DOC022.97.

90368

DR 6000
04/2013, Edition 3

Basic User Manual en

Manual básico del usuario es
Manuel d'utilisation de base fr
基本ユーザー マニュアル ja
기본 사용 설명서 ko
Manual do utilizador básico pt
基本用户手册 zh
 Technical data Performance specifications
Changes reserved! Zero point at 546 nm for 10 hours ≤ 0.0034 Abs Long-term stability
5000 measurement values (result, date, time, sample
Performance specifications ID, user ID) Data log
50 scans, 50 time scans
Transmittance (%), Absorbance and Concentration Operating mode
200 User programs
Deuterium lamp (UV) and halogen lamp (visual
Source lamp Physical and environmental specifications
range)
190–1100 nm Wavelength range 500 mm (19.69 in) Width

± 1 nm (wavelength range 200–900 nm) Wavelength Accuracy 215 mm (8.46 in) Height

Wavelength 460 mm (18.11 in) Depth

< 0.1 nm
reproducibility
11 kg (24.25 lb) Weight
0.1 nm Wavelength resolution
10–40 °C (50–104 °F), maximum 80% relative
Ambient operating
Automatic Wavelength calibration humidity
requirements
(without condensate formation)
Automatic, based on method selection Wavelength selection –25–60 °C (–13–140 °F), maximum 80% relative
Ambient storage
humidity
900 nm/min (in 1-nm steps) Scanning speed requirements
(without condensate formation)
2 nm (1.5–2.9 nm at 656 nm, 1 nm for D2 line) Spectral bandwidth Additional technical data
Photometric measuring 100–240 V/50–60 Hz Power connection
± 3 Abs (wavelength range 200–900 nm)
range
150 VA Power consumption
5 mAbs at 0.0–0.5 Abs
Photometric accuracy
< 1% at 0.50–2.0 Abs at 546 nm T 2A H; 250 V (2 units) Fuse
< 0.5% to 2 Abs Use only shielded cable with maximum length of 3 m:
Photometric linearity
≤ 1% at > 2 Abs with neutral glass at 546 nm 2x USB type A
KI solution at 220 nm 1x USB type B
Stray light
< 3.3 Abs / < 0.05% Interfaces
Use only shielded cable (for example STP, FTP, S/
190–199 nm +/- 0.0100 Abs FTP)
200–349 nm +/- 0.0054 Abs Photometric drift against with maximum length of 20 m:
blank reading
350–899 nm +/- 0.0034 Abs 1x Ethernet
(30-min baseline stable)
900–1100 nm +/- 0.0100 Abs IP20 with closed cell compartment cover Housing rating

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 Performance specifications General information
Class I Protection class
Safety notes
This product has been tested to the requirements of
CAN/CSA-C22.2 No. 61010-1, second edition, Read the entire user manual carefully before you unpack, set up or
including Amendment 1, or a later version of the operate the device. Observe all danger and warning notes. Non-
same standard incorporating the same level of testing observance could lead to serious injury of the operator or to damage to
requirements. the device.
2 Pollution Degree To make sure that the protection provided by this instrument is not
impaired, do not use or install this instrument in any manner other than
II Installation Category that specified in these operating instructions.
2000 m (6560 ft) Maximum Altitude

DANGER
Indicates a potentially or imminently hazardous situation that, if not avoided, can
result in death or serious injury.

WA R N I N G
Indicates a potentially or imminently dangerous situation that, if it is not avoided,
can lead to death or to serious injuries.

CAUTION WA R N I N G
Indicates a possible dangerous situation that can have minor or moderate injuries Indicates a situation that, if it is not avoided, can lead to damage to the device.
as the result. Information that requires special emphasis.

Note: Information that supplements aspects from the main text.

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Warning labels Safety around source lamps
Observe all marks and labels that are attached to the device. Non- The source lamps are operated at high temperatures.
observance may result in personal injury or damage to the device. For To avoid the risk of electrocution, make sure the instrument is
symbols attached to the device, corresponding warning notes are found disconnected from the power source before changing the lamps.
in the user manual.

This symbol may be attached to the device and references the

operation- and/or safety notes in the user manual. CAUTION
Health hazard caused by ozone.
Hazardous levels of ozone can be generated when the UV lamp is not cooled.
This symbol on the device is an indication of hot surfaces.

Electrical equipment marked with this symbol may as of August 12,

WA R N I N G
2005 Europe-wide no longer be disposed of in unsorted house or Health hazard caused by UV light.
industrial waste. According to valid provisions (EU Directive 2002/96/ UV-Licht can cause eye and skin damage. Protect eyes and skin from direct
EC), from this point consumers in the EU must return old electrical exposure to UV light.
devices to the manufacturer for disposal. This is free for the Do not look directly at an energized lamp without UV safety glasses.
consumer.
Note: Contact the manufacturer or supplier to find out how
you can return worn out devices, electrical accessories CAUTION
supplied by the manufacturer and all auxiliary articles for Burn hazard, allow the lamp(s) to cool down for at least 30 minutes before they
correct disposal or recycling. are serviced/replaced.

