done in accordance with IS 2 : 1960 ‘Rules for rounding off numerical
values ( revised )’.
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IS 1202 : 2021

Indian Standard
METHODS FOR TESTING TAR AND BITUMINOUS
MATERIALS — DETERMINATION OF
SPECIFIC GRAVITY
( Second Revision )

1 SCOPE 3.2 Apparatus

This standard covers the methods for the determination Specific gravity bottles of 50 ml capacity shall be used.
of specific gravity of asphalt, bitumen, bituminous One of the two types of specific gravity bottles, namely
products, road tar, coal tar, coal tar pitch, creosote and (a) the ordinary capillary type specific gravity bottle
anthracene oil. with a neck of 6 mm diameter (see Fig. lA) and (b)
the wide-mouthed capillary type specific gravity bottle
2 TERMINOLOGY (see Fig. IB) with a neck of 25 mm diameter shall be
used.
For the purpose of this standard, the following definition
and those given in IS 334 : 1965 shall apply. The stopper shall be provided with a bore 1.0 to 2.0 mm
in diameter centrally located in reference to the vertical
2.1 Specific Gravity — The ratio of the mass of a given axis. The top surface of the stopper shall be smooth
volume of the substance to the mass of an equal volume and substantially plain and the lower surface shall be
of water, at the same temperature. concave in order to allow all air to escape through the
bore. The height of the concave section shall be 4.0 to
2.1.1 The specific gravity of bitumens, fluxed native 6.0 mm at the centre.
asphalt, road tars, coal tar pitch and blown bitumen
shall be determined at 25 °C and that of creosote oil 3.2.1 The ordinary specific gravity bottle shall be used
and anthracene oil at 38 °C and shall be expressed as for materials which remain absolutely fluid at 25 °C
specific gravity 25 °C/25 °C or 38 °C/38 °C. while the wide mouth capillary type shall be used for
materials which remain semisolid at 25 °C.
3 METHOD A (PYKNOMETER METHOD)
3.2.2 Constant Temperature Bath — A water bath
3.1 This method covers the determination of specific having a depth greater than that of Pyknometer capable
gravity for semisolid bitumen road tars and creosote of being maintained within 0.2 °C of the desired
and anthracene oil. temperature.

Fig. 1A Ordinary Capillary Type Fig. 1B Wide-Mouthed Capillary Type

Specific Gravity Bottle Specified Gravity Bottle

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IS 1202 : 2021

3.2.3 Bath Thermometer — It shall conform to the 3.4 Calculation

following requirements: Calculate the specific gravity of the material as follows:
Characteristic Requirement a) Specific gravity (solids and semisolids) =
Range 0 to 44 °C c−a
Least Count 0.1 °C (b − a ) − (d − c)

3.3 Procedure e−a

b) Specific gravity (Liquids) =
Clean, dry and weigh the specific gravity bottle b−a
where
together with the stopper (a). Fill it with freshly boiled
and cooled distilled water and insert the stopper firmly. a = mass of the specific gravity bottle,
Keep the bottle up to its neck for not less than half b = mass of the specific gravity bottle filled with
an hour in a beaker of distilled water maintained at a distilled water,
temperature of 27.0 ± 0.l °C or any other temperature c = mass of the specific gravity bottle about half
at which specific gravity is to be determined; wipe all filled with the material,
surplus moisture from the surface with a clean, dry
d = mass of the specific gravity bottle about half
cloth and weigh again (b). After weighing the bottle
filled with the material and the rest with
and water together (b) the bottle shall be dried again.
distilled water, and
3.3.1 In the case of solids and semisolids, bring a small e = mass of the specific gravity bottle completely
amount of the material to a fluid condition by gentle filled with the material.
application of heat, care being taken to prevent loss c) Calculate density to the nearest 0.001 as follows
by evaporation. When the material is sufficiently fluid,
pour a quantity into the clean, dry specific gravity Density = Specific gravity × WT.
bottle mentioned at 3.3 to fill at least half. Slightly Here, WT is the density of water at the test
warm the bottle before filling. Keep the material away temperature.
from touching the sides above the final level of the Use density of water at 25 °C as 997.0 kg/m3 and at
bottle and avoid the inclusion of air bubbles. The use of 15.6 °C as 999.0 kg/m3 and at 38 °C as 993.1kg/ m3
a small funnel will prevent contamination of the neck
of the bottle. To permit escape of entangled air bubbles, 3.5 Precision
allow the partly filled bottle to stand for half an hour With samples which are neither very volatile nor very
at a temperature between 60-70 °C, then cool to I the viscous and using a pyknometer of at least 25 ml
specified temperature and weigh with the stopper (c). capacity, the results of duplicate tests should not differ
3.3.2 Fill the specific gravity bottle containing the by the following:
bituminous binders with freshly boiled distilled water Repeatability Reproducibility
placing the stopper loosely in the specific gravity
bottle. Do not allow any air bubble to remain in the 0.002 0.005
specific gravity bottle. Place the specific gravity bottle 3.6 Precautions
in the water bath and press the stopper firmly in place.
Allow the specific gravity bottle to remain in the water When making the specific gravity determination, it is
bath for a period of not less than 30 min. Remove the important that:
specific gravity bottle from the water bath, wipe all a) only freshly boiled and cooled distilled water shall
surplus moisture from the surface with a clean dry cloth be used;
and weigh it along with the stopper. b) at no time of weighing shall the temperature of
3.3.3 In the case of liquids such as creosote and the apparatus be allowed to exceed the specified
anthracene oil, fill the bottle up to the brim and insert temperature;
the stopper firmly. Keep the filled bottle for not less than c) precautions shall be taken to prevent expansion
half an hour in a beaker of distilled water maintained at and over-flow of the contents resulting from the
a temperature of 27.0 ± 0.1 °C, remove the bottle from heat of the hand when wiping the surface of the
the beaker, wipe all surplus water from the surface with apparatus;
a clean, dry cloth and weigh again. d) all air bubbles shall be eliminated in filling the
apparatus and inserting the stopper;

