IS 73:2006

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Indian Standard
PAVING BITUMEN SPECIFICATION ( Third Revision)

lCS 93.080.20

0 BIS 2006

BUREAU

OF

INDIAN

STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARC NEW DELHI 110002

2006

Price Group 2

Bitumen, Tar and Their Products Sectional Committee, PCD 6

FOREWORD This Indian Standard (Third Revision) was adopted by the Bureau of Indian Standards, after the draft finalized by the Bitumen, Tar and Their Products Sectional Committee had been approved by the Petroleum, Coal and Related Products Division Council. This standard was first published in 1950 as Specification for asphaltic bitumen and fluxed native asphalt for road making purpose which was revised in 1961 to change the grades of material and incorporate the methods of test as per 1S 1201 to IS 1220:1958 Methods for testing tar and bitumen. In the first revision, the grades of fluxed native asphalt were deleted and essentially the paving grades were included. Based on the revised methods of test in IS 1201 to IS 1220:1978 Methods for testing tar and bituminous materials (first revision) and the additional data that had become available, second revision was prepared in 1992. Bituminous mixes prepared with binders having high wax content have tendencies to become brittle in cold weather and to bleed in hot weather. In the second revision, separate tables of requirements of paving grade bitumen derived from waxy crude and non-waxy crude have been prepared. Requirements of performance tests like penetration ratio, paraffin wax content, and viscosity at 60C and 135C and retained penetration after thin film oven test have been incorporated. Besides, six grades of bitumen derived from waxy crude have been unified into four grades and in the case of bitumen from non-waxy crude, an additional grade of 50/60 penetration has been introduced on the basis of the data made available ilom a study carried out jointly by the Central Road Research Institute and the Indian Oil Corporation (R& D) Centre, Faridabad. In this third revision grading of bitumens is changed from penetration grade to viscosity grade. The variability in performance at high temperatures can be addressed by adopting a viscosity-graded bitumen specification (based on viscosity at 60C) in lieu of the current penetration-graded specification (based on penetration at 25C). Tender aspha[t mixtures, which push and shove under the roller wheels presenting problems during compaction, have also been encountered in the recent past. Since the viscosity-graded bitumen specification has a requirement of minimum viscosity at 135C, it will also be helpful in minimizing the tender mix problems in the field. Adoption of viscosity-graded paving bitumen specification will also reduce the number of total tests to 7, which will reduce the cost of testing bitumen. This will result from eliminating empirical tests/parameters such as -penetration ratio, paraftln wax content, and Fraass breaking point without compromising the qua] ity of bitumen. Also, no new tests need to be introduced in implementing this specification. Since high penetration values are desirable for pavement durability, requirement for a minimum penetration value is adequate and has been retained in the viscosity-graded specification. Speci@ing a maximum value for penetration is undesirable and will reject some good quality bitumens unreasonably. This standard is one of the series of standards on bitumen. Other specifications so far published in this series are:
IS No. 7Me

217:1988 454:1994 702:1988

Specification for cutback bitumen (second revision) Cutback bitumen tlom waxy crude Specification (second revision) Specification for industrial bitumen (second revision)

For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded off in accordance with IS 2: 19.60Rules for rounding off numerical values (revised,). The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.

IS 73:2006

Indian Standard
PAVING BITUMEN SPECIFICATION (Third Revision)
1 SCOPE This standard covers the requirement for physico-chemical properties of various grades of paving grade bitumen for use as binders in the construction of pavements related to highways, expressways, air fields, rural roads and other allied construction and maintenance works. 2 REFERENCES The following standards contain provisions, which through reference in W texg constitute provisions ofthis standard. At the time of publication the editions indicated were valid. All standards are subject to revision and parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below: IS No. 334:2002 1201: 1203: 978 978
Title Glossary of terms relating to bitumen and tar (third revision)

3 TERMINOLOGY

For the purpose of this standard, the definitions given in [S 334 shall apply. 4 DESCRIPTION Bitumens shall be prepared by the refining of crude petroleum by suitable methods using appropriate crude or by blending different crudes or different short residue to achieve desired properties of paving grade bitumen conforming to specifications.
S GRADES

Bitumens shall be classified into four types, .bas.edon viscosity, as given below: a) VG-I O b) VG-20
C)