RFID module (not available on all models)

RFID technology is a radio application. Radio applications are subject to
WA R N I N G national conditions of authorization. The use of the DR 6000 (model with
The manufacturer is not responsible for any damages due to misapplication or RFID module) is currently permitted in the following countries: EU, CH,
misuse of this product including, without limitation, direct, incidental and NO, HR, RS, MK, TR, CY, US, CA, AU, NZ. We point out that the use of
consequential damages, and disclaims such damages to the full extentpermitted
under applicable law.
the DR 6000 (model with RFID module) outside of the named regions
may contravene national law. The manufacturer reserves the right also
The user is solely responsible to identify critical application risks and install
appropriate mechanisms to protect processes during a possible equipment
to obtain authorization in other countries. For questions about use in
malfunction. your area, please contact your distributor.

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 The DR 6000 contains an RFID module for the reception and Changes or modifications to this equipment not expressly approved by
transmission of information and data. The RFID module operates with a the party responsible for compliance could void the user's authority to
frequency of 13.56 MHz. operate the equipment.
This equipment has been tested and found to comply with the limits for a
WA R N I N G Class A digital device, pursuant to Part 15 of the FCC rules. These limits
are designed to provide reasonable protection against harmful
The spectrophotometer may not be used in dangerous environments.
interference when the equipment is operated in a commercial
The manufacturer and its suppliers reject any express or indirect guarantee for
use with high-risk activities.
environment. This equipment generates, uses and can radiate radio
frequency energy and, if not installed and used in accordance with the
Follow the following safety information, in addition to any local guidelines instruction manual, may cause harmful interference to radio
in force. communications. Operation of this equipment in a residential area is
likely to cause harmful interference, in which case the user will be
Safety information for the correct use of the instrument: required to correct the interference at their expense. The following
• Do not operate the instrument in hospitals or comparable techniques can be used to reduce interference problems:
establishments in the vicinity of medical equipment, such as pace 1. Disconnect the equipment from its power source to verify that it is
makers or hearing aids. or is not the source of the interference.
• Do not operate the instrument near highly flammable substances, 2. If the equipment is connected to the same outlet as the device
such as fuels, highly combustible chemicals and explosives. experiencing interference, connect the equipment to a different
outlet.
• Do not operate the device near combustible gases, vapors or dust.
3. Move the equipment away from the device receiving the
• Do not vibrate or jolt the instrument. interference.
• The instrument can cause interference in immediate proximity to 4. Reposition the receiving antenna for the device receiving the
televisions, radios and computers. interference.
• Do not open the instrument. 5. Try combinations of the above.
• Guarantee is voided if the instrument is not used in accordance with Chemical and Biological Safety
the guidelines present in this document.
Certification (integrated RFID module)
FCC ID: YUH-QR15HL DANGER
Potential danger with contact with chemical/biological substances.
IC: 9278A-QR15HL Working with chemical samples, standards and reagents can be dangerous.
This device complies with Part 15 of the FCC rules and Industry Canada Make yourself familiar with the necessary safety procedures and the correct
license exempt RSS standard(s). handling of the chemicals before use and read and follow all relevant safety data
sheets.
Operation is subject to the following two conditions:
Normal operation of this device may require the use of chemicals or
1. this device may not cause interference, and samples that are biologically unsafe.
2. this device must accept any interference, including interference that
may cause undesired operation of the device.

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• Observe all cautionary information printed on the original solution Installation
containers and safety data sheets prior to their use.
• Dispose of all consumed solutions in accordance with the local and
national regulations and laws. WA R N I N G
• Select the type of protective equipment suitable to the concentration Electrical dangers and fire hazard.
and quantity of the dangerous material being used. Only use the supplied power cable.
Only qualified experts may perform the tasks described in this section of the
Product overview manual, while adhering to all locally valid safety regulations.

The DR 6000 is a UV-VIS-spectrophotometer with a wavelength range

of 190 to 1100 nm. The visible spectrum (320 to 1100 nm) is covered by
a halogen lamp and a deuterium lamp produces the light in the
WA R N I N G
Removable power cables must not be replaced with inadequately dimensioned
ultraviolet spectrum (190 to 360 nm). power cables.
The instrument is supplied with a complete range of application
programs and supports several languages. Unpacking the instrument
The DR 6000 spectrophotometer contains the following programs and The DR 6000 spectrophotometer package is supplied with the following
operating modes: items:
• Stored programs (pre-installed tests) • DR 6000 spectrophotometer
• Barcode Programs • Dust cover
• User Programs • USB dust cover, fitted as standard
• Favorites • Power cord for US and EU (when shipped to China power cord for
• Single Wavelength CN)

