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    24 Mscphy

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    24 Mscphy

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    of 2

    ELECTIVE - LIST 1 – 4.

    CRYSTAL GROWTH AND THIN FILMS

    Inst. Hours
    Category

    Credits

    Marks
    Subject
    Subject Name L T P
    Code

    CRYSTAL GROWTH AND THIN


    23UPPHY1E04 Elective 4 1 0 3 5 75
    FILMS

    Learning Objectives
     To acquire the knowledge on Nucleation and Kinetics of crystal growth
     To understand the Crystallization Principles and Growth techniques
     To study various methods of Crystal growth techniques
     To understand the thin film deposition methods
     To apply the techniques for the Characterization of materials

    UNITS Course Details


    Basic Concepts, Nucleation and Kinetics of growth Ambient phase
    UNIT I: equilibrium - Super saturation - Equilibrium of finite phases equation of
    CRYSTAL GROWTH Gibbs - Thomson -Types of Nucleation - Formation of critical Nucleus -
    KINETICS Classical theory of Nucleation - rate of Nucleation - epitaxial growth -
    Growth mechanism and classification - Kinetics of growth of epitaxial
    films
    Crystallization Principles - Solvents and solutions - Solubility diagram -
    UNIT II: Super solubility - Expression for super saturation - Metastable zone and
    CRYSTALLIZATION introduction period - Miers TC diagram - Solution growth - Low and high
    PRINCIPLES and temperatures solution growth - Slow cooling and solvent evaporation
    Solution Growth methods - Constant temperature bath as a Crystallizer.
    Gel, Melt and Vapour growth techniques Principle of Gel techniques -
    UNIT III: Various types of Gel - Structure and importance of Gel - Methods of Gel
    GEL, MELT AND growth and advantages - Melt techniques - Czochralski growth - Floating
    VAPOUR GROWTH zone - Bridgeman method - Flux growth - Hydrothermal growth - Vapour
    phase growth - Physical vapour deposition - Chemical vapour deposition.
    Thin film deposition methods of thin film preparation, Thermal
    UNIT IV: evaporation, Electron beam evaporation, pulsed LASER deposition,
    THIN FILM Cathodic sputtering, RF Magnetron sputtering, MBE, chemical vapour
    DEPOSITION deposition methods, Sol Gel spin coating, Spray pyrolysis, Chemical bath
    METHODS deposition.
    X–ray diffraction – Powder and single crystal – Fourier transform infrared
    UNIT V:
    analysis – Transmission– UV-Vis-NIR spectrometer – Vickers micro
    CHARACTERIZATION
    hardness –Basic principles and operations of SEM and TEM- Nonlinear
    TECHNIQUES
    Optical phenomenon (qualitative) - Kurtz powder SHG method.
    Extended Professional
    Component (is a part of
    Expert Lectures, Online Seminars - Webinars on Industrial
    internal component only.
    Interactions/Visits, Competitive Examinations, Employable and
    Not to be included in the
    Communication Skill Enhancement, Social Accountability and Patriotism
    external examination
    question paper)

    1. Crystal Growth for Beginners: Fundamentals of Nucleation, Crystal


    Growth and Epitaxy, V. Markov, 2nd edition, 2004
    2. Thin Film Fundamentals, A. Goswami, New Age, New Delhi, 2008
    3. Modeling of Crystal Growth Rates from Solution, M. Ohora and R. C.
    Reid, 1973
    TEXT BOOKS
    4. Crystal Growth from High Temperature Solution, D. Elwell and H. J.
    Scheel, 1976
    5. Crystal Growth in Gels, Heinz K. Henish, Cambridge University Press,
    USA, 1973

    1. Crystal Growth Process, J.C. Brice, John Wiley, New York, 1986
    2. UGC Summer School Notes, P. Ramasamy and F. D. Gnanam, 1983
    3. Crystal Growth Processes, P. Santhana Raghavan and P. Ramasamy,
    REFERENCE BOOKS
    KRU Publications, 2000
    4. Crystal Growth, H.E. Buckley, John Wiley and Sons, New York, 1951
    5. Crystal Growth, B.R. Pamplin, Pergamon Press, London, 1980

    1. https://www.youtube.com/playlist?list=PLbMVogVj5nJRjLrXp3kMtrI
    O8kZl1D1Jp
    2. https://www.youtube.com/playlist?list=PLFW6lRTa1g83HGEihgwcy7
    Ke TLUuBu3WF
    WEB SOURCES 3. https://www.youtube.com/playlist?list=PLADLRin7kNjG1Dlna9MDA5
    3 CMKFHPSi9m
    4. https://www.youtube.com/playlist?list=PLXHedI
    xbyr8xIl_KQFs_R_oky3Yd1Emw
    5. https://www.electrical4u.com/thermal-conductivity-of-metals/

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