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IS 1202 : 2021

e) weighing shall be done quickly after filling the treated. Take precautions to prevent the inclusion of air
apparatus and shall be accurate to 0.1 mg; and bubbles. The hot material should be slightly more than
f) to prevent breakage of the apparatus when cleaning that required to fill the mould, and when cool, the excess
after a determination has been made upon a very may be cut off with a hot spatula. Remove the specimen
viscous of semisolid material, it is advisable to from the mould when cooled to room temperature.
warm it in an oven at a temperature not above 4.4 Procedure
100 °C, until most of the material is poured out
and then to swab it with a piece of soft cloth or Tare the balance first with a piece of fine waxed silk
cotton waste. When cool, it may be finally rinsed thread sufficiently long to reach from the hook on one
with carbon disulphide, benzol or other solvent of the pan supports to the rest. Attach the test specimen
and wiped clean. to the thread. So as to be suspended about 25 mm
above the straddle from the hook on the pan support,
4 METHOD B (BALANCE METHOD) and weigh to the nearest 0.1 mg. Weigh the specimen,
still suspended by thread, and completely immersed in
4.1 This test method is intended for the determination of freshly boiled and cooled distilled water at 27.0 ± 0.1 °C,
the specific gravity of semi-solid and solid bituminous to the nearest 0.1 mg, adhering air bubbles being first
materials by weighing in air and in water. removed with a fine wire.
4.2 Apparatus 4.5 Calculation
4.2.1 Balance Analytical Calculate the specific gravity of the material as follows:
a
4.2.2 Thermometer — As given in Method A. Specific gravity =
a −b
where
4.2.3 Balance Straddle — A pan straddle of convenient
size to support a beaker and permit determination of the a = mass of the dry specimen, and
weight of the specimen in water (see Fig. 2). b = mass of the specimen when immersed in
distilled water.
4.2.4 Thread — A length of fine, waxed, silk thread.
4.6 Report
4.2.5 Brass Moulds — Cubical, measuring
approximately 20 mm on each edge. Report the specific gravity to the nearest 0.001 at
25 °C/ 25 °C. The buoyancy/correction in this case is
4.3 Test Specimen negligible.
The test specimen shall be a cube of the material 4.7 Precision
measuring approximately 20 mm on each edge. Prepare
the specimen by melting a small sample of the material The duplicate results shall not differ by more than the
by gentle application of heat, taking care to prevent following:
loss by evaporation, and pouring the material when Size of Sample Repeatability Reproducibility
sufficiently fluid into a 20 mm brass cubical mould
that has been treated with a 1 : 1 mixture of glycerine 5 g or larger 0.005 0.007
and dextrin and placed on a brass plate previously so

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IS 1202 : 2021

Fig. 2 Analytical Balance Equipment with Pan Straddle

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IS 1202 : 2021

ANNEX A
( Foreword )
COMMITTEE COMPOSITION
Bitumen, Tar and Related Products Sectional Committee, PCD 06

Organization Representative(s)

CSIR-Central Road Research Institute, New Delhi Prof Satish Chandra (Chairman)