• Multi Wavelength • Universal cell adapter

• Wavelength Scan • Operator RFID tag (not available on all models)

• Time course • 1 Inch cells, matched pair

The DR 6000 spectrophotometer provides digital readouts of • Basic DR 6000 user manual, LINK2SC user manual
concentration, absorbance and percent transmittance. Further information, detailed user manuals and documentation are
When selecting a user-generated or programmed method, the menus available on the website of the manufacturer.
and prompts serve to direct the user through the test. Note: If any of these items are missing or damaged, please contact the
This menu system can also produce reports, statistical evaluations of manufacturer or a sales representative immediately.
generated calibration curves and reports on instrument diagnostic
checks. Operating environment
Observe the following points so that the device functions faultlessly and
thus has a long service life.

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• Place the device securely on an even surface. Push no objects Front and back view
under the device.
Figure 1 Front view
• Position the device so that the power cord is not impaired.
• The ambient temperature must be 10–40 °C (50–104 °F).

NOTICE
Protect the instrument from extreme temperatures from heaters, direct sunlight
and other heat sources.

• The relative humidity should be less than 80%; moisture should not
condense on the instrument.
• Leave at least a 15 cm clearance at the top and on all sides for air
circulation to avoid overheating of electrical parts.
• Do not use or store the device in extremely dusty, humid or wet
places.
• Keep the surface of the instrument, the cell compartment and all
accessories clean and dry at all times. Immediately remove
splashes or spilt materials on or in the instrument (refer to
Maintenance, page 26).

5 Touch screen 1 USB port type A

6 Power save key 2 Cell compartment cover

7 RFID module (not available on all 3 Lamp compartment cover

models) 4 Fan outlet

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 Figure 2 Back view Power connections

NOTICE
Use only a grounded socket for the connection of this device to the power supply.
If you are not sure if the sockets are grounded, have this checked by a qualified
electrician. The power plug serves in addition to the power supply to isolate the
device quickly from the power source where necessary. During the disconnection
from the power source it must be made sure that the correct power plug is pulled
(for example by labeling the sockets). This is recommended for long-term storage
and can prevent potential dangers in the event of a fault. Therefore make sure
that the socket to which the device is connected is easy to reach by each user at
all times.

WA R N I N G
Electrical dangers and fire hazard.
Only use the supplied power cable.

1. Plug the power cable into the back of the instrument (Back view,
page 9).
2. Insert the plug of the power cable into a grounded mains socket
(100–240 V~ / 50–60 Hz).
3. Switch the power button to "On" to turn on the instrument (Back
4 USB port type B 1 On/off switch view, page 9).
5 USB port type A 2 Socket for power cable
6 Filter pad cover 3 Ethernet port

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How to position the universal cell adapter Startup
1. Open the cell compartment.
2. Raise the universal cell adapter by approx. 1 cm. Switch on the instrument, startup process
3. Rotate the universal cell adapter such that the guide of the required 1. Connect the power cable to a power socket.
cell profile faces left toward the cell compartment (1). 2. Switch on the instrument via the power switch on the back.
4. Press the universal cell adapter down until it snaps into place. 3. The device automatically starts an approximately 45 second long
startup process. The display shows the logo of the manufacturer. At
Figure 3 How to position the universal cell adapter the end of the startup process, a startup melody is heard.
Note: Wait approximately 20 seconds before switching on again so as
not to damage the electronics and mechanics of the instrument.

Language selection

The DR 6000 software includes several language options. The first time
the instrument is switched on, the language selection screen will be
shown automatically after the startup process.
1. Select the required language.
2. Press OK to confirm the language selection. The self-check will
then start automatically.

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Change the language setting Sleep mode
The device works in the selected language until the option is changed.
1. Turn the instrument on.
2. During the startup process, touch the display at any point until
(approximately 45 seconds) the list for the selection of a language
is shown.
3. Select the required language.
4. Press OK to confirm the language selection. The self-check will
then start automatically.

Self-check

The instrument can be put into sleep mode.

1. Press the power save key beneath the display.
The "Sleep mode" message is shown. The display will then switch
off automatically.
2. Press the power save key again to switch back on.
The self-check will start automatically.
After that, the instrument is ready to use.

Power off the instrument

1. Press the power switch on the back of the instrument.
Each time the instrument is powered up, a test program begins.
This procedure, which takes approximately two minutes, checks the
system, lamp, filter adjustment, wavelength calibration and voltage.
Each checked function is marked accordingly on the display.
The Main Menu is displayed when diagnostics are completed.
Note: In the event of further error messages during the test program,
refer to Troubleshooting, page 27.