VG-30

d) VG-40 6 REQUIREMENTS 6.-1 The paving bitumen binder shall be homogeneous and shall not foam when heated to 175C. 6.2 The various grades of bitumen shall conform to the requirements prescribed in Table 1. 7 SAMPLING AND CRITERIA FOR CONFORMITY 7.1 Lot In any consignment, all the containers of paving grade bitumen binders of same category and grade from the same batch of manufacture shall be grouped to constitute a lot. 7.2 The number of containers to be selected at random from the lot shall depend upon the size of the lot given in Table 2 7.3 From each of the containers selected as in 7.2 an average sample representative of the material in the container shall be drawn in accordance with the methods prescribed in IS 1201, taking all the precautions mentioned therein. All these samples from individual containers shall be stored separately. 1

Methods for testing tar and bituminous materials: Sampling (first revision) Methods of testing tar and-bituminous materials: Determimtion of penetration
~rst revision)

1205:1978

Methods for testing tar and bituminous materials: Determination of softening point @st revision) Methods of testing tar and bituminous materials: Determination of viscosity:

1206

(Part 2): 1978 Absolute viscosity (Part 3): 1978 Kinematic viscosity 1208:1978 Methods for testing tar and bituminous materials: Determination of ductility
(first revision)

1269 :197.8

Methods for testing.tar and bituminous materials: Determination of flash point and fwe point (fwst revision) Methods for testing tar and bituminous materials: Determination of volubility in carbon disulphide or trichloroethylene
(first revision)

1216:1978

IS 73:2006

Table 1 Requirements for Paving Bitumen (Clause 6.2)

SI
No,
(1) i)

Characteristics
VG 10

(2)
Absolute viscosity at Poises,A4in 60C, Kinematic viscosity at 135C, cSt, Min Flash point, (Cleveland open cup), C. &fin Volubility in trichloroethylene, percent, WI Penetration at 25C, 100g,5s,0.1 mm Softening point (R&B), C, Min Testson residue from thinfilm oven tests/RTFOT 1) Viscosity ratio at 6&C, M-Y Ductility at 25C, cm, L@ afier thin-film oven test

(3)
800

Paving Grades VG 20 VG 30 (4) (5)

VG 40

Methods of Test, Ref to IS No. (7) IS 1206 (Part 2)

(6)

2400

3200
400

ii)

250

300

350

IS 1206 (Part 3)

iii)

220

220

220

220

IS 1209

iv)

99.0

99.0

99.0

99.0

IS 1216

v)

80-100

60-80

50-70

40-60

IS 1203

vi)

40

45

47

50

IS 1205

vii)

4,0

4.0

4.0

4.0

IS 1206 (Part 2)

2)

75

50

40

25

IS 1208

Table 2 State of Sampling (Clause 7.2)

7.5.1 The lot shall be considered as conforming to the requirements of this standard, if the conditions mentioned under 7.5.2 and 7.5.3 are satisfied. 7.5.2 From Ihe test results of absolute viscosity at 60C, penetration and softening point, the mean (~) and the range (R) shall be calculated. The following conditions shall be satisfied: a) [~ 0.6ft] shall be greater than or equal to the minimum specification limit specified in Table 1, and b) [~ + -0.6 R] shall be less than or equal to the maximum specification limit -specified in Table 1. 7.5.3 The composite sample when tested for the characteristics mentioned in 7.4.2 shall satisfy the corresponding requirements of the characteristics given in Table 1. 8 PACKING AND MARKING 8.1 Packing Penetration grade bitumen of all types shall be suitably packed in a container as agreed to between the purchaser and the supplier. 2

Lot Size (2)

No. of Containers to be Selected (3)

7.4 Number of Tests 7.4.1 All the individual samples-shall be tested for absolute viscosity at 60C, penetration and sot?ening point tests. 7.4.2 For the remaining characteristics, a composite sample prepared by mixing together equal quantities of paving grade bitumen, sampled, as the case may be, from all individual samples taken from each sample container, shall be tested. 7.5 Criteria for Conformity

IS 73:2006 8.2 Marking Each container of penetration grade bitumen shall be legibly and indelibly marked with the following a) b) c) d) Manufacturers name or trade-mark, if any; Month and year of-manufacture; T~e of the material and Grade; and Batch number. 8.3 BIS Certification Marking The container may also be marked with the Standard Mark. 8.3.1 The use of Standard Mark is governed by the provisions of the Bureau of Indian Standarh Act, 1986 and the Rules and Regulations made thereunder. The details of conditions under which the Iicence for the use of the Standard Mark may be granted to manufactures or producers may be obtained from the Bureau of Indian Standards.

Bureau of Indian Standards

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Amendments Issued Since Publication Amend No. Date of Issue Text Affected

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