Airports Authority of India, New Delhi Shri Suprio Gosh

Shri Vinod Kumar Sharma (Alternate)
Bharat Petroleum Corporation Limited, R & D Ms Sonal Maheshwari
Centre, Noida
Bharat Petroleum Corporation Limited, Mumbai Shri C. Shanmuganathan
Bharat Petroleum Corporation Limited, Kochi Shri Adalazhagan K.
Refinery
Birla Institute of Technology and Science, Pilani Shri Sridhar Raju
CSIR-Central Building Research Institute, Roorkee Ms Rajani Lakhani
CSIR-Central Road Research Institute, New Delhi Dr Ambica Behl
CSIR-North East Institute of Science and Technology, Dr Shashi D. Baruah
Jorhat Dr B. P. Baruah (Alternate)
Central Public Works Department, New Delhi Shri Divakar Agrawal
Chennai Petroleum Corporation Limited, Chennai Shri H. Ramakrishnan
Dr V. Selvavathi (Alternate)
Dilip Buildcon Limited, Bhopal Shri B. B. Kameswara Rao
Shri Anush K.C. (Alternate)
Directorate General Border Roads, New Delhi Shri Umakant Kumar
Shri Ashok Kumar (Alternate)
Directorate General of Quality Assurance, Ministry Shri Vivekanand
of Defence, New Delhi Shri Anil Kumbhare (Alternate I)
Shri Sachin Vinayak Zope (Alternate II)
Engineer in Chief Branch, New Delhi Shri O. P. Srivatava
Shri R. Jayaprasad (Alternate)
G R Infra-Projects Limited, Gurugram Shri U. C. Gupta
G P Global Asphalt Private Limited, New Delhi Shri Rajesh Kumar Jain
Highways Research Station, Chennai Shri T. S. Sundar
Shri R. Geetha (Alternate)
Hindalco Industries Limited, Mumbai Shri Harshad Kumar Pandit
Hindustan Colas Private Limited, Mumbai Shri K. G. Ranganatha
Shri T. K. Subhaash (Alternate)
Hindustan Petroleum Corporation Limited (HP Green Shri B. Ravi
R & D Center), Bengaluru Shri K. R. Krishna (Alternate)
Hindustan Petroleum Corporation Limited, Mumbai Shri Santosh Dhaku Bhogale

Indian Institute of Petroleum, Dehradun Shri Manoj Srivastava

Dr Kamal Kumar (Alternate)
Indian Institute of Technology Bombay, Mumbai Dr Dharamveer Singh

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IS 1202 : 2021

Organization Representative(s)

Indian Institute of Technology Delhi, New Delhi Dr Aravind Swamy

Indian Institute of Technology Madras, Chennai Dr J. Murali Krishnan
Dr A. Veeraraghavan (Alternate)
Indian Institute of Technology Roorkee, Roorkee Shri Sham Sundar Ravindranath (Alternate)
Indian Oil Corporation (R & D Centre), Faridabad Shri Dhanesh Kumar
Dr I. Devotta (Alternate)
Indian Oil Corporation Limited-Refineries and Shri S. B. Lahkar
Pipelines Division, New Delhi Shri K. Medhi (Alternate I)
Ms K. Geethashree (Alternate II)
Indian Oil Corporation Limited, New Delhi Shri N. S. Raman
Indian Road Congress, New Delhi Shri S. K. Nirmal
Shri R. V. Patil (Alternate)
Indian Oil Total Private Limited, Mumbai Shri Gaurav Gogne
Dr Pankaj Kumar Jain (Alternate)
Ministry of Road Transport and Highways, Shri Varun Aggarwal
New Delhi Shri Sanjeev Kumar (Alternate)
National Rural Roads Development Agency, Shri B. C. Pradhan
New Delhi
National Test House, Kolkata Shri Vinay Kumar
Nayara Energy Limited, Mumbai Shri Dhiraj Gondalia
Shri Mriganka Tarafdar (Alternate)
Om Infracon Private Limited, Guwahati Shri A. N. Das
Shri Manish Bajaj (Alternate I)
Shri Digambar Deka (Alternate II)
Ooms Polymer Modified Bitumen Private Limited, Shri B. R. Tyagi
Gurugram Shri Palash Kathal (Alternate)
Shell Bitumen India Private Limited, Gurugram Shri Nilanjan Sarker
Zydex Industries Limited Shri Vishal Saluja
Shri Himanshu Agarwal (Alternate I)
Shri Ajay Ranka (Alternate II)
In Personal Capacity Dr P. S. Kandhal
BIS Director General Shrimati Nagamani T., Scientist ‘E’ and Head (PCD)
[ Representing Director General ( Ex-officio ) ]

Member Secretary
Shrimati D. Uma
Scientist ‘D’ (PCD), BIS

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This Indian Standard has been developed from Doc No.: PCD 06 (16138).

Amendments Issued Since Publication

Amend No. Date of Issue Text Affected

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