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Standard programs This display is used to enter letters, numbers and symbols as needed
when programming the instrument. Unavailable options are disabled
(grayed out). The symbols left and right on the display are described in
Overview Table 1.
Tips for using the touch screen The designations of the center keypad change according to the selected
The entire display reacts to touch. Make selections by tapping with a entry function. Touch each key repeatedly until the required character is
shown on the display. A space can be entered by using the underscore
fingernail, fingertip, eraser or stylus. Do not touch the display with sharp
on the YZ_ key.
objects (for example a ballpoint pen tip).
Press Cancel to cancel an entry, or press OK to confirm an entry.
• Do not place anything on top of the screen, to prevent damage or
scratches on the screen. Note: It is also possible to use a USB keyboard (with US keyboard
• Press buttons, words or icons to select them. layout) or a hand-held USB barcode scanner (refer to Replacement
parts, page 30).
• Use scroll bars to move up and down long lists very quickly. Press
and hold the scroll bar, then move up or down to move through the Table 1 Alphanumeric keypad
list.
• Highlight an item from a list by pressing it once. When the item has Function Description Icon / key
been successfully selected, it will be displayed as reversed text Toggles the character input mode between upper
(light text on a dark background). Alphabetic ABC/abc
and lower case.

Use of the alphanumeric keypad Punctuation, symbols and numerical sub- and
Symbols #%
superscripts may be entered.

For entering regular numbers. Numeric 123

Clear the entry. Clear Entry CE

Deletes the current character and goes back one

Back key Left Arrow
position.
Right
Navigates to the next space in an entry. Next
Arrow

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 Main menu Table 2 Main Menu options
Function Option

User programs make "made to measure analysis" possible:

• Users can program methods they have
developed themselves
• Existing HACH- and HACH-LANGE procedures User Programs
can be stored as user programs. These
procedures can then be modified according to
separate requirements.
List of methods/tests created by the user to suit his own
Favorites
requirements.
Single wavelength readings are:
Absorbance readings: The light absorbed by the sample is
measured in absorbance units.
Transmittance reading (%): Measures the percent of the Single
original light that passes through the sample and reaches the Wavelength
A variety of modes may be selected from the Main Menu. The following detector.
table briefly describes each menu option. Concentration readings: A concentration factor can be
You find a toolbar on the right in the display. Press to activate the entered to enable the measured absorbance values to be
various functions. converted into concentration values.
In the Multi Wavelength mode, absorbance (Abs) or
Table 2 Main Menu options percentage transmittance (%T) is measured at up to four
Multi
wavelengths and absorbance differences and absorbance
Function Option Wavelength
relationships are calculated. Simple conversions into
concentrations can also be carried out.
Stored programs are pre-programmed methods that make
use of HACH chemicals and HACH-LANGE pipette tests. Stored A wavelength scan shows how the light from a sample is
The working procedures for HACH-LANGE tests are Programs / absorbed over a defined wavelength spectrum. This function
included in the test packs. Additional information is available Barcode can be used to determine the wavelength at which the Wavelength
on the manufacturer's website. Programs maximum absorbance value can be measured. The Scan
Further information, as well as illustrated, step-by-step pro- (HACH-LANGE absorbance behavior is displayed graphically during the
cess instructions for analyses using HACH programs, are programs) scan.
available on the website of the manufacturer. The time scan records the absorbance or % transmittance at
Time course
a wavelength over a defined time.
The "System check" menu offers a number of options,
including optical checks, output checks, lamp history,
System checks
instrument update, service time, settings for analytical quality
assurance and instrument backup.

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 Table 2 Main Menu options Recall stored data from the data log
Function Option

Recall
Stored data can be called up, filtered, sent and deleted. measurement
data

In this mode, user-specific or method-specific settings can

Instrument
be entered: operator ID, sample ID, date & time, sound, PC
Setup
& printer, password, energy-saving mode and stored data.

Save, recall, send and delete data

The data log
The data log can store up to 5000 readings saved by the following
programs:
• Stored Programs,
• Barcode Programs, 1. Press Recall Data in the Main Menu.
• User programs,
• Favorites,
• Single Wavelength and
• Multi Wavelength.
A complete record of the analysis is stored, including the Date, Time,
Results, Sample ID and Operator ID.

2. Press Data Log.

A listing of the stored data is displayed.

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3. Press Filter: On/Off. 5. Press OK to confirm the selection.
The function Filter Settings is used to search for specific items. The chosen items are listed.
4. Activate On. The data can now be filtered using the following
selection criteria. Send data from the data log
• Sample ID Data is sent from the internal data log as an XML (Extensible Markup
• Operator ID Language) file or as a CSV (Comma Separated Value) file, to a directory
with the name DataLog on a USB mass storage device or a network
• Start Date drive. The file can then be processed using a spreadsheet program. The
• Parameter file name has the format: DLYear-Month-
or any combination of the four. Day_Hour_Minute_Second.csv or DLYear-Month-
Day_Hour_Minute_Second.xml.

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 4. Tap on Options and then on the
PC & Printer symbol.

1. Plug the USB storage device into the USB A interface on the
DR 6000 or connect the DR 6000 with a network drive.
2. Press Recall Data from the Main Menu. 5. Select the data to be sent.
3. Select the data category to be transferred, e.g. Data Log. The following options are available:
• Single point: only this selected reading will be sent
A list of the selected measurement data is displayed.
• Filtered data: only readings that correspond to the set filters
will be sent
• All data: all data in the selected data category will be sent.
6. Press OK to confirm.
Note: The number in parentheses is the total number of data sets
assigned to this selection.

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Stored Programs 4. Follow the chemical procedural instructions. Further information are
available on the website of the manufacturer.
Over 200 pre-programmed processes can be recalled via the Stored
Programs menu. Stored Programs do not include any barcode tests. Note: To display the procedural instructions in the display, press the
info icon. This option is not available for all tests.
Select a saved test/method; entering user-specific basic
data Analysis of samples

1. Press Stored Programs in the Main Menu to view an alphabetical 1. Press Stored Programs and select a program.
list of stored programs with program numbers. Note: If available, the procedural instruction is indicated on the
The "Stored Programs" list will appear. display via the Info icon.
2. Highlight the required test. 2. Insert the zero solution cell into the cell compartment.
Note: Select the program by name or scroll through the list using 3. Press Zero.
the arrow keys. Highlight the program or press Select by No. to
search for a specific program number. Press OK to confirm.
3. Press Start to run the program. The respective measurement
window is displayed.
Note: All corresponding data (wavelength, factors and constants) is
already preset.

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 Perform a barcode test

4. Remove the zero solution cell from the cell compartment. Insert the
sample cell into the cell compartment.
1. Prepare the barcode test in accordance with the work instruction
5. Press Read. The result will be displayed. and insert the cell into the cell compartment (1).
Note: To define a sample dilution, press the Dilution key in the • When a coded cell is inserted into the cell compartment (1)
toolbar. (How to position the universal cell adapter, page 10), the
corresponding measurement program is automatically
6. For data storage, refer to section The data log, page 14. activated in the main menu.

Barcode Programs
A special barcode reader in cell compartment #1 automatically reads the
barcode on the 13 mm cuvette/vial as the cuvette/vial completes a single
rotation. The instrument uses the barcode identification to automatically
set the correct wavelength for the analysis and calculates the result
immediately with the help of stored factors.
In addition, readings are recorded at 10 different positions during a
rotation. A special outlier-elimination program is run and then the
average of the measured values is calculated. Cell and round cell faults
and contaminations are detected and therefore a very precise result is
determined.

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 The measurement is started automatically and the results are shown.
Note: To define a sample dilution, press the Dilution key in the toolbar.
To evaluate other cell tests and other parameters insert the prepared cell
into the cell compartment and read off the result.
Note: The control bar, which is shown on the right on the display, shows
the relationship of the measurement result with the measurement range.
The blue bar shows the reading result independently of any dilution factor
that was entered.

Expanded programs
Single Wavelength (absorbance, concentration and
transmittance readings)
The Single Wavelength mode can be used in three ways. For sample
• Otherwise select in the main menu the menu option Barcode readings at a single wavelength, the instrument can be programmed to
Programs and insert a zero cell (depending on work measure the absorbance, % transmittance or concentration of the
instruction) into the cell compartment (1). analyte.
Note: To obtain further information on the Help Guide ("Information" • Absorbance readings: The light absorbed by the sample is
symbol). measured in absorbance units.
• % Transmittance measures the percent of the original light that
passes through the sample and reaches the detector.
• Turning on the concentration factor allows selection of a specific
multiplier for converting absorbance readings to concentration. In a
graph of concentration versus the absorbance, the concentration
factor is the slope of the line.

Set up Single Wavelength mode

1. Press Single Wavelength in the Main Menu.
2. Press Options for Parameter Setup.

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 Table 3 Options for Single Wavelength (Continued)
Table 3 Options for Single Wavelength
Description Options
Description Options
Single Reading: One measurement result is shown after
For further Options More tapping on Read.
Continuous Readings: After the zero measurement, all
Recall saved measurement data, wavelength scans or time readings are displayed automatically and continuously.
courses, refer to Save, recall, send and delete data, Recall Reading Mode
page 14. measurement data Carousel 1 inch square: Optional measurement of
symbol carousel insert with up to 5 square cells.
Carousel 1 cm square: Optional measurement of carousel
Switches from % transmittance to concentration or insert with up to 7 square cells.
% Trans/Abs
absorbance in reading mode.
Recall saved measurement data, wavelength scans or time
To input the wavelength setting. Use the alphanumeric Recall
courses, refer to Save, recall, send and delete data,
keypad to enter the reading wavelengths. A wavelength in λWavelength page 14.
measurement data
the range of 190–1100 nm can be entered.
Basic data of the instrument, refer to Save, recall, send and Instrument Setup
This functions as a stopwatch. It helps to make sure that
delete data, page 14. mode
the steps of an analysis are correctly timed (e. g. reaction
times, wait times, etc., can be exactly specified). When the Timer icon
specified time has elapsed, a sound is emitted. The use of
the timer has no influence on the reading program.
Multiplication factor for converting absorbance values into Concentration
concentration values. Factor: Off/On

Concentration
To select the number of decimal places.
Resolution
To store the selected parameters as a User Program, refer
to Single Wavelength (absorbance, concentration and Save as User
transmittance readings), page 19. Program

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Multi Wavelength mode – readings with more than one
wavelength
In the Multi Wavelength mode, absorbance values can be measured at
up to four wavelengths and the results can be mathematically processed
to obtain sums, differences and relationships.
• Absorbance readings: The light absorbed by the sample is
measured in absorbance units.
• % Transmittance measures the percent of the original light that
passes through the sample and reaches the detector.
• Turning on the concentration factor allows selection of a specific Table 4 Multi wavelength setup options
multiplier for converting absorbance readings to concentration. In a Description Options
graph of concentration versus the absorbance, the concentration
factor is the slope of the line. Concentration is calculated using a For further Options More
single factor for each wavelength, which is input by the user.
Recall saved measurement data, wavelength scans or time Recall
courses, refer to Save, recall, send and delete data, page 14. measurement
Set reading mode at different wavelengths data symbol
Press Multi Wavelength in the Main Menu. Press Options for
Switches from % transmittance to concentration or
Parameter Setup. % Trans/Abs
absorbance in reading mode.
To input the wavelength setting. Use the alphanumeric
keypad to enter the reading wavelengths. A wavelength in λWavelength
the range of 190–1100 nm can be entered.
This functions as a stopwatch. It helps to make sure that the
steps of an analysis are correctly timed (e. g. reaction times,
wait times, etc., can be exactly specified). When the Timer icon
specified time has elapsed, a sound is emitted. The use of
the timer has no influence on the reading program.
Multiplication factor for converting absorbance values into Concentration
concentration values. Factor

Concentration
To select the number of decimal places.
Resolution

Absorbance
Calculation basis for evaluating samples
Formula
To store the selected parameters as a User Program, refer to
Save as User
Single Wavelength (absorbance, concentration and
Program
transmittance readings), page 19.

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 Wavelength Scan mode – recording of absorbance
and transmission spectrums
In the Wavelength Scan mode, the absorbance of the light in a solution
over a defined wavelength spectrum is measured.
The reading results can be displayed as a curve, as percentage
transmittance (%T) or as Absorbance (Abs). The collected data can be
printed as a table or a curve.
The data is available for formatting changes. These include automatic
Table 4 Multi wavelength setup options (Continued) scaling and zoom functions. Maximum and minimum values are
determined and shown as a table.
Description Options
The cursor can be moved to any point on the curve for the purpose of
Single Reading: A single reading is displayed after Read is reading off the absorbance or transmittance value and the wavelength.
pressed. The data associated with each data point can also be shown as a table.
Carousel 1 inch square: Optional measurement of carousel
Reading Mode
insert with up to 5 square cells.
Carousel 1 cm square: Optional measurement of carousel
insert with up to 7 square cells.
Recall
Recall saved measurement data, wavelength scans or time
measurement
courses, see Save, recall, send and delete data, page 14.
data
Basic data of the instrument, refer to Single Wavelength
Instrument Setup
(absorbance, concentration and transmittance readings),
mode
page 19.

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 Set up the wavelength scan
Press Wavelength Scan in the Main Menu. Press Options for
Parameter Setup.

Table 5 Options during wavelength scan (Continued)

Description Option
To select Track or Peak/Valley. The selection for this menu
Table 5 Options during wavelength scan option determines to which points on the graph the cursor Cursor Mode
moves.
Description Option
To send data to a printer, computer or USB memory stick
Send Data
Further options are displayed More (Type A)
The integral gives the area and the derivative of the integral
To store the scan data Folder icon Integral: On/Off
gives the original function
From the displayed list of stored scans, a record is selected Scale: In the automatic scaling mode, the y-axis is
for use as a reference scan/superimposed scan. This can be automatically adapted so that the total scan is shown.
highlighted or shown in the background in comparison with The manual Scaling mode allows sections of the scan to be Scale & Units
the actual measured scan. Reference Off/On displayed.
Units: Choice of absorbance or transmittance.
Note: This option is only available when there are
stored scans with the same wavelength range and Single Reading: One measurement result is shown after
step. tapping on Read.
Carousel 1 inch square: Optional measurement of carousel
Enter the wavelength spectrum and scan interval λ insert with up to 5 square cells.
Reading Mode

This functions as a stopwatch. It helps to make sure that the Carousel 1 cm square: Optional measurement of carousel
steps of an analysis are correctly timed (e. g. reaction times, insert with up to 7 square cells.
wait times, etc., can be exactly specified). When the Timer icon
Recall
specified time has elapsed, a sound is emitted. The use of Recall saved measurement data, wave-length scans or time
measurement
the timer has no influence on the reading program. courses, see Save, recall, send and delete data, page 14.
data
Enables the switching between the display of tabular scan
data (wavelength/absorbance) and the graphical Basic data of the instrument, refer to Save, recall, send and Instrument Setup
representation of the curve. View delete data, page 14. mode
Table/Graph
Note: "View Table" is activated after the first
measurement.

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Perform a wavelength scan
After selecting all scan parameters, record a base line (initial zero
reading). If a scan parameter is changed, a new base line must be
recorded. After the scan of the baseline the device is ready for the
scanning of one or several samples.

3. Press Zero.
"Zeroing" is shown below the graph as the baseline scan begins.
4. Insert the prepared analysis cell into the cell compartment and
close the cell compartment cover.
5. Press Read.
1. Select in the main menu the menu option Wavelength Scan. Under the graph, the display "Reading..." appears, and a graph of
2. Insert the zero solution cell in the cell compartment and close the the absorbance or transmission values for the scanned wavelengths
cell compartment cover. is continuously displayed.

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 Time course of absorbance/transmittance
The Time Course mode is used to collect data in either absorbance or
transmittance for a user-specified length of time. This data can be
displayed in either a graph or a table.

Time course setup parameters

1. Press Time Course mode in the Main Menu.
2. Press Options to configure parameters.

The Wavelength Scan is complete, if

• the graph is shown full-size,
• the scaling of the x-axis occurs automatically,
Table 6 Time course options
• the Cursor functions in the vertical navigation bar are
highlighted. Description Options
• a sound is emitted For further options More
• To save the scan, press Options > Store symbol.
To store the scan data Folder icon
To input the total time for data collection and the time interval
Time & Interval
between the collection of data points
To input the wavelength setting λ
To display readings in absorbance, transmittance or
concentration. This can be changed after sample data is View Table
collected
This functions as a stopwatch. It helps to make sure that the
steps of an analysis are correctly timed (e. g. reaction times,
wait times, etc., can be exactly specified). When the Timer icon
specified time has elapsed, a sound is emitted. The use of
the timer has no influence on the reading program.

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 Maintenance

CAUTION
Potential Chemical, Biological Eye and Skin Hazards.
Only qualified personnel should conduct the tasks described in this section of the
manual.

Table 6 Time course options (Continued) NOTICE

Remove all cells remaining in the instrument. Dispose of the cells or their
Description Options contents in an authorised manner.
Scale: In the automatic Scaling mode, the y-axis is
automatically adjusted so that the total scan is displayed. Lamp replacement
The manual Scaling mode allows sections of the scan to be Scale & Units
displayed.
Units: Choice of absorbance or transmittance.
DANGER
To send Data to a printer, computer or USB memory stick
Send Data
(Type
Risk A)
of electric shock
Disconnect the instrument
Single Reading: from the power
One measurement source
result before
is shown the lamp replacement
after
procedure
tapping onis commenced
Read. and until the lamp replacement procedure is complete.
Carousel 1 inch square: Optional measurement of carousel
Reading Mode
insert with up to 5 square cells.

CAUTION
Carousel 1 cm square: Optional measurement of carousel
insert with up to 7 square cells.
Burn hazard.
Recall saved measurement data, wave-length scans or time Recall
Wait until the
courses, seelamp cools
Save, down.
recall, Contact
send with the
and delete hotpage
data, lamp14.
can cause burns.
measurement
data

Basic data of the instrument. Instrument Setup

NOTICE
Only hold lamp at lamp holder. Avoid touching the glass, as substances on the
skin can bake onto the lamp bulb and thus accelerate the ageing process of the
lamp.

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Troubleshooting Resolution Cause Error displayed

Fault
Resolution Cause Error displayed Check the lamp and Test program stopped!
replace it if necessary. Test program stops when Please check lamp
Test execution errors Close lid. the instrument is started
Close the lid.
Press Start Again.
Reinsert the cell. Error [xx]
If the barcode is not Barcode faulty Barcode label not read
recognised, contact Fault
Remove the cuvette/
technical support. Test program stopped!
sample cell from the cell Test program stops when Please remove the
compartment. the instrument is started
Close the cover. Please close the cover. cuvette
Press OK.
Close the lid.
Dilute sample and The measured
Absorbance > 3.5!
measure again absorbance exceeds 3.5
Error
Fault Contact technical support Selfcheck stopped.
Barcode check and indicate the error Electronic defect
Deviation to the stored number Hardware error.
Update program data number?
data Error [x]
Please update program
data!
Error
Switch the instrument off Too much ambient
Decrease ambient light. The instrument sensors
and then back on again. It’s recommended to light!
Check of the air values (Avoid direct sunlight.) detects too much
If the system check is not execute a Full System Move instrument into
failed Close lid. ambient light.
successful, contact Check shade
technical support.
or close the lid
Blank value correction
Blank value correction
not possible with No help function is
not possible!
LCW919. available for this
program.
Fault
Program not The analysis is possibly
Shelf life exceeded!
Update program data Barcode test not present accessible. erroneous. Use new
Use chemicals?
Please update program chemicals
data!
Check programming Error in the test database
No evaluation!
The cuvette is dirty or Contact technical support / user database
Clean the cuvette; allow Fault
there are undissolved
the particles to settle Clean cuvette! Reinsert the cell.
particles in the cuvette
If the barcode is not No barcode found No barcode!
recognised, contact
technical support.

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Resolution Cause Error displayed Resolution Cause Error displayed

Forgotten your The analysis is possibly

Possible interference
password? erroneous due to Interference Check
Password incorrect Entry invalid! from:
Contact technical interferences.
support. Contact technical support
Data analysis not for an inspection of the Next service is due!
No valid data for these instrument.
Change the selection. possible, no
parameters!
measurement data Check concentration of The calculated result is
Negative result!
View Data not possible in sample negative
Change the selection. No valid data found!
data log
Avoid direct sunlight at Unstable lighting
No help function the measuring location. conditions!
present.
Switch the instrument off
Data analysis settings and then back on again.
Measurement of air System check
cannot be configured No measurement data If the system check is not
Change the selection. values failed incorrect!
without measurement present! successful, contact
data. technical support.

This is a warning notice. Switch of the instrument

Data analysis limits not Control range not and allow it to cool for a Temperature too high.
The control limit set was
reached reached! few minutes. If Measurement not
not reached.
necessary, move it to a possible!
This is a warning notice. cooler place.
Data analysis limits Control range
The control limit was
exceeded. exceeded!
exceeded. Update errors
Dilute sample and Calculated concentration
Concentration too high! Start the procedure again An error occurred
measure again is higher than 999999
or contact technical when uploading the
The measured support. instrument data.
Dilute sample and absorbance is above the
Over measuring range
measure again calibration range of the Start the procedure again An error occurred when
test or contact technical reading from the USB
support. memory stick.
If possible, select a test The measured
with a lower reading absorbance is below the
Under measuring range Start the procedure again An error occurred when
range or use a cuvette calibration range of the
or contact technical writing to the USB
with a longer path length test
support. memory stick.
The analysis is possibly
Possible interference
erroneous due to Interference Check Check the USB memory Please check on the
by: Error during update.
interferences. stick. current update file.

Please contact
Error during update.
Customer Service.

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Resolution Cause Error displayed Resolution Cause Error displayed

Insert a USB memory Network setup: default

Please insert the USB Try to create the Error during default
stick into a USB A port gateway cannot be set
memory stick. connection again. gateway setup.
on the instrument. for fixed IP address

Check the USB memory File for instrument Error during network
Error during update. Check the settings. setup Error during network
stick. update missing.
Define target directory. The target directory does drive setup!
Save the update file not exist.
File for instrument
again and repeat the Error during update.
update is faulty. Network setup: Subnet
procedure. Enter the subnet mask Error during subnet
mask cannot be set for
Start the procedure again again. mask setup.
Error copying from USB fixed IP address
or contact technical Error during update
memory stick. Make sure that the
support. Error in FTP
instrument is connected FTP error
connection.
Check the USB memory No instrument backup to the network.
stick. present!
Network setup off, when
Activate the online
access to instruments Network switched off.
Select a memory with Insufficient memory for connection.
Error during update. homepage via sidebar
more space. update .
Make sure that the
Save the update file instrument is connected
again and repeat the Error during update. Update file is faulty. to the network. Error during network Remote server cannot
procedure. setup be reached.
The fixed address of the
Check the USB memory USB memory stick is DR 6000 is not accepted.
Update not possible.
stick. not connected. The fixed address of the
Switch to "Automatic".
DR 6000 is not accepted. Remote server
Network connection errors Enter the correct server
The server name entered unreachable!
name.
is incorrect.
Please check network
configuration. Try the connection again Instruments homepage Web server cannot be
later. cannot be reached. reached.
Please check the
connection.

Please check the

Network setup or FTP
connection and contact
error
the administrator.

Network setup: DHCP

Enter the IP address Error when calling up
client has no connection
again. the local IP address.
to the DHCP server

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Replacement parts

Description Cat. No.

Halogen lamp A23778

Deuterium lamp A23792
LZV902.99.0002
Universal cell adapter
0
Power cord EU YAA080
Power cord CH XLH051
Power cord UK XLH057
Power cord US 1801000
Power cable China/Australia XLH069
Fuse A23772
Filter pad LZV915
Dust cover LZV886
USB interface protection LZV881

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